Methods for constructing parts with improved properties using metallic glass alloys
US-2015315678-A1 · Nov 5, 2015 · US
US8962067B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-8962067-B2 |
| Application number | US-201313749307-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jan 24, 2013 |
| Priority date | Jan 24, 2013 |
| Publication date | Feb 24, 2015 |
| Grant date | Feb 24, 2015 |
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Processes for real time process control of the Polymer Dispersion Index (PDI) during polymerization processes. By tuning this chain length distribution in real time, a resulting polymer can have predetermined physical properties such as thickness, physical yield strength, decomposition time, thermal stability, etc. Techniques herein can dynamically control chain length distribution through use of a mass density measurement device located within a processing chamber and providing real time feedback of polymer growth. Chamber parameters can be controlled or modified before and during polymerization based on mass density feedback. Such chamber parameters can include pressure, temperature, chemistry, and process gas flow rates and flow periods.
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The invention claimed is: 1. A method of forming a polymer film, the method comprising: disposing a substrate on a substrate holder in a process chamber of a vapor deposition system; positioning a mass density measurement device in the process chamber adjacent to the substrate holder, wherein positioning the mass density measurement device in the process chamber includes positioning a quartz crystal microbalance (QCM) sensor in the process chamber adjacent to the substrate holde…
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