Method and apparatus for separation of mixture

Patent metadata

Field	Value
Publication number	US-9561511-B2
Application number	US-201214239657-A
Country	US
Kind code	B2
Filing date	Aug 24, 2012
Priority date	Aug 25, 2011
Publication date	Feb 7, 2017
Grant date	Feb 7, 2017

Abstract

The present invention is a method for applying a gradient magnetic field to a paramagnetic supporting liquid containing a mixture of first particles and second particles to separate the mixture by particle type. A magnetic susceptibility of the first particles is lower than that of the liquid, and a magnetic susceptibility of the second particles is higher than that of the liquid. A gradient magnetic field is applied to the liquid in a separation tank provided with a magnetic filter and the liquid is stirred. The first particles float in the liquid by a magneto-Archimedes effect. A horizontal magnetic force acts on the first particles by the gradient magnetic field, so that the first particles travel to a region lateral to or outward from the magnetic filter and are gathered in the region. The magnetic filter is excited by the gradient magnetic field to catch the second particles.

First claim

The invention claimed is:

1. A mixture separation method for applying a gradient magnetic field to a paramagnetic supporting liquid containing a mixture of first particles and second particles of different types to separate the mixture by particle type,
wherein a magnetic susceptibility of the first particles is lower than a magnetic susceptibility of the supporting liquid, and
a magnetic susceptibility of the second particles is higher than the magnetic susceptibility of the supporting liquid,
the mixture separation method comprising:
applying the gradient magnetic field to the supporting liquid in a separation tank provided with a magnetic filter and stirring the supporting liquid;
applying the gradient magnetic field so that the first particles float in the supporting liquid or at a liquid surface thereof by the magneto-Archimedes effect, at least over the magnetic filter; and
catching the second particles in the supporting liquid with the magnetic filter excited by the gradient magnetic field.

2. The mixture separation method according to claim 1 , wherein a horizontal magnetic force acts on the first particles by the gradient magnetic field, and the first particles travel to a region lateral to or outward from the magnetic filter by the magnetic force and are gathered in the region.

3. The mixture separation method according to claim 1 , wherein the first particles are all disposed at a single elevation in the supporting liquid.

4. The mixture separation method according to claim 1 , wherein the gradient magnetic field is axially symmetrical about a central axis in a vertical direction, a magnetic field gradient of the gradient magnetic field has a component of a vertical direction and a component of a radial direction, and a magnetic force in a radial direction is applied to the first particles so that the first particles move away from the central axis by applying the gradient magnetic field to the supporting liquid.

5. The mixture separation method according to claim 1 , wherein the first particles are formed of a diamagnetic substance or a paramagnetic substance, the second particles are formed of a paramagnetic substance or an antiferromagnetic substance, and the supporting liquid is an aqueous solution of a paramagnetic inorganic salt.

6. The mixture separation method according to claim 1 , wherein the magnetic includes a net plate formed of a ferromagnetic substance, and the gradient magnetic field is applied orthogonally to the net plate.

7. A mixture separation method for applying a gradient magnetic field to a paramagnetic supporting liquid containing a mixture of first particles and second particles of different types to separate the first particles or the second particles from the mixture,
wherein a magnetic susceptibility of the first particles is lower than a magnetic susceptibility of the supporting liquid, and
a magnetic susceptibility of the second particles is higher than the magnetic susceptibility of the supporting liquid,
the mixture separation method comprising:
applying the gradient magnetic field to the supporting liquid in a separation tank provided with a magnetic filter and stirring the supporting liquid;
applying the gradient magnetic field so that the first particles float in the supporting liquid or at a liquid surface thereof by the magneto-Archimedes effect, at least over the magnetic filter; and
catching the second particles in the supporting liquid with the magnetic filter excited by the gradient magnetic field.

8. The mixture separation method according to claim 7 , wherein a horizontal magnetic force acts on the first particles by the gradient magnetic field, and the first particles travel to a region lateral to or outward from the magnetic filter by the magnetic force and are gathered in the region.

9. The mixture separation method according to claim 7 , wherein the first particles are disposed at the same elevation in the supporting liquid.

10. The mixture separation method according to claim 7 , wherein the gradient magnetic field is axially symmetrical about a central axis in a vertical direction, a magnetic field gradient of the gradient magnetic field has a component of a vertical direction and a component of a radial direction, and a magnetic force in a radial direction is applied to the first particles so that the first particles move away from the central axis by applying the gradient magnetic field to the supporting liquid.

11. The mixture separation method according to claim 7 , wherein the first particles are formed of a diamagnetic substance or a paramagnetic substance, the second particles are formed of a paramagnetic substance or an antiferromagnetic substance, and the supporting liquid is an aqueous solution of a paramagnetic inorganic salt.

12. The mixture separation method according to claim 7 , wherein the magnetic filter includes a net plate formed of a ferromagnetic substance, and the gradient magnetic field is applied orthogonally to the net plate.

Assignees

• Nishijima Shigehiro
• MISHIMA Fumihito
• Kaiso Koji
• Shimakawa Toshihiro
• Ube Industries
• Univ Osaka

Inventors

• Nishijima Shigehiro
• MISHIMA Fumihito
• Kaiso Koji
• Shimakawa Toshihiro

Classifications

• B03C1/32 Primary

  acting on the medium containing the substance being separated, e.g. magneto-gravimetric-, magnetohydrostatic-, or magnetohydrodynamic separation · CPC title

• B03C2201/18

  Magnetic separation whereby the particles are suspended in a liquid · CPC title

• B03C1/032

  Matrix cleaning systems · CPC title

• B03C1/30

  Combinations with other devices, not otherwise provided for · CPC title

• B03C1/286

  disposed at the inner circumference of a recipient, e.g. magnetic drain bolt · CPC title