Solid electrolyte, and method for producing same
US-12404173-B2 · Sep 2, 2025 · US
US2018148333A1 · US · A1
| Field | Value |
|---|---|
| Publication number | US-2018148333-A1 |
| Application number | US-201715822723-A |
| Country | US |
| Kind code | A1 |
| Filing date | Nov 27, 2017 |
| Priority date | Nov 28, 2016 |
| Publication date | May 31, 2018 |
| Grant date | — |
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A method for producing complexed particles, wherein the method comprises: obtaining a good solvent solution, by dissolving Li 2 S, and LiX (X is at least one selected from a group consisting of F, Cl, Br, and I) in a good solvent, and precipitating particles by contacting the good solvent solution with a poor solvent having a temperature at least 165° C. higher than the boiling point of the good solvent, to evaporate off the good solvent; and, wherein the method satisfies at least one of the following: (i) the good solvent solution being obtained by further dissolving H 2 S in the good solvent, and (ii) H 2 S being dissolved in the poor solvent.
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1 . A method for producing complexed particles, wherein the method comprises: obtaining a good solvent solution, by dissolving Li 2 S, and LiX (X is at least one selected from a group consisting of F, Cl, Br, and I) in a good solvent, and precipitating particles by contacting the good solvent solution with a poor solvent having a temperature at least 165° C. higher than the boiling point of the good solvent, to evaporate off the good solvent; and, wherein the method satisfies at least one of the following: (i) the good solvent solution being obtained by further dissolving H 2 S in the good solvent, and (ii) H 2 S being dissolved in the poor solvent. 2 . The method according to claim 1 , wherein the LiX is LiI and LiBr. 3 . The method according to claim 1 , wherein at least the (i) is satisfied. 4 . The method according to claim 3 , wherein in the (i), the good solvent solution is obtained by further dissolving H 2 S in the good solvent by blowing H 2 S into the good solvent. 5 . The method according to claim 1 , wherein at least the (ii) is satisfied. 6 . The method according to claim 5 , wherein in the (ii), the H 2 S is dissolved in the poor solvent by blowing H 2 S into the poor solvent. 7 . The method according to claim 1 , wherein the ratio of the LiX (X is at least one selected from a group consisting of F, Cl, Br, and I) is 0.30 mol to 0.60 mol based on 1 mol of Li 2 S. 8 . A method for producing complexed particles, wherein the method comprises: obtaining a good solvent solution, by dissolving LiHS, and LiX (X is at least one selected from a group consisting of F, Cl, Br, and I) in a good solvent, and precipitating particles by contacting the good solvent solution with a poor solvent having a temperature at least 165° C. higher than the boiling point of the good solvent to evaporate off the good solvent. 9 . The method according to claim 8 , wherein the ratio of the LiX (X is at least one selected from a group consisting of F, Cl, Br, and I) is 0.30 mol to 0.60 mol based on 1 mol of LiS. 10 . The method according to claim 8 , wherein the LiX is LiI and LiBr. 11 . The method according to claim 1 , wherein the contacting the good solvent solution with the poor solvent is by dropping, spraying, or injecting the good solvent solution into the poor solvent. 12 . The method according to claim 11 , wherein the contacting the good solvent solution with the poor solvent is by dropping the good solvent solution into the poor solvent.
diffraction · CPC title
Making shaped products, e.g. granules · CPC title
Sulfur compounds · CPC title
Treatment of the solvent · CPC title
Halides · CPC title
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