Inorganic-compound particles and process for producing same

Patent metadata

Field	Value
Publication number	US-9340431-B2
Application number	US-201314142199-A
Country	US
Kind code	B2
Filing date	Dec 27, 2013
Priority date	Mar 25, 2011
Publication date	May 17, 2016
Grant date	May 17, 2016

Abstract

A method of producing inorganic compound particles is provided. It includes a step of impregnating a melt liquid of second raw particles into first raw particles by heating a raw material including them at a temperature, which equals to or higher than an eutectic temperature between a region-II (solid-liquid phase range) and a region-I (solid phase range) in a phase diagram and lower than the melting temperature of the inorganic compound. The first raw particles contain an element with a melting point equals to or higher than a melting point of the inorganic compound. The second raw particles contain an element with a melting point lower than the inciting point of the inorganic compound. The method also includes a step of synthesizing inorganic compound particles by a synthetic reaction in the first raw particles between the elements contained in the first and second raw particles.

First claim

The invention claimed is:

1. A method of producing inorganic compound particles of a composite including Mg and Si, the method comprising the steps of:
impregnating a melt liquid of second raw particles into first raw particles by heating a raw material including the first raw particles, at least some of which contain Si as a major constituent element, and the second raw particles, which contain Mg as a major constituent element, at a temperature, which equals to or higher than an eutectic temperature between a region-II (solid-liquid phase range) and a region -I (solid phase range) in a phase diagram of Mg and Si, and lower than the melting temperature of the inorganic compound; and
synthesizing the inorganic compound particles by a reaction in the first raw particles between the element contained in the first raw particles and the element contained in the second raw particles wherein
heating in the step of impregnating is performed at a temperature of 650° C. or higher and lower than 945.6 ° C,
particle sizes of the first raw particles are more than 20 μm and equal to or less than 500 μm, and
particle sizes of the inorganic compound particles are more than 25 μm and equal to 1 mm or less after the step of synthesizing the inorganic compound particles.

2. The method of making inorganic compound particles according to claim 1 ,
wherein the first raw particles and the second raw particles are mixed in the raw material by an atomic ratio corresponding to the ratio of Si and Mg in the intended inorganic compound.

3. The method of producing inorganic compound particles according to claim 2 ,
wherein the first raw particles are mixtures including particles which consist of Si and particles which consist of elements other than Si.

4. The method of producing inorganic compound particles according to claim 2 ,
wherein the first raw particles are composite particles which consist of Si and elements other than Si.

5. The method of producing inorganic compound particles according to claim 1 ,
wherein the first raw particles are mixtures including particles which consist of Si and particles which consist of elements other than Si.

6. The method of producing inorganic compound particles according to claim 1 ,
wherein the first raw particles are composite particles which consist of Si and elements other than Si.

Assignees

• Nat Inst For Materials Science
• Mitsuba Corp

Inventors

• Isoda Yukihiro
• Shioda Naoki

Classifications

• Y10T428/2993

  Silicic or refractory material containing [e.g., tungsten oxide, glass, cement, etc.] · CPC title

• B22F2999/00

  Aspects linked to processes or compositions used in powder metallurgy · CPC title

• B22F9/04

  starting from solid material, e.g. by crushing, grinding or milling ({C22C1/1084 takes precedence}; crushing, grinding or milling, in general, see the relevant subclasses, e.g. B02C) · CPC title

• B22F2203/11

  temperature, temperature profile · CPC title

• B22F2201/013

  Hydrogen · CPC title