Spray dryer

Patent metadata

Field	Value
Publication number	US-2025180287-A1
Application number	US-202218845590-A
Country	US
Kind code	A1
Filing date	Mar 11, 2022
Priority date	Mar 11, 2022
Publication date	Jun 5, 2025
Grant date	—

Abstract

A spray dryer with which a fluid that has been subjected to a fluid processing in a spray device can be directly sprayed from the spray device into a drying chamber so that the fluid can be dried, without the need for a dispersion machine for adjusting the dispersion state of a dispersion solution to be sprayed into the drying chamber. The spray dryer includes a spray device. The spray device includes processing surfaces disposed opposing each other, and a rotation mechanism that rotates at least one of the processing surfaces relative to the other. The processing surfaces define a circular flow path through which is passed a fluid to be processed containing a first fluid and a second fluid. The circular flow path includes introduction ports. A first introduction port introduces, at an opening which connects to the circular flow path, the first fluid from the inside of the circular flow path. A second introduction port opens in the middle of the circular flow path, and combines the second fluid with the first fluid which has been constrained into a thin-film fluid by the processing surfaces. The fluid to be processed is subjected to fluid processing between the processing surfaces, and the fluid-treated fluid is sprayed to the outside from between the processing surfaces.

First claim

1 . A spray dryer comprising a spray device, wherein the spray device comprises:
at least two processing surfaces disposed in a position opposite to each other; and a rotation mechanism for rotating at least one of the at least two processing surfaces relative to the other, wherein the at least two processing surfaces define a circular flow path through which a fluid to be processed passes, wherein the circular flow path includes at least two introduction ports, wherein the fluid to be processed includes a first fluid and a second fluid, wherein the device is configured such that one of the introduction ports is an opening leading to the circular flow path, and the first fluid is introduced from inside the circular flow path, and wherein the other one of introduction ports is opened in the middle of the circular flow path, the second fluid is merged with the first fluid which has become a thin-film fluid forced by the at least two processing surfaces to perform the fluid processing to the fluid to be processed between the at least two processing surfaces, and the fluid subjected to the fluid processing is sprayed outside from between the at least two processing surfaces.

2 . A spray dryer comprising a spray device, wherein the spray device comprises:
at least two processing surfaces disposed in a position opposite to each other; and a rotation mechanism for rotating at least one of the at least two processing surfaces relative to the other, wherein the at least two processing surfaces define a circular flow path through which a fluid to be processed passes, wherein the fluid to be processed comprises two or more kinds of raw material fluids, wherein the device is configured such that the two or more kinds of raw material fluids are introduced into the circular flow path, respectively, and wherein the two or more kinds of raw material fluids pass through the circular flow path from the inside to the outside in the radial direction in a state of thin-film fluids, whereby the fluid processing to the fluid to be processed is subjected between the at least two processing surfaces, and the fluid subjected to the fluid processing is sprayed outside from between the at least two processing surfaces.

3 . The spray dryer according to claim 1 ,
wherein a spray drying chamber for housing the spray device is provided, and wherein the difference (p 1 −p) between a pressure p 1 of the fluid subjected to the fluid processing at the outlet portion between the at least two processing surfaces and a pressure p in the spray drying chamber is 20 kPa or more and 200 kPa or less.

4 . The spray dryer according to claim 1 ,
wherein the thin-film fluid formed by merging of the fluid to be processed in the circular flow path contains particles, and wherein the spray device is configured to give a rotation imparting force to the particles.

5 . The spray dryer according to claim 1 , wherein the fluid processing is a chemical reaction.

6 . The spray dryer according to claim 1 , wherein the distance between the at least two processing surfaces is 1 mm or less.

7 . The spray dryer according to claim 1 , wherein the at least two processing surfaces rotate relatively at a rotation speed of 6,000 rpm or less.

8 . The spray dryer according to claim 1 , wherein the spray dryer comprises a raw material supply device that supplies the fluid to be processed as a raw material to the spray device, a spray drying chamber that houses the spray device, and a gas supply device that supplies gas for drying the fluid subjected to the fluid processing sprayed from the spray device to the spray drying chamber.

9 . The spray dryer according to claim 3 , wherein a microwave irradiation mechanism is installed in the spray drying chamber to irradiate microwaves to the fluid subjected to the fluid processing sprayed from the spray device.

10 . The spray dryer according to claim 2 ,
wherein a spray drying chamber for housing the spray device is provided, and wherein the difference (p 1 −p) between a pressure p 1 of the fluid subjected to the fluid processing at the outlet portion between the at least two processing surfaces and a pressure p in the spray drying chamber is 20 kPa or more and 200 kPa or less.

11 . The spray dryer according to claim 2 ,
wherein the thin-film fluid formed by merging of the fluid to be processed in the circular flow path contains particles, and wherein the spray device is configured to give a rotation imparting force to the particles.

12 . The spray dryer according to claim 2 , wherein the fluid processing is a chemical reaction.

13 . The spray dryer according to claim 2 , wherein the distance between the at least two processing surfaces is 1 mm or less.

14 . The spray dryer according to claim 2 , wherein the at least two processing surfaces rotate relatively at a rotation speed of 6,000 rpm or less.

15 . The spray dryer according to claim 2 , wherein the spray dryer comprises a raw material supply device that supplies the fluid to be processed as a raw material to the spray device, a spray drying chamber that houses the spray device, and a gas supply device that supplies gas for drying the fluid subjected to the fluid processing sprayed from the spray device to the spray drying chamber.

16 . The spray dryer according to claim 3 ,
wherein the thin-film fluid formed by merging of the fluid to be processed in the circular flow path contains particles, and wherein the spray device is configured to give a rotation imparting force to the particles.

17 . The spray dryer according to claim 3 , wherein the fluid processing is a chemical reaction.

18 . The spray dryer according to claim 4 , wherein the fluid processing is a chemical reaction.

19 . The spray dryer according to claim 3 , wherein the distance between the at least two processing surfaces is 1 mm or less.

20 . The spray dryer according to claim 4 , wherein the distance between the at least two processing surfaces is 1 mm or less.

Assignees

• M Technique Co Ltd

Inventors

• Enomura Masakazu
• Araki Kaeko

Classifications

• B01D1/18

  to obtain dry solids (B01D1/24 takes precedence) · CPC title

• B22F2304/058

  Particle size above 300 nm up to 1 micrometer · CPC title

• B22F2304/056

  Particle size above 100 nm up to 300 nm · CPC title

• B22F2203/11

  temperature, temperature profile · CPC title

• B22F2009/0892

  casting nozzle; controlling metal stream in or after the casting nozzle · CPC title