Methods of forming composite material films
US-10103378-B2 · Oct 16, 2018 · US
US9283693B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-9283693-B2 |
| Application number | US-201113813323-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jul 27, 2011 |
| Priority date | Jul 30, 2010 |
| Publication date | Mar 15, 2016 |
| Grant date | Mar 15, 2016 |
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A hot press sintering apparatus according to the embodiment includes a chamber; a mold member located in the chamber and including a mold space section to be filled with a raw material; a press member for pressing and processing the raw material in the mold member; and a heating member for heating an interior of the chamber. The mold member includes a first mold part and a second mold part inserted into the first mold part and formed with the mold space section.
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The invention claimed is: 1. A hot press sintering apparatus comprising: a chamber; a mold member located in the chamber and including a mold space section to be filled with a raw material; a press member for pressing and processing the raw material in the mold member; upper and lower moving members to move the press member up and down; and a heating member for heating an interior of the chamber, wherein the mold member includes a first mold part and a second mold part inserted into the first mold part, the second mold part being formed with the mold space section; wherein the press member includes a press section adjacent to the mold space section and an adiabatic section disposed at the press section; wherein the adiabatic section has a thermal conductivity lower than a thermal conductivity of the press section; wherein the press section includes graphite, the graphite having an impurity with a concentration equal to or smaller than 20 parts per million (ppm); wherein the adiabatic section is formed with a composite material including a carbon fiber reinforced carbon composite material, and wherein the adiabatic section is positioned between the press section and the upper and lower moving members, wherein the composite material is woven in a vertical direction, wherein the composite material has a thermal conductivity equal to or smaller than 10 W/Mk, wherein a width of the adiabatic section is smaller than a distance between two outmost lateral sides of the upper moving member or than a distance between two outmost lateral sides of the lower moving member, wherein the adiabatic section includes a first part positioned at one surface of the press section and a second part surrounding a lateral side of the press section, wherein a thickness of the first part and a thickness of the second part are both in a range of 5 mm to 200 mm, and wherein the adiabatic section has a cap shape. 2. The hot press sintering apparatus of claim 1 , wherein the second mold part has purity higher than purity of the first mold part. 3. The hot press sintering apparatus of claim 1 , wherein a lower portion of the second mold part is narrower than an upper portion of the second mold part. 4. The hot press sintering apparatus of claim 3 , wherein the lower portion of the second mold part is larger than the mold space section. 5. The hot press sintering apparatus of claim 3 , wherein an area of the second mold part is gradually reduced from the upper portion to the lower portion of the second mold part. 6. The hot press sintering apparatus of claim 5 , wherein, when a value obtained by subtracting a radius of the mold space section from a radius of the second mold part measured from the upper portion of the second mold part is “a” and a value obtained by subtracting a radius of the mold space section from a radius of the second mold part measured from the lower portion of the second mold part is “b”, a ratio of “b” to “a” is in a range of 0.1 to 0.9. 7. The hot press sintering apparatus of claim 1 , further comprising a sheet attached to an inner wall defining the mold space section, wherein the sheet has purity higher that purity of the second mold part. 8. The hot press sintering apparatus of claim 1 , wherein the first mold part includes graphite having purity not less than 90% but less than 99.9%, and the second mold part includes graphite having purity in a range of 99.99% to 99.9999%. 9. The hot press sintering apparatus of claim 8 , further comprising a sheet attached to an inner wall defining the mold space section, wherein the sheet includes graphite having purity in a range of 99.99% to 99.9999%. 10. The hot press sintering apparatus of claim 1 , wherein the first mold part is formed with an opening having a shape corresponding to an outer appearance of the second mold part. 11. A press member of a hot press sintering apparatus, the press member comprising: a press section for applying pressure; and an adiabatic section positioned at one end of the press section; wherein the press section includes graphite, the graphite having an impurity with a concentration equal to or smaller than 20 parts per million (ppm); wherein the adiabatic section is formed with a composite material including a carbon fiber reinforced carbon composite material; wherein the adiabatic section has a thermal conductivity lower than a thermal conductivity of the press section; wherein the adiabatic section includes a first part positioned at one surface of the press section and a second part surrounding a lateral side of the press section; and wherein a thickness of the first part and a thickness of the second part are both in a range of 5 mm to 200 mm, wherein the composite material is woven in a vertical direction, wherein the composite material has a thermal conductivity equal to or smaller than 10 W/Mk, wherein the adiabatic section includes a first part positioned at one surface of the press section and a second part surrounding a lateral side of the press section, and wherein a thickness of the first part and a thickness of the second part are both in a range of 5 mm to 200 mm, and wherein the adiabatic section has a cap shape.
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