Fluid-segmentation device, flow mixing and segmentation device, continuous-flow reactor system, and method for producing nanoparticles

Patent metadata

Field	Value
Publication number	US-2018161748-A1
Application number	US-201615577751-A
Country	US
Kind code	A1
Filing date	May 27, 2016
Priority date	May 29, 2015
Publication date	Jun 14, 2018
Grant date	—

Abstract

The fluid-segmentation device according to an embodiment of the present invention includes: a first conduit in which a first fluid flows, and a second conduit in which a second fluid immiscible with the first fluid flows. The second conduit of the fluid-segmentation device includes an intersection region, to which the first conduit is connected and into which the first fluid is introduced, and a first region downstream of the intersection region. The cross-sectional area of the intersection region of the second conduit in a plane perpendicular to the flow direction of the second fluid is less than the cross-sectional area of the first region of the second conduit in a plane perpendicular to the flow direction of the second fluid.

First claim

1 - 13 . (canceled)

14 . A method for producing nanoparticles
by using a second fluid containing precursors of nanoparticles, a first fluid which is immiscible and non-reacting with the second fluid, a first conduit in which the first fluid flows, and a second conduit in which the second fluid flows by forming a segmented flow of the second fluid, which is separated by intervening segments of the first fluid, and by energizing and/or activating the segmented flow, wherein the second conduit comprises at least a region of intersection in which the first conduit and the second conduit intersect, and a widening region located downstream of the region of intersection in a flow direction of the second fluid and configured such that a cross-sectional area of the second conduit in a plane perpendicular to the flow direction widens, by introducing the intervening segments of the first fluid from the first conduit to the second conduit to form the segmented flow and by passing the segmented flow through a widening region of the conduit, thereby making the intervening segments of the segmented flow in the flow direction downstream of the widening region shorter than the intervening segments of the segmented flow in the flow direction upstream of the widening region.

15 . The method for producing nanoparticles according to claim 14 , wherein the first fluid is a gas and the second fluid is a liquid.

16 . The method for producing nanoparticles according to claim 14 , wherein the second conduit has a first region downstream of the widening region in which the segmented flow is stabilized.

17 . The method for producing nanoparticles according to claim 15 , wherein the second conduit has a first region downstream of the widening region in which the segmented flow is stabilized.

18 . The method for producing nanoparticles according to claim 16 , wherein energizing and/or activating the segmented flow is performed downstream of the first region

19 . The method for producing nanoparticles according to claim 17 , wherein energizing and/or activating the segmented flow is performed downstream of the first region

20 . The method for producing nanoparticles according to claim 18 , wherein the region of intersection and a region in which energizing and/or activating are thermally insulated.

21 . The method for producing nanoparticles according to claim 19 , wherein the region of intersection and a region in which energizing and/or activating are thermally insulated.

22 . The method for producing nanoparticles according to claim 14 , wherein the second conduit further includes a constant-width portion, having a cross-sectional area equal to the intersection region, between the intersection region and the widening region.

23 . The method for producing nanoparticles according to claim 15 , wherein the second conduit further includes a constant-width portion, having a cross-sectional area equal to the intersection region, between the intersection region and the widening region.

24 . The method for producing nanoparticles according to claim 14 , wherein an amount of the first fluid introduced into the intersection region is controlled on the basis of a flow rate of the second fluid.

25 . The method for producing nanoparticles according to claim 15 , wherein an amount of the first fluid introduced into the intersection region is controlled on the basis of a flow rate of the second fluid.

26 . The method for producing nanoparticles according to claim 14 , wherein a plurality of fluids which are immiscible and non-reacting with the first fluid flow in the second conduit.

27 . The method for producing nanoparticles according to claim 15 , wherein a plurality of fluids which are immiscible and non-reacting with the first fluid flow in the second conduit.

28 . The method for producing nanoparticles according to claim 26 , wherein the plurality of fluids are mixed upstream of the region of intersection and introduced to the second conduit.

29 . The method for producing nanoparticles according to claim 27 , wherein the plurality of fluids are mixed upstream of the region of intersection and introduced to the second conduit.

30 . The method for producing nanoparticles according to claim 28 , wherein the plurality of fluids are mixed and homogenized and then are introduced to the second conduit.

31 . The method for producing nanoparticles according to claim 29 , wherein the plurality of fluids are mixed and homogenized and then are introduced to the second conduit.

32 . The method for producing nanoparticles according to claim 14 , wherein species and/or amount of the fluid flowing the second conduit is measured.

33 . The method for producing nanoparticles according to claim 15 , wherein species and/or amount of the fluid flowing the second conduit is measured.

Assignees

• Shoei Chemical Ind Co

Inventors

• Peterson Daniel
• Haben Patrick Michael
• Barsic David
• Dreilinger Rachel

Classifications

• B01J2219/00033

  Continuous processes · CPC title

• B01J19/24

  Stationary reactors without moving elements inside (B01J19/08, B01J19/26 take precedence; with stationary particles B01J8/02) · CPC title

• B01J19/06 Primary

  Solidifying liquids (making microcapsules B01J13/02) · CPC title

• B01J19/2415 Primary

  Tubular reactors · CPC title

• B01F25/431971

  Mounted on the wall · CPC title