Method for drying biomass

Patent metadata

Field	Value
Publication number	US-2016249642-A1
Application number	US-201415027429-A
Country	US
Kind code	A1
Filing date	Oct 1, 2014
Priority date	Oct 8, 2013
Publication date	Sep 1, 2016
Grant date	—

Abstract

It has been found in accordance with the invention that a biomass comprising an oxidation-sensitive material of value may be particularly readily converted into a particulate, flowable composition if a silica, especially a hydrophilic or hydrophobic silica, is added as additive.

First claim

1 - 15 . (canceled)

16 . A method for preparing a particulate free-flowing biomass comprising an oxidation-sensitive material of value, wherein said method comprises:
a) obtaining a fermentation broth comprising biomass; b) optionally concentrating said fermentation broth to produce a concentrated broth; c) drying either said fermentation broth or said concentrated broth; d) adjusting the amount of silica in said fermentation broth or said concentrated broth either before or after the drying of step c) so that the concentration of silica in said particulate free-flowing biomass is 0.1-8% by weight.

17 . The method of claim 16 , wherein the silica is a hydrophilic silica.

18 . The method of claim 17 , wherein the hydrophilic silica has a specific surface area of 150 to 600 m 2 /g and a dioctyl adipate absorption value of 2-3.5 ml/g.

19 . The method of claim 16 , wherein the silica is a hydrophobic silica.

20 . The method of claim 19 , wherein the hydrophobic silica has a methanol wettability of at least 40%.

21 . The method of claim 16 , wherein the oxidation-sensitive material of value is an unsaturated fatty acid.

22 . The method of claim 16 , wherein the silica is adjusted so that the concentration of silica in the particulate biomass is 0.2 to 6% by weight.

23 . The method of claim 16 , wherein the biomass comprises cells from the taxon Labyrinthulomycetes.

24 . The method of claim 16 , wherein the fermentation broth has a solids content of 10 to 50% by weight, and is converted to the particulate biomass by drying.

25 . The method of claim 16 , wherein biomass is dried by a thermal process and silica is added during the drying process.

26 . The method of claim 16 , wherein:
a) the oxidation-sensitive material of value is an omega-3 fatty acid or an omega-6 fatty acid; b) the silica is adjusted so that the concentration of silica in the particulate biomass is 0.2 to 6% by weight; and c) the biomass comprises cells from the family of Thraustochytriaceae.

27 . The method of claim 16 , wherein:
a) the oxidation-sensitive material of value is DHA; b) the silica is adjusted so that the concentration of silica in the particulate biomass is 0.5 to 2.5% by weight; and c) the biomass comprises cells from the genera Thraustochytrium, Schizochytrium or Aurantiochytrium.

28 . A particulate free-flowing biomass comprising an oxidation-sensitive material of value and silica in an amount of 0.1 to 8% by weight.

29 . The particulate biomass of claim 28 , wherein the silica is a hydrophilic silica with a specific surface area of 130 to 600 m 2 /g and a dioctyl adipate absorption value of 1.5-4.0 ml/g.

30 . The particulate biomass of claim 28 , wherein the silica is a hydrophobic silica with a methanol wettability of at least 40%.

31 . The particulate biomass of claim 28 , wherein at least 80% of particles by weight have a particle size of 100 to 3500 micrometres.

32 . The particulate biomass of claim 28 , wherein the biomass comprises cells from the taxon Labyrinthulomycetes.

33 . The particulate biomass of claim 28 , wherein:
a) the particulate biomass comprises silica in an amount of 0.2 to 6% by weight; b) the silica is either:
i) a hydrophilic silica with a specific surface area of 130 to 600 m 2 /g, and a dioctyl adipate absorption value of 1.5-4.0 ml/g; or
ii) a hydrophobic silica with a methanol wettability of at least 40%;
c) at least 80% by weight of the particles have a particle size of 100 to 3500 micrometres; d) the biomass comprises cells from the family Thraustochytriaceae.

34 . The particulate biomass of claim 28 , wherein:
a) the particulate biomass comprises silica in an amount of 0.5 to 2.5% by weight; b) the silica is either:
i) a hydrophilic silica with a specific surface area of 160 to 550 m 2 /g, and a dioctyl adipate absorption value of 2.0 to 3.2 ml/g; or
ii) a hydrophobic silica, with a methanol wettability of at least at least 50%;
c) at least 95% by weight, of the particles have a particle size of 100 to 2500 micrometres; d) the biomass comprises cells from the genera Thraustochytrium, Schizochytrium or Ulkenia.

35 . A feedstuff or foodstuff containing the particulate biomass of claim 28 and also other feedstuff ingredients.

Assignees

• Evonik Degussa Gmbh

Inventors

• Rabe Christian
• Alt Hans Christian
• Fischer Frank
• Eils Stefan
• Priefert Horst
• Diehl Michael

Classifications

• A23K20/28

  Silicates, e.g. perlites, zeolites or bentonites · CPC title

• C12N1/20

  Bacteria; Culture media therefor · CPC title

• A23K40/10

  by agglomeration; by granulation, e.g. making powders · CPC title

• A23K20/158

  Fatty acids; Fats; Products containing oils or fats · CPC title

• C11B5/00

  Preserving by using additives, e.g. anti-oxidants · CPC title