Method for producing crystallized glass member having curved shape
US-2024018029-A1 · Jan 18, 2024 · US
US12590027B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-12590027-B2 |
| Application number | US-202017763809-A |
| Country | US |
| Kind code | B2 |
| Filing date | Sep 24, 2020 |
| Priority date | Sep 26, 2019 |
| Publication date | Mar 31, 2026 |
| Grant date | Mar 31, 2026 |
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The invention relates to the field of materials based on mineral fibers, in particular mineral wool such as glass wool or rock wool. More specifically, the present invention relates to a method and a device for recycling the water recovered in a fiberizing and shaping method when using a specific acid binder based on monomeric polycarboxylic acid, or a salt of such an acid.
Opening claim text (preview).
The invention claimed is: 1 . A method for reducing the corrosion of equipment during production of a mineral fiber mat, said method comprising: fiberizing fibers and then bonding them with the aid of an aqueous binder comprising at least one sugar selected from hydrogenated sugars, reducing sugars, and non-reducing sugars, and at least one monomeric polycarboxylic acid or salt thereof in a forming zone; cross-linking the aqueous binder in an oven; and washing the equipment in the forming zone with wash water that is continuously recycled in a first recycling loop and whose pH is adjusted to a value between 6 and 9 before being recycled to said forming zone along said first recycling loop, the method further comprising washing fumes from the oven with water and recycling the fumes' wash water; in a second recycling loop, separate from the first, a portion of the recycled fumes' wash water being transferred at intervals to a zone for preparing said aqueous binder, without adjusting its pH. 2 . The method according to claim 1 , wherein the pH value is adjusted with a base selected from an alkali metal hydroxide, an alkali metal carbonate, an alkaline earth metal hydroxide, and an alkaline earth metal carbonate. 3 . The method according to claim 1 , wherein the aqueous binder comprises at least one hydrogenated sugar selected from: erythritol, arabitol, xylitol, sorbitol, mannitol, iditol, maltitol, isomaltitol, lactitol, cellobitol, palatinitol, maltotriol, hydrogenation products of starch hydrolysates, and hydrogenation products of lignocellulosic materials. 4 . The method according to claim 1 , wherein the aqueous binder comprises at least one reducing sugar selected from: a monosaccharide and a disaccharide. 5 . The method according to claim 1 , wherein the aqueous binder comprises at least one non-reducing sugar selected from: disaccharides, trisaccharides, tetrasaccharides and pentasaccharides. 6 . The method according to claim 1 , wherein the monomeric polycarboxylic acid is selected from dicarboxylic acids, tricarboxylic acids, and tetracarboxylic acids. 7 . The method according to claim 1 , wherein a quantity of water equivalent to the quantity of wash water transferred to the preparation zone of said aqueous binder is introduced at intervals into the fumes' wash water. 8 . The method according to claim 1 , wherein the recycled fumes' wash water is filtered before being used for the preparation of the aqueous binder. 9 . The method according to claim 1 , wherein the aqueous binder comprises at least one hydrogenated sugar selected from: xylitol, maltitol, sorbitol, hydrogenation products of starch hydrolysates, and hydrogenation products of lignocellulosic materials. 10 . The method according to claim 1 , wherein the aqueous binder comprises at least one reducing sugar selected from: glucose, galactose, mannose, and fructose. 11 . The method according to claim 1 , wherein the aqueous binder comprises at least one reducing sugar selected from: glucose and fructose. 12 . The method according to claim 1 , wherein the aqueous binder comprises at least one reducing sugar selected from: lactose, maltose, isomaltose, and cellobiose. 13 . The method according to claim 1 , wherein the aqueous binder comprises a non-reducing sugar, which is sucrose. 14 . The method according to claim 1 , wherein the monomeric polycarboxylic acid is citric acid.
After-treatment · CPC title
by dipping, immersion · CPC title
Cleaning, e.g. for reuse (C03C25/62 -C03C25/66 take precedence) · CPC title
obtained otherwise than by reactions involving only carbon-to-carbon unsaturated bonds · CPC title
Dipping · CPC title
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