Fractionating and refining device

Patent metadata

Field	Value
Publication number	US-8968563-B2
Application number	US-200913262524-A
Country	US
Kind code	B2
Filing date	Mar 31, 2009
Priority date	Mar 31, 2009
Publication date	Mar 3, 2015
Grant date	Mar 3, 2015

Abstract

A fractionating and refining device includes a solution sending flow path for supplying a solution, including a fractionated target component, a gas supply flow path, a collecting vessel, a warming mechanism for warming the collecting vessel, and a probe formed by integrating tip end portions of the solution sending flow path and the gas supply flow path with each other. A lid of the vessel includes a solution inlet to which the tip end portion of the solution sending flow path is connected, gas inlets to which the tip end portion of the gas supply flow path is connected, and gas discharge ports connecting an inside and an outside of a vessel main body of the vessel.

First claim

The invention claimed is:

1. A fractionating and refining device comprising:
a solution sending device for supplying a solution including a fractionated target component from a tip end of a solution sending flow path;
a gas supply flow path for supplying gas from a tip end thereof;
a collecting vessel for collecting solid material of the fractionated target component, said collecting vessel comprising a lid and a vessel main body having a bottom,
the lid closing an opening portion of the collecting vessel main body and being able to be opened and closed, and
the lid including a solution inlet to which the tip end portion of the solution sending flow path is connected and through which the solution is supplied into the vessel main body, a gas inlet to which the tip end portion of the gas supply flow path is connected and through which the gas from the gas supply flow path is supplied into the vessel main body, and a gas discharge port connecting an inside and an outside of the vessel main body;
a warming mechanism for warming the collecting vessel to such a temperature as to facilitate evaporation of a solvent in the solution in the collecting vessel; and
a probe formed by integrating the tip end portion of the solution sending flow path and the tip end portion of the gas supply flow path with each other, wherein the solution inlet and the gas inlet in the lid are disposed in positions respectively corresponding to the tip end portion of the solution sending flow path and the tip end portion of the gas supply flow path integrated in the probe so that the tip end portion of the solution sending flow path and the tip end portion of the gas supply flow path are respectively connected to the solution inlet and the gas inlet in the lid when the probe is mounted to the lid,
wherein the lid has a recessed portion, in which the solution inlet and the gas inlet are open, for mounting the probe therein to detachably connect to detachably place an end surface of the tip end portion of the solution sending flow path in contact with an end surface of the solution inlet and to detachably place an end surface of the gas supply flow path in contact with an end surface of the gas inlet.

2. The fractionating and refining device according to claim 1 , wherein
the tip end portion of the probe is made up of a concentrically arranged double tube and one tube of the double tube is connected to the solution sending flow path and the other is connected to the gas supply flow path and
the solution inlet and the gas inlet in the lid are formed as one central inlet disposed at a center of the lid and corresponding to a central outlet of the double tube and a plurality of outer inlets disposed around the central inlet and on a circumference corresponding to an outer outlet of the double tube.

3. The fractionating and refining device according to claim 2 , wherein
the inner tube of the double tube is connected to the solution sending flow path and the outer tube of the double tube is connected to the gas supply flow path.

4. The fractionating and refining device according to claim 2 , wherein
a plurality of gas discharge ports are provided in the lid and disposed at equal intervals on a circumference outside the circumference on which the outer inlets are disposed.

5. The fractionating and refining device according to claim 1 , comprising means for gas heating on the gas supply flow path.

6. The fractionating and refining device according to claim 1 , comprising means for solution heating on the solution sending flow path.

Assignees

• Iwata Yosuke
• Yamazaki Tomoyuki
• Stasica Przemyslaw
• Boughtflower Bob
• Shimadzu Corp

Inventors

• Iwata Yosuke
• Yamazaki Tomoyuki
• Stasica Przemyslaw
• Boughtflower Bob

Classifications

• G01N30/80 Primary

  Fraction collectors · CPC title

• B01D15/24

  relating to the treatment of the fractions to be distributed · CPC title

• G01N30/84

  Preparation of the fraction to be distributed · CPC title

• G01N2030/8447

  Nebulising, aerosol formation or ionisation · CPC title

• G01N2030/8494

  Desolvation chambers · CPC title