Ultra-refractory material that is stable in a wet environment, and process for manufacturing same

Patent metadata

Field	Value
Publication number	US-9340460-B2
Application number	US-201214241948-A
Country	US
Kind code	B2
Filing date	Aug 6, 2012
Priority date	Aug 31, 2011
Publication date	May 17, 2016
Grant date	May 17, 2016

Abstract

A refractory material withstanding high temperatures in an oxidizing medium contains at least hafnium boride and tantalum boride, hafnium and tantalum being present in the refractory material exclusively in compound form.

First claim

The invention claimed is:

1. A refractory material containing:
50% by volume HfB 2 ;
25% by volume HfC; and
25% by volume TaB 2 .

2. A refractory part, the part being wherein it is constituted by a refractory material according to claim 1 .

3. A part comprising a substrate made up of a determined material, said part being provided with a protective coating for providing protection, the part being wherein said protective coating is constituted by a refractory material according to claim 1 .

4. The part according to claim 3 , wherein the substrate is made of a monolithic ceramic material based on silicon carbide or of a monolithic material based on carbon, or of a ceramic matrix composite material comprising silicon carbide.

5. The part according to claim 3 , wherein the substrate is made of C/C composite material.

6. The part according to claim 5 , further comprising a layer of silicon carbide close to the C/C composite material of the substrate of said part and a layer of zirconium carbide or of hafnium carbide interposed between the silicon carbide layer and the protective coating.

7. A method of making a part out of refractory material, the method comprising:
making a composition containing:
50% by volume HfB 2 ;
25% by volume HfC;
25% by volume TaB 2 ; and

shaping the composition and densifying said composition.

8. A method of making a protective layer on a part comprising a substrate made of a determined material, said method comprising:
applying on the part a composition containing:
50% by volume HfB 2 ;
25% by volume HfC;
25% by volume TaB 2 ; and

densifying said composition.

9. The method according to claim 8 , wherein the substrate is made of monolithic ceramic material based on silicon carbide, or on monolithic material based on carbon, or of ceramic matrix composite material comprising silicon carbide.

10. The method according to claim 8 , wherein the substrate is made of C/C composite material.

11. The method according to claim 10 , further comprising forming a layer of silicon carbide close to the C/C composite material of the substrate of said part and forming a layer of zirconium carbide or of hafnium carbide interposed between the layer of silicon carbide and the protective layer.

Assignees

• Courcot Mendez Emilie
• Thebault Jacques
• Sauveroche Anne
• Herakles

Inventors

• Courcot Mendez Emilie
• Thebault Jacques
• Sauveroche Anne

Classifications

• C04B2235/6567

  Treatment time · CPC title

• C04B41/87

  Ceramics · CPC title

• C04B41/507

  Borides · CPC title

• C04B2235/3225

  Yttrium oxide or oxide-forming salts thereof · CPC title

• C04B2235/9684

  Oxidation resistance · CPC title