Method for manufacturing microneedle biosensor
US-11945164-B2 · Apr 2, 2024 · US
US9302522B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-9302522-B2 |
| Application number | US-201113324747-A |
| Country | US |
| Kind code | B2 |
| Filing date | Dec 13, 2011 |
| Priority date | Dec 13, 2010 |
| Publication date | Apr 5, 2016 |
| Grant date | Apr 5, 2016 |
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A process for making patterned cigarette wrapper includes the steps of: preparing a printing solution including the steps of: mixing at least water and a starch to form a starch mixture, heating the starch mixture to a temperature of at least about 180° F. preferably for at least about 30 minutes to release amylopectin and amylose, adding propylene glycol to the starch mixture, and mixing the starch mixture and propylene glycol to form a printing solution, wherein the solution is maintained and applied at elevated temperature (120° F. to 150° F.). The process also includes providing a base web of wrapper and applying the printing solution to the wrapper in a predetermined pattern.
Opening claim text (preview).
What is claimed is: 1. A process for making patterned wrapper of a smoking article comprising the steps of: preparing a printing solution including the steps of: mixing at least water and a starch to form an aqueous starch solution; heating the aqueous starch mixture to a temperature of at least about 180° F. for a time sufficient to release at least one of amylopectin and amylose; adding propylene glycol to the aqueous starch mixture; and mixing the starch mixture and propylene glycol to form a printing solution; and providing a base web of wrapper; applying the printing solution to the wrapper in a predetermined pattern; and between said preparing step and said applying step, cooling to and continuously maintaining the printing solution at a temperature ranging from about 120° F. to about 150° F. 2. The process of claim 1 , wherein the mixing step includes incorporating oxidized starch. 3. The process of claim 1 , wherein the printing solution is applied to the wrapper at a temperature ranging from about 120° F. to about 150° F. 4. The process of claim 1 , wherein the viscosity of the printing solution ranges from about 16.5 seconds to about 19.5 seconds as measured by a Zahn #2 cup at 120° F. 5. The process of claim 1 , further including agitating the printing solution during the heating step. 6. The process of claim 1 , wherein the printing solution is applied to the wrapper in transversely extending bands. 7. The process of claim 1 , wherein the printing solution has a pH in the range of about 4 to about 5 after adding propylene glycol. 8. The process of claim 1 , wherein the base web has a transverse direction and wherein the predetermined pattern comprises generally parallel bands extending generally transversely on the base web. 9. The process of claim 1 , wherein the base web has a longitudinal direction and wherein the predetermined pattern includes a longitudinally extending stripe. 10. The process of claim 1 , wherein the base web has a transverse direction and a longitudinal direction and wherein the predetermined pattern includes a plurality of regions extending transversely and spaced longitudinally on the base web. 11. The process of claim 1 , wherein the printing process is selected from the group comprising gravure printing, flexographic printing, offset printing, inkjet printing, spraying, and die printing. 12. The process of claim 11 , wherein the printing process is gravure printing. 13. The process of claim 1 , wherein the printing solution is applied in at least a single pass to the base web. 14. The process of claim 1 , further including adding calcium carbonate to the printing solution. 15. The process of claim 14 , wherein the calcium carbonate is added to the printing solution after the heating and maintaining step and before the printing step. 16. The process of claim 1 , wherein the printing solution has a viscosity ranging from about 40 cP to about 60 cP after the cooling step. 17. The process of claim 1 , wherein during the maintaining step, the temperature is maintained for at least 30 minutes or more. 18. The process of claim 1 , wherein the at least water and oxidized starch are mixed at a temperature of about 75° F. 19. The process of claim 1 , wherein the oxidized starch mixture has a viscosity of about 50 cP to about 80 cP after the heating step. 20. The process of claim 1 , wherein the viscosity of the printing solution is about 16.5 seconds to about 19.5 seconds as measured by Zahn #2 cup at 120° F. at application to a base web. 21. The process of claim 1 , wherein propylene glycol is a stabilizing agent and wherein the propylene glycol is added in an amount of about 7% to about 10% by weight based on the weight of the cooked starch solution. 22. The process of claim 1 , wherein the printing solution when applied has a solids content of about 21%, the viscosity of the printing solution ranges from about 16.5 seconds to about 19.5 seconds as measured by a Zahn #2 cup at 120° F., and the printing solution is applied to a base web in a single pass.
characterised by features other than the chemical nature of the binder · CPC title
the covers having material applied to defined areas, e.g. bands for reducing the ignition propensity · CPC title
based on carbohydrates · CPC title
Patterns of chemical products used for a specific purpose, e.g. pesticides, perfumes, adhesive patterns; use of microencapsulated material; Printing on smoking articles · CPC title
Discontinuous or differential coating, impregnation or bond [e.g., artwork, printing, retouched photograph, etc.] · CPC title
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