Systems and Methods for Analyzing Contaminants in Flowing Bulk Powder Compositions

Patent metadata

Field	Value
Publication number	US-2017010221-A1
Application number	US-201415113253-A
Country	US
Kind code	A1
Filing date	Apr 22, 2014
Priority date	Apr 22, 2014
Publication date	Jan 12, 2017
Grant date	—

Abstract

Methods including optically interacting electromagnetic radiation with a flowing powder composition and a first integrated computation element (“ICE”), the first ICE being configured to detect a contaminant in the powder composition; receiving the electromagnetic radiation with a detector; and generating an output signal corresponding to a characteristic of the contaminant in the powder composition.

First claim

The invention claimed is:

1 . A method comprising:
optically interacting electromagnetic radiation with a flowing powder composition and a first integrated computation element (“ICE”), the first ICE being configured to detect a contaminant in the powder composition; receiving the electromagnetic radiation with a detector; and generating an output signal corresponding to a characteristic of the contaminant in the powder composition.

2 . The method of claim 1 , wherein the electromagnetic radiation is at least one selected from the group consisting of infrared radiation, near-infrared radiation, visible light, ultraviolet light, X-ray radiation, and gamma ray radiation.

3 . The method of claim 1 , wherein the electromagnetic radiation is provided by at least one of a light bulb, a light emitting device, a laser, a blackbody, a photonic crystal, an X-Ray source, and a gamma ray source.

4 . The method of claim 1 , wherein the powder composition is a cement composition, a weighting agent composition, or a proppant material composition.

5 . The method of claim 1 , wherein the contaminant is selected from the group consisting of a free aqueous liquid, a bound aqueous liquid, a free organic liquid, a bound organic liquid, a free carbonic acid, a bound carbonic acid, a gaseous contaminant, a dry contaminant, and any combination thereof.

6 . The method of claim 1 , wherein the flowing powder composition is flowing during pneumatic conveyance, gravity conveyance, or mechanical mixing.

7 . The method of claim 1 , further comprising at least one of modifying the powder composition based on the characteristic of the contaminant, and modifying external conditions relative to the powder composition based on the characteristic of the contaminant.

8 . A method comprising:
optically interacting electromagnetic radiation with a flowing powder composition and an integrated computational element (“ICE”), the ICE being configured to detect a contaminant in the powder composition; receiving the electromagnetic radiation with a detector; generating an output signal corresponding to a concentration of the contaminant in the powder composition; and determining if the concentration of the contaminant is within an acceptable limit range in the powder composition.

9 . The method of claim 8 , wherein the electromagnetic radiation is at least one selected from the group consisting of infrared radiation, near-infrared radiation, visible light, ultraviolet light, X-ray radiation, and gamma ray radiation.

10 . The method of claim 8 , wherein the electromagnetic radiation is provided by at least one of a light bulb, a light emitting device, a laser, a blackbody, a photonic crystal, an X-Ray source, and a gamma ray source.

11 . The method of claim 8 , wherein the powder composition is a cement composition, a weighting agent composition, or a proppant material composition.

12 . The method of claim 8 , wherein the contaminant is selected from the group consisting of a free aqueous liquid, a bound aqueous liquid, a free organic liquid, a bound organic liquid, a free carbonic acid, a bound carbonic acid, a gaseous contaminant, a dry contaminant, and any combination thereof.

13 . The method of claim 8 , wherein the flowing powder composition is flowing during pneumatic conveyance, gravity conveyance, or mechanical mixing.

14 . The method of claim 8 , further comprising at least one of modifying the powder composition based on the characteristic of the contaminant, and modifying external conditions relative to the powder composition based on the characteristic of the contaminant.

15 . A method comprising:
optically interacting electromagnetic radiation with a flowing powder composition and a first integrated computational element (“ICE”), the first ICE configured to detect a first contaminant in the powder composition; optically interacting electromagnetic radiation with the flowing powder composition and at least a second ICE, the second ICE configured to detect a second contaminant in the powder composition; receiving the electromagnetic radiation with at least one detector; and generating a first output signal corresponding to a characteristic of the first contaminant in the powder composition and a second output signal corresponding to a characteristic of the second contaminant in the powder composition, or a combined output signal corresponding to a combined characteristic of the first and second contaminants in the powder composition.

16 . The method of claim 15 , wherein the electromagnetic radiation is at least one selected from the group consisting of infrared radiation, near-infrared radiation, visible light, ultraviolet light, X-ray radiation, and gamma ray radiation.

17 . The method of claim 15 , wherein the electromagnetic radiation is provided by at least one of a light bulb, a light emitting device, a laser, a blackbody, a photonic crystal, an X-Ray source, and a gamma ray source.

18 . The method of claim 15 , wherein the powder composition is a cement composition, a weighting agent composition, or a proppant material composition.

19 . The method of claim 15 , wherein the contaminant is selected from the group consisting of a free aqueous liquid, a bound aqueous liquid, a free organic liquid, a bound organic liquid, a free carbonic acid, a bound carbonic acid, a gaseous contaminant, a dry contaminant, and any combination thereof.

20 . The method of claim 15 , wherein the flowing powder composition is flowing during pneumatic conveyance, gravity conveyance, or mechanical mixing.

21 . The method of claim 15 , further comprising at least one of modifying the powder composition based on the characteristic of the first contaminant, the characteristic of the second contaminant, or the combined characteristic of the first and second contaminants in the powder composition, and modifying external conditions relative to the powder composition based thereon.

22 . The method of claim 15 , wherein the characteristic of the first contaminant is a concentration of the first contaminant in the powder composition and wherein the characteristic of the second contaminant is a concentration of the second contaminant in the powder composition, or where the combined characteristic of the first and second contaminants is a combined concentration of the first and second contaminants in the powder composition.

23 . The method of claim 22 , further comprising:
determining if the concentration of the first contaminant in the powder composition is within a first acceptable limit range and/or if the concentration of the second contaminant in the powder composition is within a second acceptable limit range.

24 . The method of claim 22 , further comprising:
determining if the combined concentration of the first and second contaminants in the powder composition is within a combined acceptable limit range.

Assignees

• Halliburton Energy Services Inc

Inventors

• Heaton John Gilbert
• Freese Robert Paul

Classifications

• G01N21/85 Primary

  Investigating moving fluids or granular solids · CPC title

• G01N21/94 Primary

  Investigating contamination, e.g. dust (G01N21/85 takes precedence) · CPC title

• G01N2021/8592

  Grain or other flowing solid samples · CPC title

• G01N23/02

  by transmitting the radiation through the material · CPC title

• G01N23/20

  by using diffraction of the radiation by the materials, e.g. for investigating crystal structure; by using scattering of the radiation by the materials, e.g. for investigating non-crystalline materials; by using reflection of the radiation by the materials · CPC title