Method and fluidized bed granulator for the production of granules from a slurry

Patent metadata

Field	Value
Publication number	US-12233394-B2
Application number	US-201917271317-A
Country	US
Kind code	B2
Filing date	Oct 18, 2019
Priority date	Oct 18, 2018
Publication date	Feb 25, 2025
Grant date	Feb 25, 2025

Abstract

A method for granulating a slurry in a fluidized bed granulator having a main longitudinal direction from a seed end where granulation is initiated, to a product discharge end where granules are discharged from the fluidized bed granulator, including at least one fluidized bed compartment, an injection section and a granulation section, separated by a bottom plate including one or more injection nozzles, wherein a feed slurry is provided to the injection section, wherein a first fraction of the feed slurry provided to the injection section is injected into the granulation section through the one or more injection nozzles and a second fraction of the feed slurry, being the remainder of the feed slurry, is passed through the injection section without being injected into the granulation section. A fluidized bed granulator for the granulation of slurries for fertilizer products such as UAS according to the method of the invention.

First claim

The invention claimed is:

1. A method for production of fertilizer granules by granulating a feed slurry in a fluidized bed granulator having a main longitudinal direction from a seed end where granulation is initiated, to a product discharge end where the fertilizer granules are discharged from the fluidized bed granulator, comprising at least one fluidized bed compartment, an injection section and a granulation section, separated by a bottom plate comprising one or more injection nozzles, wherein the feed slurry is provided to the injection section of the fluidized bed granulator, characterized in that a first fraction of the feed slurry provided to the injection section is injected into the granulation section through the one or more injection nozzles and a second fraction of the feed slurry, being a remainder of the feed slurry, is continuously passed through the injection section without being injected into the granulation section and is continuously returned to the injection section after it is mixed with the feed slurry, wherein the feed slurry maintains a predetermined minimum velocity within the injection section of the fluidized bed granulator.

2. The method according to claim 1 , wherein the predetermined minimum velocity of the feed slurry within the injection section is at least 0.5 m/s.

3. The method according to claim 1 , wherein the first fraction of the feed slurry ranges between 70% and 99% of the total feed slurry.

4. The method according to claim 1 , wherein the second fraction of the feed slurry ranges between 1% and 30% of the total feed slurry.

5. The method according to claim 1 , wherein the feed slurry comprises urea.

6. The method according to claim 1 , wherein the feed slurry comprises one or more of the following: ammonium sulfate, calcium dihydrogen phosphate, ammonium phosphate and potassium salts.

7. The method according to claim 1 , wherein the feed slurry comprises urea and, relative to the urea, more than 12 weight % of ammonium sulfate.

8. A method for reducing clogging of an injection section in a fluidized bed granulator for production of fertilizer granules, comprising at least one fluidized bed compartment having a main longitudinal direction from a seed end where granulation is initiated, to a product discharge end where granules are discharged from the fluidized bed granulator, an injection section and a granulation section, separated by a bottom plate comprising one or more injection nozzles, wherein a feed slurry is provided to the injection section of the fluidized bed granulator, characterized in that a first fraction of the feed slurry, provided to the injection section, is injected into the granulation section through the one or more injection nozzles and a second fraction of the feed slurry, being a remainder of the feed slurry, is continuously passed through the injection section without being injected into the granulation section and is continuously returned to the injection section after it is mixed with the feed slurry, wherein the feed slurry maintains a predetermined minimum velocity within the injection section of the fluidized bed granulator.

9. The method according to claim 1 , wherein the predetermined minimum velocity of the feed slurry within the injection section is higher than 2.0 m/s.

10. The method according to claim 1 , wherein the first fraction of the feed slurry ranges between 85% and 95% of the total feed slurry.

11. The method according to claim 1 , wherein the second fraction of the feed slurry ranges between 5% and 15% of the total feed slurry.

12. The method according to claim 8 , wherein the predetermined minimum velocity of the feed slurry within the injection section is at least 0.5 m/s.

13. A method for production of fertilizer granules by granulating a feed slurry in a fluidized bed granulator having a main longitudinal direction from a seed end where granulation is initiated, to a product discharge end where the fertilizer granules are discharged from the fluidized bed granulator, comprising at least one fluidized bed compartment, an injection section and a granulation section, separated by a bottom plate comprising one or more injection nozzles, wherein the feed slurry is provided to the injection section of the fluidized bed granulator, characterized in that a first fraction of the feed slurry provided to the injection section is injected into the granulation section through the one or more injection nozzles and a second fraction of the feed slurry, being a remainder of the feed slurry, is continuously passed through the injection section without being injected into the granulation section and is continuously returned to the injection section after it is mixed with the feed slurry, wherein the first fraction of the feed slurry ranges between 70% and 99% of the total feed slurry.

14. The method according to claim 13 , wherein the second fraction of the feed slurry ranges between 1% and 30% of the total feed slurry.

Assignees

• Yara Int Asa

Inventors

• Volke Howard

Classifications

• C05C9/00

  Fertilisers containing urea or urea compounds · CPC title

• C05B19/00

  Granulation or pelletisation of phosphatic fertilisers, other than slag (granulating apparatus B01J2/00; granulating slag C04B) · CPC title

• C05B7/00

  Fertilisers based essentially on alkali or ammonium orthophosphates (C05B11/00 takes precedence) · CPC title

• C05B3/00

  Fertilisers based essentially on di-calcium phosphate (C05B11/00 takes precedence) · CPC title

• B01J2/16 Primary

  by suspending the powder material in a gas, e.g. in fluidised beds or as a falling curtain · CPC title