Method of preparing hollow metal or metal oxide nano- or microspheres
US-2016311132-A1 · Oct 27, 2016 · US
US8940179B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-8940179-B2 |
| Application number | US-201213679288-A |
| Country | US |
| Kind code | B2 |
| Filing date | Nov 16, 2012 |
| Priority date | Nov 5, 2012 |
| Publication date | Jan 27, 2015 |
| Grant date | Jan 27, 2015 |
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The present invention relates to a method for preparing magnetite nanoparticles from low-grade iron ore using solvent extraction and magnetite nanoparticles prepared by the same. According to the method for magnetite nanoparticles from low-grade iron ore of the present invention, it is possible to prepare high-purity magnetite nanoparticles having a purity of 99% or higher by solvent extraction using low-grade iron ore as a starting material, and thus it is possible to reduce the processing cost and the amount of energy used, thus supplying a high-efficiency magnetite nanoparticle adsorbent, which can be industrially applied to wastewater treatment or desalination plant, in large quantities at low cost. In particular, it is possible to effectively treat livestock wastewater, heavy metal wastewater, oil discharged into rivers, etc. at low cost, thus significantly contributing to the prevention of environmental pollution. Moreover, the magnetite nanoparticles prepared by the present invention has a purity of 99.5% and thus can be used as raw materials for high-tech products such as nanoparticle catalysts, magnetic fluids, MRI contrast agents, etc.
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What is claimed is: 1. A method for preparing magnetite nanoparticles from low-grade iron ore, comprising: (1) adding iron ore powder to an acidic solution and stirring the mixture to obtain iron ore leachate; (2) centrifuging the iron ore leachate and separating and discharging residual powder to obtain a supernatant; (3) adding an oxidant to the supernatant to oxidize all Fe 2+ ions to Fe 3+ ions, adding a solvent extractant thereto to form an iron-solvent extractant compl…
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