Method and device for processing of granules

Patent metadata

Field	Value
Publication number	US-9527104-B2
Application number	US-201414270620-A
Country	US
Kind code	B2
Filing date	May 6, 2014
Priority date	Apr 28, 2008
Publication date	Dec 27, 2016
Grant date	Dec 27, 2016

Abstract

A method for processing of granules, by forming at least one injection zone in a fluidized bed where a feed stream of seed particles is contacted or coated by a liquid product by simultaneous injection of the feed stream of the seed particles and a feed stream of the liquid product, forming at least one granulation zone in the fluidized bed where the contacted or coated seed particles may be at least one of dried, shaped, and cooled to form granules, extracting the granules from the at least one granulation zone and sorting the extracted granules into undersize granules, on-size granules, and oversize granules, passing the on-size granules to post-processing treatment, removing the oversize granules, and passing the undersize granules back into the feed stream of the seed particles, wherein the extracted granules are made to pass through at least one classifier located in the at least one granulation zone.

First claim

The invention claimed is:

1. A granulator for forming granules from a liquid product, the granulator comprising:
a reactor with a fluidizing bed comprising i) one or more injection zone(s) where a feed stream of seed particles is contacted/coated by the liquid product, and ii) one or more granulation zone(s) where the contacted/coated seed particles are dried, shaped and cooled into solid granules;
a liquid feed inlet for introducing a feed stream of the liquid product into the one or more injection zone(s) in the form of a spray of dispersed liquid droplets;
a seed particle inlet for introducing the feed stream of seed particles into the one or more injection zone(s) such that the seed particles are contacted/coated with the liquid product in the form of the spray of dispersed liquid droplets;
an outlet for extracting granules from the one or more granulation zone(s) and sorting equipment for sorting the extracted granules into three size fractions; undersize granules with too small diameters compared to a desired size range, on-size granules with diameters within the desired size range, and oversize granules with too large diameters compared to the desired size range from the one or more granulation zone(s);
transportation means for passing the fraction of on-size granules to post-treatment equipment for forming product granules;
removal means for removing the fraction of oversize granules from the granulation process; and
transportation means for passing the fraction of undersize granules into the feed stream of seed particles,
wherein the fluidized bed comprises a classifier in the one or more granulation zone(s), and wherein the classifier segregates the granules according to size, the classifier passes at least a fraction of the segregated undersize granules in the classifier back to the one or more injection zone(s), and the classifier comprises two or more heat exchanger tubes, at a distance from each other, extending across a horizontally oriented cross-sectional area of the classifier.

2. The granulator according to claim 1 , wherein the removal means for removing the fraction of oversize granules comprises one or more of the following:
means for crushing the oversize granules to undersize granules and then passing the crushed granules to the feed stream of seed particles;
means for passing the oversize granules to the feed stream of the liquid product and thus recycling the oversize granules as liquid product; or
means for discharging the oversize granules to external facilities for end uses.

3. The granulator according to claim 2 , wherein the classifier has an overflow that directs the fraction of undersize granules back to the one or more injection zone(s).

4. The granulator according to claim 2 , wherein:
the reactor is shaped as a vertically oriented shaft with a square horizontal cross section and narrows in a funnel shape at an upper portion thereof, such that the funnel represents an exit for the fluidization air; and
the fluidization zone is formed on top of an air-distribution grate when fluidization air is made to pass through the air-distribution grate, and the fluidization zone is divided by a partition wall into an injection zone and a granulation zone.

5. The granulator according to claim 2 , wherein the liquid product is a urea melt.

6. The granulator according to claim 1 , wherein the two or more heat exchanger tubes are positioned at several heights of the classifier.

7. The granulator according to claim 1 , wherein the classifier has an overflow that directs the fraction of undersize granules back to the one or more injection zone(s).

8. The granulator according to claim 1 , wherein:
the reactor is shaped as a vertically oriented shaft with a square horizontal cross section and narrows in a funnel shape at an upper portion thereof, such that the funnel represents an exit for the fluidization air; and
the fluidization zone is formed on top of an air-distribution grate when fluidization air is made to pass through the air-distribution grate, and the fluidization zone is divided by a partition wall into an injection zone and a granulation zone.

Assignees

• Yara Int Asa

Inventors

• Ledoux Francois
• Vanmarcke Luc
• Volke Howard
• Bakker Peter De
• Fouw Remco De
• Elderson Roeland

Classifications

• B05C9/12 Primary

  the auxiliary operation being performed after the application (B05C9/14 takes precedence) · CPC title

• B05C3/02

  the work being immersed in the liquid or other fluent material · CPC title

• B01J2/16 Primary

  by suspending the powder material in a gas, e.g. in fluidised beds or as a falling curtain · CPC title