Process for preparing a powder of material of natural origin

Patent metadata

Field	Value
Publication number	US-12351691-B2
Application number	US-202117759892-A
Country	US
Kind code	B2
Filing date	Feb 3, 2021
Priority date	Feb 3, 2020
Publication date	Jul 8, 2025
Grant date	Jul 8, 2025

Abstract

A process for preparing a powder of a material of natural origin, which includes a step of treating a substance containing at least 70% by weight of one or more leather wastes in particle form in a twin-screw extruder, wherein a temperature profile is applied that increases from an initial temperature of between 10 and 40° C. up to a maximum temperature of between 60 and 120° C., in the presence of water in an amount such that the weight ratio of water to substance is between 0.20 and 6.

First claim

What is claimed is:

1. A method for preparing a powder of a material of natural origin, comprising a step of treating an initial substance containing at least 70% by weight of leather prepared from non-human animal skin by tanning, in particulate form, in a twin-screw extruder wherein a temperature profile is applied that increases from an initial temperature of between 10° C. and 40° C. in an entry zone of the twin-screw extruder, up to a maximum temperature of between 60° C. and 120° C. in a last kneading zone of the twin-screw extruder, in the presence of water in an amount such that the weight ratio of water to said initial substance is between 0.20 and 6.

2. The method according to claim 1 , wherein the step of treating the initial substance is carried out in the presence of water in an amount such that the weight ratio of water relative to the initial substance is greater than or equal to 0.2 and less than 1.6.

3. The method according to claim 1 , wherein the step of treating the initial substance is carried out in the presence of water in an amount such that the weight ratio of water relative to the initial substance is between 1.6 and 6.

4. The method according to claim 1 , wherein said twin-screw extruder is a co-rotating screw extruder.

5. The method according to claim 1 , wherein said initial substance is in particulate form with a grain size between 5 mm and 10 cm.

6. The method according to claim 1 , wherein an input flow rate of said initial substance in particulate form into the twin-screw extruder is between 1 and 15 kg/h.

7. The method according to claim 1 , wherein said twin-screw extruder includes at least two kneading zones.

8. The method according to claim 7 , wherein a rotational speed of the twin-screw extruder screws is between 100 and 400 rpm.

9. The method according to claim 1 , wherein said initial substance is placed in the presence of water by introducing an aqueous solution into the twin-screw extruder.

10. The method according to claim 9 , wherein the aqueous solution contains an agent for decomplexing chromium-collagen complexes.

11. The method as claimed in claim 9 , wherein the aqueous solution is introduced into the twin-screw extruder before a first kneading zone of said twin-screw extruder.

12. The method according to claim 1 , comprising a step of drying an extrudate obtained following said treatment step.

13. The method as claimed in claim 1 , wherein the step of treating the initial substance is carried out in the presence of water in an amount such that the weight ratio of water relative to the initial substance is equal to 0.25.

14. The method as claimed in claim 1 , wherein the step of treating the initial substance is carried out in the presence of water in an amount such that the weight ratio of water relative to the initial substance is equal to 0.6.

15. The method as claimed in claim 1 , wherein the initial substance comprises no polymer or polymer precursor substance, and it is not mixed with any polymer or polymer precursor substance during said step of treating in said twin-screw extruder.

16. The method as claimed in claim 1 , wherein said twin-screw extruder does not include any die at the exit.

17. A method for preparing a powder of a material of natural origin, comprising a step of treating an initial substance containing at least 70% by weight of leather prepared from non-human animal skin by tanning, in particulate form, in a twin-screw extruder wherein a temperature profile is applied that increases from an initial temperature of between 10° C. and 40° C. in an entry zone of the twin-screw extruder, up to a maximum temperature of between 60° C. and 120° C. in a last kneading zone of the twin-screw extruder, in the presence of water in an amount such that the weight ratio of water to said initial substance is between 0.20 and 6, wherein the step of treating an initial substance is carried out in the presence of water in the amount such that the weight ratio of water relative to the initial substance is comprised between 0.2 and 0.6.

Assignees

• Authentic Mat
• Inst Nat Polytechnique Toulouse
• Institut National De Rech Pour Lagriculture Lalimentation Et Lenvironnem
• Institut National De Rech Pour Lagriculture Lalimentation Et Lenvironnment

Inventors

• Jumeaux Margaux
• Verniolle Paul
• Rouilly Antoine
• Vandenbossche Virginie

Classifications

• B29C48/875

  for achieving a non-uniform temperature distribution, e.g. using barrels having both cooling and heating zones · CPC title

• C08L89/06

  derived from leather or skin {, e.g. gelatin} · CPC title

• B29C48/78

  Thermal treatment of the extrusion moulding material or of preformed parts or layers, e.g. by heating or cooling · CPC title

• B29K2911/08

  Leather · CPC title

• B29B9/10

  by moulding the material, i.e. treating it in the molten state · CPC title