Method for forming a film comprising nanocellulose
US-11518858-B2 · Dec 6, 2022 · US
US12398996B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-12398996-B2 |
| Application number | US-202017757253-A |
| Country | US |
| Kind code | B2 |
| Filing date | Dec 18, 2020 |
| Priority date | Dec 20, 2019 |
| Publication date | Aug 26, 2025 |
| Grant date | Aug 26, 2025 |
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The present document discloses a method of determining thickness of a wet film, in particular of microfibrillated cellulose. The method comprises conveying said film ( 20 ) in a wet state on a conveyor ( 10 ) having a conveyor width, the wet film having a film width which is less than the conveyor width, providing a laser projection ( 1511 ) across a film edge, acquiring a series of images, each depicting an area of the conveyor, wherein the laser projection, a portion of the film and a portion of an exposed conveyor surface are visible, and using at least some of said images to determine at least one of a film thickness and a film thickness distribution across the film width. The document also discloses a method of forming a film, in particular a microfibrillated cellulose film, and a device for producing such film.
Opening claim text (preview).
The invention claimed is: 1. A method of determining thickness of a wet cellulose-based film, comprising: forming said wet cellulose-based film on a conveyor using a casting device, wherein said wet cellulose-based film comprises a film forming component distributed in a medium; conveying said wet cellulose-based film, in a wet state, on the conveyor having a conveyor width, the wet cellulose-based film having a wet film width which is less than the conveyor width; providing a laser projection across the conveyor, the laser projection extending across a wet film edge; acquiring a series of images, each depicting an area of the conveyor, wherein the laser projection, a portion of the wet film, and a portion of an exposed conveyor surface are visible, wherein said wet cellulose-based film comprises at least 75% by weight of the medium when the series of images is acquired, and using at least some of said images to determine at least one of a wet film thickness and a wet film thickness distribution across the wet film width; and drying the wet cellulose-based film in a first drying device. 2. The method as claimed in claim 1 , wherein the laser projection extends over a width which is greater than the wet film width. 3. The method as claimed in claim 1 , wherein the wet cellulose-based film comprises at least 90% by weight of the medium when the series of images is acquired. 4. The method as claimed in claim 1 , wherein the wet cellulose-based film is a cellulose based film. 5. The method as claimed in claim 1 , wherein the laser projection is applied between the casting device and the first drying device. 6. The method as claimed in claim 1 , wherein the laser projection is applied at a position along a forward direction of the conveyor, where a belt support is arranged. 7. The method as claimed in claim 1 , wherein the conveyor is a metal belt conveyor, a polymer conveyor, or a paper conveyor. 8. The method as claimed in claim 1 , wherein the conveyor extends laterally beyond the wet film edge at both lateral sides of the wet cellulose-based film. 9. The method as claimed in claim 1 , wherein the laser projection is applied as a fixed pattern, or wherein the laser is scanned with a frequency that is greater than an image capture frequency so as to effectively present a pattern. 10. The method as claimed in claim 1 , wherein the laser projection is applied from a laser direction which extends at an angle to a direction of travel of the conveyor, and in a vertical plane containing said direction of travel, said angle being 5-80 degrees. 11. The method as claimed in claim 1 , wherein the laser projection is applied from a laser direction which extends at an angle to a direction of travel of the conveyor, and in a vertical plane containing said direction of travel, said angle being 100-175 degrees. 12. The method as claimed in claim 10 , wherein the images are captured such that an image plane of the image capture device is perpendicular to a line that extends in the vertical plane and at an angle of 30-150 degrees to the laser direction. 13. The method as claimed in claim 1 , wherein a wet film thickness is determined as a difference between a measured distance to a conveyor surface laterally outside the wet cellulose-based film and a measured distance to a wet film surface. 14. The method as claimed in claim 1 , wherein an average wet film thickness is determined as a difference between a measured distance to a conveyor surface laterally outside the wet film and a plurality of measured distances to a wet film surface within the wet film width. 15. The method as claimed in claim 1 , wherein the wet cellulose-based film is a microfibrillated cellulose film. 16. A method of producing a wet cellulose-based film, comprising: providing a continuous conveyor having a conveyor width, using a casting device for applying the wet cellulose-based film comprising a film forming component, which is distributed in a medium that is to be essentially removed, onto the conveyor, so as to solvent cast the wet cellulose-based film, determining a wet film thickness, or a wet film thickness distribution, or both by: providing a laser projection across the conveyor, the laser projection extending across a wet film edge, acquiring a series of images, each depicting an area of the conveyor, wherein the laser projection, a portion of the wet cellulose-based film, and a portion of an exposed conveyor surface are visible, wherein said wet cellulose-based film comprises at least 75% by weight of the medium when the series of images is acquired, and using at least some of said images to determine at least one of the wet film thickness and the wet film thickness distribution across the wet film width, and adjusting at least one casting parameter based on said determined wet film thickness, or said wet film thickness distribution, or both, so as to change the wet film thickness, the wet film thickness distribution, or both provided by the casting device. 17. The method as claimed in claim 16 , wherein adjusting at least one casting parameter comprises adjusting a wet film feed rate, or a feed distribution, or both. 18. The method as claimed in claim 16 , wherein adjusting at least one casting parameter comprises adjusting a doctor blade, which is configured for controlling the wet film thickness, or the wet film thickness distribution, or both. 19. The method as claimed in claim 16 , wherein adjusting at least one casting parameter comprises adjusting a lip of a slot die type casting unit. 20. A device for producing a wet cellulose-based film, comprising: a continuous conveyor having a conveyor width; a casting device for applying the wet cellulose-based film comprising a film forming component, which is distributed in a medium that is to be essentially removed, onto the conveyor, for solvent casting the wet cellulose-based film to provide a wet film width that is less than the conveyor width; a laser projection device configured to provide a laser projection across a wet film edge; an image capture device configured to acquire a series of images, each depicting an area of the conveyor, wherein the laser projection, a portion of the wet cellulose-based film, and a portion of an exposed conveyor surface are visible, the image capture device positioned at a location wherein said wet cellulose-based film comprises at least 75% by weight of the medium when the series of images is acquired; and a processing device, configured to use at least some of said images to determine at least one of a wet film thickness and a wet film thickness distribution across the wet film width. 21. The device as claimed in claim 20 , further comprising an adjustable device configured for adjusting the casting device based on said determined wet film thickness, said determined wet film thickness distribution, or both so as to change the wet film thickness, the wet film thickness distribution, or both provided by the casting device.
Objects on a conveyor · CPC title
Fibrous material · CPC title
Method using an image detector and processing of image signal · CPC title
Investigating thin films, e.g. matrix isolation method · CPC title
by measuring distance between sensor and object (G01B11/0608 takes precedence) · CPC title
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