Polycrystalline diamond compacts having parting compound and methods of making the same
US-10213835-B2 · Feb 26, 2019 · US
US9249059B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-9249059-B2 |
| Application number | US-201213440868-A |
| Country | US |
| Kind code | B2 |
| Filing date | Apr 5, 2012 |
| Priority date | Apr 5, 2012 |
| Publication date | Feb 2, 2016 |
| Grant date | Feb 2, 2016 |
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A post manufacture method and apparatus for reducing residual stresses present within a component. The component includes a substrate, a polycrystalline structure coupled thereto, and residual stresses present therein. The method includes obtaining a component from a component category, determining a critical temperature and a critical time period for the component category at which the component becomes structurally impaired, determining a heat treatment temperature and a heat treatment time period based upon the critical temperature and the critical time period, and heating one or more remaining components from the component category to the heat treatment temperature for the heat treatment time period. The apparatus includes a heater defining a heating chamber and a molten bath positioned within the heating chamber. The components are placed within the pre-heated molten bath and isolated from oxygen during heating to the heat treatment temperature for the heat treatment time period.
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What is claimed is: 1. A post manufacture method for reducing residual stresses present within a component, the method comprising: obtaining one or more components from a component category, each component comprising a substrate, a polycrystalline structure coupled to the substrate, and a plurality of residual stresses formed therein; determining a critical temperature and a critical time period for the component category by determining the structural integrity of the one or more components, the critical temperature and the critical time period being the temperature and the time period corresponding to the best structural integrity results; determining a heat treatment temperature and a heat treatment time period for the component category based upon the critical temperature and the critical time period; and performing a high temperature heat treatment process on one or more remaining components where the one or more remaining components are heated to about the heat treatment temperature for about the heat treatment time period, wherein the one or more components and the one or more remaining components are representative of the component category. 2. The method of claim 1 , wherein the heat treatment temperature is a percentage of the critical temperature. 3. The method of claim 2 wherein the heat treatment temperature ranges from about eighty-five percent to about ninety-eight percent of the critical temperature and is greater than 750° C. and less than 900° C. 4. The method of claim 2 wherein the heat treatment temperature ranges from about eighty-five percent to about ninety-eight percent of the critical temperature and is greater than 850° C. 5. The method of claim 1 , wherein the heat treatment temperature ranges from about 10° C. to about 100° C. below the critical temperature and is greater than 750° C. 6. The method of claim 1 , wherein the heat treatment temperature ranges from about 10° C. to about 100° C. below the critical temperature and is greater than 850° C. 7. The method of claim 1 , wherein the heat treatment time period is a percentage of the critical time period. 8. The method of claim 7 , wherein the heat treatment time period ranges from about thirty percent to about ninety-eight percent of the critical time period and is less than thirty minutes. 9. The method of claim 7 , wherein the heat treatment time period ranges from about thirty percent to about ninety-eight percent of the critical time period and is less than about ten minutes. 10. The method of claim 1 , wherein at least one of the heat treatment temperature and the heat treatment time period is less than the critical temperature and the critical time period, respectively, while the other is equal to or greater than the critical temperature and the critical time period, respectively, the heat treatment temperature and the heat treatment time period being tested when determining the critical temperature and the critical time period for the component category. 11. The method of claim 1 , wherein the determining a critical temperature and a critical time period for the component category using the one or more components, comprises: heating and cooling a first component through a first temperature and time cycle, the first temperature and time cycle comprising a temperature component and a time period component; determining the structural integrity of the first component; heating and cooling a different component through a different temperature and time cycle, the different temperature and time cycle comprises at least one of the temperature component and the time period component being different than the temperature component and the time period component of the first temperature and time cycle; determining the structural integrity of the different component; and continue heating and cooling a different component and determining the structural integrity of the different component until determining a lowest different temperature and time cycle that causes failure of the structural integrity of the different component, the lowest different temperature and time cycle providing the critical temperature and the critical time period. 12. The method of claim 1 , wherein performing a high temperature heat treatment process on the one or more remaining components, comprises: heating the one or more remaining components to about the heat treatment temperature; maintaining the one or more remaining components at about the heat treatment temperature for about the heat treatment time period; and cooling the one or more remaining components. 13. The method of claim 12 , wherein the heating one or more remaining components to about the heat treatment temperature, comprises: heating the one or more remaining components to an intermediate temperature; and heating the one or more remaining components from the intermediate temperature to the heat treatment temperature. 14. The method of claim 13 , wherein heating the one or more remaining components from the intermediate temperature to the heat treatment temperature is rapid. 15. The method of claim 12 , wherein heating the one or more remaining components to the heat treatment temperature is rapid. 16. The method of claim 12 , wherein the heating one or more remaining components to about the heat treatment temperature, comprises dropping the one or more remaining components into a molten bath comprising a molten material, the temperature of the molten material being at the heat treatment temperature, the one or more remaining components being surrounded by the molten material. 17. The method of claim 16 , wherein the molten material comprises at least one of a molten metal, sodium chloride, and borosilicate. 18. The method of claim 12 , wherein the heating one or more remaining components to about the heat treatment temperature is performed using an induction unit. 19. The method of claim 1 , further comprising removing at least a portion of a catalyst material from the polycrystalline structure of the one or more components after performing a high temperature heat treatment process on the one or more remaining components. 20. The method of claim 1 , further comprising removing at least a portion of a catalyst material from the polycrystalline structure of the one or more components before performing a high temperature heat treatment process on the one or more remaining components.
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