Transparent frozen soil and preparation method and application thereof

Patent metadata

Field	Value
Publication number	US-2016290898-A1
Application number	US-201414763531-A
Country	US
Kind code	A1
Filing date	May 27, 2014
Priority date	Apr 30, 2014
Publication date	Oct 6, 2016
Grant date	—

Abstract

The present invention discloses a transparent frozen soil, which is prepared from a fluorine-containing polymer, cube ice and a colorless pore fluid by steps of preparing materials, blending, vacuuming, consolidating, and freezing. The fluorine-containing polymer is Teflon AF 1600 produced by American DuPont Company, with the refractive index of 1.31, the particle diameter ≦0.074 mm, and the density of 2.1-2.3 g/cm 3 . The present invention also provides the application of above transparent frozen soil in the frozen soil directional blasting model test and the frozen soil road embankment model thaw-slumping landslide test. The transparent frozen soil prepared by the present invention can well simulate the properties of natural transparent frozen clay, is effectively used in model tests in the geotechnical engineering, with accurate measurement results, and can realize the visualization of the internal deformation of a soil body, and it is low in the expense, and simple in the operation.

First claim

1 . A transparent frozen soil, characterized in that it is prepared from a fluorine-containing polymer, cube ice and a colorless pore fluid by steps of preparing materials, blending, vacuuming, consolidating, and freezing, and the dosages of said fluorine-containing polymer, cube ice and colorless pore fluid are calculated by the test conditions and the sample sizes; said colorless pore fluid is water, said fluorine-containing polymer is particles with the particle diameter ≦0.074 mm, and its particles have irregular shape, and are Teflon AF 1600 produced by American DuPont Company, with the refractive index of 1.31, and the density of 2.1-2.3 g/cm 3 ; the particle diameter of said cube ice is ≦0.074 mm; the physical properties of said transparent frozen soil are: density of 1.63-2.1 g/cm 3 , unit weight of 16-21 kN/m 3 , and over-consolidation ratio OCR value of 0.8-3; and the mechanical properties are: internal friction angle of 19°-22°, cohesion of 1-3 kPa, modulus of 5-9 MPa, and Poisson's ratio of 0.2-0.3.

2 . The transparent frozen soil according to claim 1 , characterized in that said water is purified water.

3 . A production method for the transparent frozen soil according to claim 1 , characterized in that it includes the following steps:
(1) material preparation: the dosages of the fluorine-containing polymer, the cube ice and the colorless pore fluid are calculated according to the test conditions and the sample size dimensions; said fluorine-containing polymer is particles with the particle diameter ≦0.074 mm, and is subjected to impurity cleaning and oven dried, and its particles have irregular shape, and are Teflon AF 1600 produced by American DuPont Company, with the refractive index of 1.31, and the density of 2.1-2.3 g/cm 3 ; said cube ice is obtained by mashing a frozen whole ice block, with the particle diameter ≦0.074 mm; and said colorless pore liquid is water; (2) blending: in a −6.0° C. to −8.0° C. cryogenics laboratory, firstly the fluorine-containing polymer and the cube ice are stirred uniformly, and loaded into a mold by 2-3 batches for the preparation of a sample, and compacted layer by layer; then water is added into the mold, and fills gaps between the fluorine-containing polymer particles and the cube ice; (3) vacuuming: a vacuuming device is utilized to remove bubbles residual inside the sample, so that the sample reaches a fully saturated state; (4) consolidating: placing the sample in a consolidometer for consolidation, with the over-consolidation ratio OCR value of 0.8-3; and (5) freezing: the sample is loaded in a −20° C. cryogenic box for freezing for 48 h, so as to prepare a transparent frozen soil simulating saturated frozen clay, the physical properties of which are: density of 1.63-2.1 g/cm 3 , unit weight of 16-21 kN/m 3 , and over-consolidation ratio over-consolidation ratio OCR value of 0.8-3; and the mechanical properties are: internal friction angle of 19°-22°, cohesion of 1-3 kPa, modulus of 5-9 MPa, and Poisson's ratio of 0.2-0.3.

4 . The production method of said transparent frozen soil according to claim 3 , characterized in that in step (1), said water is purified water.

5 . Application of said transparent frozen soil according to claim 1 in the frozen soil directional blasting model test.

6 . The application according to claim 5 , characterized by includes the following processes:
(1) modeling: according to the test requirements and the natural frozen soil side slope model dimensions, a transparent model tank and a transparent frozen soil side slope model simulating the natural frozen soil side slope model are made, respectively, said transparent frozen soil side slope model is made of transparent frozen soil, and reserved with blast holes; and said transparent model tank is made of transparent toughened glass; (2) mounting; the transparent frozen soil side slope model is loaded into the transparent model tank, and according to the test design, detonators and explosive are loaded in the reserved blast holes; and digital cameras capable of observing the space of the whole transparent model tank are arranged on the front view face, the side view face and the top view face outside the transparent model tank, and the digital cameras are connected with a processing device via data lines; (3) testing: the detonators and explosive are detonated, the process of the directional blasting of the transparent frozen soil side slope model to form an artificial side slope is observed and recorded by the digital cameras, and the recorded data are sent to the processing device by data lines; and (4) process (1)-process (3) are repeated, the directional blasting processes of the transparent frozen soil side slope model under the conditions of different natural side slop heights, different blast hole diameters and depths and different explosive dosages can be observed by the processing device, so as to analyze the directional blasting mechanism of the frozen soil, and complete the directional blasting test of the frozen soil side slop model.

7 . Application of transparent frozen soil according to claim 1 in the frozen soil road embankment model thawing-slumping test.

8 . The application according to claim 7 , characterized by comprising the following steps:
(1) modeling: according to the test requirements and frozen soil road embankment model dimensions the transparent model tank and the transparent frozen soil road embankment model simulating the frozen soil road embankment model are made, respectively, said transparent frozen soil road embankment model is made of the transparent frozen soil material, and pre-embedded with temperature sensors; and said transparent model tank is made of organic glass; (2) mounting; in a cryogenic laboratory, the transparent frozen soil road embankment model is loaded into the transparent model tank, and a heating source is mounted on the transparent model tank, and above the adret face of the transparent frozen soil road embankment model; outside the transparent model tank, one side parallel to the cross section of the transparent frozen soil road embankment model is provided with a laser source, and one side perpendicular to the cross section of the transparent frozen soil road embankment model is provided with a digital camera, and the digital camera and the temperature sensor are connected with the processing device via a data line; and the axial line of said digital camera is perpendicular to that of said laser source, and the intersection point of the axial line of said digital camera and that of said laser source is located inside said transparent model tank; and (3) testing: the laser source is turned on, the brightness of the tangent plane of particles formed inside the transparent frozen soil road embankment model is inspected, and the laser angle is adjusted, so that the laser is perpendicularly incident onto the tangent plane, and through the middle position of the longitudinal direction of the transparent frozen soil road embankment model; the digital camera is turned on, and the lens of the digital cameras is adjusted, so that it can cover the adret face and the ubac face of the transparent frozen soil road embankment model; i.e. the laser source irradiates the cross section of the transparent frozen soil road embankment model, and the cross section of the transparent frozen soil road embankment model irradiated by the laser source is recorded by the digital camera; and according to the experiment design, the heating source is intermittently turned on, the thawing-slumping process of the adret face of the transparent frozen soil road embankment model under the periodic cycle of freezing and thawing is observed and recorded by the digital cameras, and the recorded data are sent to the p

Assignees

• Univ Hohai

Inventors

• Kong Gangqiang

Classifications

• C09K17/00

  Soil-conditioning materials or soil-stabilising materials (specially adapted for boreholes or wells C09K8/00; fertilisers C05; consolidating by placing solidifying or pore-filling substances in the soil E02D3/12) · CPC title

• G01N33/24

  Earth materials (G01N33/42 takes precedence) · CPC title

• C08F224/00

  Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a heterocyclic ring containing oxygen (cyclic esters of polyfunctional acids C08F218/00; cyclic anhydrides of unsaturated acids C08F220/00, C08F222/00) · CPC title

• G01N1/28 Primary

  Preparing specimens for investigation {including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q}(mounting specimens on microscopic slides G02B21/34; means for supporting the objects or the materials to be analysed in electron microscopes H01J37/20 {; laboratory gas handling apparatus B01L5/00}) · CPC title

• E02D33/00

  Testing foundations or foundation structures (testing methods and apparatus, see the relevant subclasses of class G01; testing structures or apparatus as regards function, in general, G01M; testing or determining chemical or physical properties, in general G01N) · CPC title