Gas-processing systems and methods

Patent metadata

Field	Value
Publication number	US-12343671-B2
Application number	US-202217837710-A
Country	US
Kind code	B2
Filing date	Jun 10, 2022
Priority date	Jun 23, 2021
Publication date	Jul 1, 2025
Grant date	Jul 1, 2025

Abstract

Described are gas-processing systems that include a pre-heater, that are useful for processing a flow of gas flowing the gas to contact media (e.g., purification media, catalyst, adsorbent), and related methods.

First claim

The invention claimed is:

1. A gas-processing apparatus comprising:
a media vessel comprising:
a media vessel inlet end comprising a media vessel inlet,
a media vessel outlet end comprising a media vessel outlet,
a media vessel sidewall extending a length between the inlet end and the outlet end, and
a media vessel interior extending between the inlet end and the outlet end;

a gas pre-heater located along a length of the media vessel sidewall,
a gas pre-heater inlet that allows a gas to pass between an exterior location and a gas pre-heater interior, the gas pre-heater inlet being located between the media vessel inlet end and the media vessel outlet end,
a gas pre-heater outlet that allows a gas to pass between an exterior location and the pre-heater interior, and
an opening at the outlet end of the media vessel that allows gas to pass between the pre-heater interior and the media vessel interior.

2. The gas-processing apparatus of claim 1 , wherein the gas pre-heater is in thermal contact with the media vessel sidewall.

3. The gas-processing apparatus of claim 1 , the gas pre-heater extending around a circumference of the media vessel sidewall.

4. The gas-processing apparatus of claim 1 , wherein the gas pre-heater extends from the outlet end along a portion of the length of the media vessel sidewall.

5. The gas-processing apparatus of claim 1 , further comprising a heating element in thermal contact with at least a portion of the gas pre-heater, with the gas pre-heater disposed between the media vessel sidewall and the heating element.

6. The gas-processing apparatus of claim 1 , further comprising thermal insulation that covers at least a portion of the gas pre-heater, with the gas pre-heater disposed between the media vessel and the thermal insulation.

7. The gas-processing apparatus of claim 1 , further comprising an apertured endwall at the media vessel outlet, the apertured endwall separating the media vessel interior from an interior of the gas pre-heater.

8. The gas-processing apparatus of claim 1 , wherein the gas pre-heater has a pre-heater interior volume that is less than 30 percent of a volume of the media vessel interior.

9. The gas-processing apparatus of claim 1 , the gas pre-heater comprising:
an inner sidewall extending along a portion of the length of the media vessel sidewall and around a perimeter of the sidewall,
an outer sidewall extending along a portion of the length of the media vessel sidewall and around a perimeter of the sidewall,
a pre-heater endwall spaced from the media vessel outlet, and
a pre-heater interior volume comprising:
an annular volume bounded by the inner sidewall and the outer sidewall, and
an end volume bounded by an end of the media vessel outlet, and the pre-heater endwall.

10. The gas-processing apparatus of claim 9 , wherein the annular volume comprises a spiral channel that causes gas to flow through the annular volume in a spiral-shaped path around a circumference of the annular volume.

11. The gas-processing apparatus of claim 9 , wherein the annular volume comprises a spiral channel that causes gas to flow through the annular volume in a spiral-shaped path around a circumference of the annular volume.

12. The gas-processing apparatus of claim 1 , the media vessel comprising media selected from adsorption media and catalyst.

13. A method of using a gas-processing apparatus, the apparatus comprising:
a media vessel comprising:
a media vessel inlet end comprising a media vessel inlet,
a media vessel outlet end comprising a media vessel outlet,
a media vessel sidewall extending a length between the inlet end and the outlet end,

a media vessel interior extending between the inlet end and the outlet end, and
media contained in the interior;

a gas pre-heater located along a length of the media vessel sidewall; and
a heating element covering at least a portion of the pre-heater, the method comprising:
flowing a gas through the gas pre-heater to pre-heat the gas, and
passing the pre-heated gas through the media vessel interior and in contact with the media.

14. The method of claim 13 , wherein the media is adsorption media and the gas is a regeneration gas, the method comprising:
flowing raw material gas through the media vessel interior and in contact with the adsorption media to allow an impurity contained in the raw material gas to be adsorbed by the adsorption media and removed from the process gas,
after flowing the raw material gas through the media vessel interior:
flowing a regeneration gas through the gas pre-heater to pre-heat the regeneration gas, and
flowing the pre-heated regeneration gas through the media vessel interior and in contact with the adsorption media.

15. The method of claim 14 , the apparatus comprising:
a pre-heater inlet that allows a gas to pass between an exterior location and a pre-heater interior, the pre-heater inlet being located between the media vessel inlet end and the media vessel outlet end,
a pre-heater outlet that allows a gas to pass between an exterior location and the pre-heater interior, and
an opening at the outlet end of the media vessel that allows gas to pass between a pre-heater interior and the media vessel interior, the method comprising:

wherein:
the process gas enters the media vessel interior through the media vessel inlet, and
the process gas leaves the media vessel interior through the media vessel outlet, to pass into the pre-heater interior, and
the process gas flows out of the pre-heater interior through the pre-heater outlet.

16. The method of claim 15 , wherein
the regeneration gas enters the pre-heater interior through the pre-heater inlet,
the regeneration gas leaves the pre-heater interior through the media vessel outlet, to pass into the media vessel interior, and
the regeneration gas flows out of the media vessel interior through the media vessel inlet.

17. The method of claim 14 , further comprising flowing the raw material gas through the media vessel interior at a raw material gas flow rate and flowing the regeneration gas through the gas pre-heater at a regeneration gas flow rate that is less than the raw material gas flow rate.

18. The method of claim 14 , further comprising flowing the raw material gas through the interior at a raw material gas pressure and flowing the regeneration gas through the gas pre-heater at a regeneration gas pressure that is less than the raw material gas pressure.

19. The method of claim 14 , wherein the raw material gas is selected from nitrogen, argon, hydrogen, ammonia, carbon dioxide, clean dry air, and oxygen.

20. A gas-processing apparatus comprising:
a media vessel comprising:
a media vessel inlet end comprising a media vessel inlet,
a media vessel outlet end comprising a media vessel outlet,
a media vessel sidewall extending a length between the inlet end and the outlet end, and

a media vessel interior extending between the inlet end and the outlet end; and
a gas pre-heater located along a length of the media vessel sidewall, the gas pre-heater comprising:
an inner sidewall extending along a portion of the length of the media vessel sidewall and around a perimeter of the sidewall,
an outer sidewall extending along a portion of the length of the media vessel sidewall and around a perimeter of the sidewall,
a pre-heater endwall spaced from the media vessel outlet, and
a pre-heater interior volume comprising:
an annular volume bounded by the inner sidewall and the outer sidewall,

Assignees

• Entegris Inc

Inventors

• Applegarth Charles H
• Le Gary
• D'Antonio Luke
• Schlotterbeck Matthew

Classifications

• B01D53/0446

  Means for feeding or distributing gases · CPC title

• B01D53/0462

  Temperature swing adsorption · CPC title

• B01D53/885

  Devices in general for catalytic purification of waste gases · CPC title

• B01D2259/4009

  using hot gas · CPC title

• B01D2259/45

  Gas separation or purification devices adapted for specific applications · CPC title