Apparatus and method for hydroconversion

Patent metadata

Field	Value
Publication number	US-9314759-B2
Application number	US-201414168099-A
Country	US
Kind code	B2
Filing date	Jan 30, 2014
Priority date	Jun 7, 2011
Publication date	Apr 19, 2016
Grant date	Apr 19, 2016

Abstract

An apparatus is disclosed for the hydroconversion of hydrocarbon feedstock with a hydrogen gas at elevated temperature and pressure with the use of a catalyst. The apparatus is a reactor vessel with a grid plate distributor for improved gas liquid distribution. The distributor comprises a grid plate and a bubble cap assembly with a plurality of tubular risers extending through the grid plate. Each tubular riser has an upper section above the grid plate and a lower section below the grid plate, the lower section terminated with an open bottom end for ingress of the hydrogen gas and hydrocarbon feedstock, the upper section having a closed top terminated with a housing cap. Each tubular riser has at least a vertical slot and a least a laterally placed opening sufficiently sized such that in operation, the liquid level in the zone below the grid plate is above the vertical slot and below the laterally placed opening.

First claim

What is claimed is:

1. A grid plate assembly for use in a hydroconversion reactor, comprising:
a grid plate having a top and a bottom dividing the hydroconversion reactor into a zone above the grid plate top and a zone below the grid plate bottom;
a plurality of tubular risers extending through the grid plate;
wherein each tubular riser comprises an upper section extending above the grid plate top and closed with a bubble cap and a lower section extending below the grid plate bottom and having an open end, at least one laterally placed vertical slot and at least one laterally placed opening,
wherein the at least one laterally placed vertical slot and the at least one laterally placed opening in each tubular riser are positioned at variable distances from the grid plate bottom such that an inclined liquid level in the zone below the grid plate bottom is maintained between the laterally placed vertical slot and the at least one laterally placed opening,
wherein the at least one laterally placed vertical slot extends from the open end of the lower section for a length ranging from ⅛ to ½ of the length of the lower section, and
wherein the laterally placed opening is located from 1 to 5″ below the grid plate bottom with a shortest dimension ranging from 1/16 to ½ of a diameter of the open bottom end of the tubular riser.

2. The grid plate assembly of claim 1 , wherein the laterally placed opening in each tubular riser has a shortest dimension ranging from ⅛ to ½″.

3. The grid plate assembly of claim 1 , wherein the upper section of each tubular riser comprises a constriction for gas liquid mixing in the tubular riser.

4. The grid plate assembly of claim 3 , further comprising a check valve located above the constriction in the upper section of each tubular riser.

5. The grid plate assembly of claim 4 , wherein the check valve in each tubular riser comprises a steel ball and a valve seat.

6. The grid plate assembly of claim 1 , wherein the bubble cap is tubular in shape.

7. The grid plate assembly of claim 1 , wherein the bubble cap is bell shaped.

8. The grid plate assembly of claim 1 , wherein each tubular riser has a plurality of laterally placed openings of equal or different sizes.

9. The grid plate assembly of claim 1 , wherein each tubular riser has a plurality of laterally placed openings spaced along a vertical length of the riser.

10. The grid plate assembly of claim 1 , wherein the tubular riser has a plurality of laterally placed openings spaced equidistant circumferentially about the riser.

11. The grid plate assembly of claim 1 , wherein each tubular riser comprises an inner pipe and an outer pipe defining an annular opening between the inner pipe and the outer pipe as the open bottom end for ingress of hydrogen gas and hydrocarbon feedstock.

12. The grid plate assembly of claim 1 , wherein the plurality of tubular risers each having at least a laterally placed opening with at least two tubular risers having laterally placed openings of different sizes.

Assignees

• Song Steven Xuqi
• Kuehne Donald Leroy
• Kemoun Abdenour
• Reynolds Bruce Edward
• Chevron Usa Inc

Inventors

• Song Steven Xuqi
• Kuehne Donald Leroy
• Kemoun Abdenour
• Reynolds Bruce Edward

Classifications

• B01J2208/025

  Two or more types of catalyst · CPC title

• B01J2208/00176

  outside the reactor · CPC title

• C10G49/12

  suspended in the oil, e.g. slurries · CPC title

• C10G45/02

  to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing · CPC title

• B01J8/005 Primary

  Separating solid material from the gas/liquid stream (separation processes per se B01D) · CPC title