Apparatus to simulate biocide performance in crude pipeline conditions

Patent metadata

Field	Value
Publication number	US-12104128-B2
Application number	US-202318340420-A
Country	US
Kind code	B2
Filing date	Jun 23, 2023
Priority date	Sep 16, 2019
Publication date	Oct 1, 2024
Grant date	Oct 1, 2024

Abstract

An apparatus to simulate biocide performance in crude oil pipeline conditions is disclosed. The apparatus includes: a reactor to simulate a two-phase crude oil pipeline which includes a crude oil phase above a water phase. The reactor has an agitator to control a flow of the water phase in the reactor in response to a motor that drives an agitation rate of the agitator. A crude oil inlet supplies crude oil to the reactor for the crude oil phase. A water inlet supplies water to the reactor for the water phase. A control circuit is configured by code to control a proportion of the water to the crude oil supplied to the reactor and to control the motor to drive a desired agitation rate of the agitator. A biocide inlet supplies biocide to the reactor. A water sample outlet enables sampling of the water phase of the reactor.

First claim

What is claimed is:

1. An apparatus to simulate biocide performance in crude oil pipeline conditions, the apparatus comprising:
a reactor to simulate a two-phase crude oil pipeline and including a crude oil phase above a water phase, the reactor comprising an agitator to control a flow of the water phase in the reactor in response to a motor that drives an agitation rate of the agitator;
a crude oil inlet to supply crude oil to the reactor for the crude oil phase;
a water inlet to supply water to the reactor for the water phase;
a control circuit configured by logic or code to:
control a proportion of the water to the crude oil supplied to the reactor by the crude oil inlet and the water inlet, and
control the motor to drive a desired agitation rate of the agitator;

a biocide inlet to supply biocide to the reactor;
a water sample outlet to sample the water phase of the reactor; and
a plurality of coupon holders each configured to hold a corrosion coupon at a bottom of the agitated water phase of the reactor during a simulation, and to permit removing and replacing of the corrosion coupon during the simulation.

2. The apparatus of claim 1 , further comprising a ball valve for each coupon holder, the ball valve being configured to seal the reactor during the removal and replacement of the corrosion coupon.

3. An apparatus to simulate oil field chemical performance in crude oil pipeline conditions, the apparatus comprising:
a plurality of reactors each configured to simulate a two-phase crude oil pipeline and including a crude oil phase above a water phase, each reactor comprising an agitator to control a flow of the water phase in the reactor in response to a motor that drives an agitation rate of the agitator;
a crude oil inlet to supply crude oil to each reactor for the crude oil phase;
a water inlet to supply water to each reactor for the water phase;
a control circuit configured by logic or code to
independently control a proportion of the water to the crude oil supplied to each reactor by the crude oil inlet and the water inlet, and
independently control the motor of each reactor to drive a desired agitation rate of the agitator of the reactor;

a dedicated oil field chemical inlet for each reactor to supply an oil field chemical to the reactor; and
a dedicated water sample outlet for each reactor to sample the water phase of the reactor.

4. The apparatus of claim 3 , wherein the oil field chemical comprises at least one of a corrosion inhibitor and a biocide.

5. The apparatus of claim 3 , further comprising:
a crude oil pump to pump the crude oil from a crude oil supply to the crude oil inlet; and
a water pump to pump the water from a water supply to the water inlet,
wherein the control circuit controls the proportion of the water to the crude oil by controlling the crude oil pump and the water pump.

6. The apparatus of claim 3 , each reactor further comprising a plurality of coupon holders each configured to
hold a corrosion coupon at a bottom of the agitated water phase of the reactor during a simulation, and
permit removing and replacing of the corrosion coupon during the simulation.

7. The apparatus of claim 6 , further comprising a ball valve for each coupon holder, the ball valve being configured to seal the reactor during the removal and replacement of the corrosion coupon.

8. The apparatus of claim 3 , wherein
each reactor further comprises a bucket and the agitator comprises a rotor at the bottom of the bucket, the agitation rate being a rotation speed of the rotor, and
the control circuit further controls the motor of each reactor to adjust a height of the rotor above the bottom of the bucket of the reactor.

9. The apparatus of claim 3 , further comprising a dedicated height-adjustable dip tube for each reactor to obtain a mixed sample of the crude oil phase and the water phase of the reactor at an interphase region of the crude oil phase and the water phase in the reactor.

10. The apparatus of claim 3 , further comprising a dedicated heating element for each reactor to heat the reactor and a dedicated temperature sensor for each reactor to sense a temperature of the reactor, wherein the control circuit is further configured by logic or code to independently control the temperature of each reactor by using the temperature sensor to sense the temperature of the reactor and by using the heating element to heat the reactor in response to the sensed temperature.

11. A method to simulate oil field chemical performance in crude oil pipeline conditions, the apparatus comprising:
independently simulating a two-phase crude oil pipeline in each of a plurality of reactors each including a crude oil phase above a water phase;
independently controlling, using a processing circuit, a flow of the water phase in each reactor by independently controlling a motor of an agitator of each reactor to drive a desired agitation rate of the agitator of the reactor to agitate the water phase of the reactor;
independently supplying, using the processing circuit, crude oil to each reactor for the crude oil phase of the reactor;
independently supplying, using the processing circuit, water to each reactor for the water phase of the reactor to reach a desired proportion of the water to the crude oil supplied to the reactor;
independently supplying, through a dedicated oil field chemical inlet of each reactor, an oil field chemical to the reactor; and
independently sampling, through a dedicated water sample outlet of each reactor, the water phase of the reactor.

12. The method of claim 11 , wherein the oil field chemical comprises at least one of a corrosion inhibitor and a biocide.

13. The method of claim 12 , wherein independently supplying the oil field chemical comprises supplying the corrosion inhibitor to one of reactors and supplying the biocide to another one of the reactors.

14. The method of claim 13 , wherein independently supplying the oil field chemical further comprises supplying both the corrosion inhibitor and the biocide to yet another one of the reactors.

15. The method of claim 11 , further comprising removing and replacing a corrosion coupon at a bottom of the agitated water phase of each reactor during a simulation in the reactor.

16. The apparatus of claim 11 , wherein
each reactor further comprises a bucket and the agitator of each reactor comprises a rotor at the bottom of the bucket, the agitation rate being a rotation speed of the rotor, and
independently controlling the motor comprises independently controlling the motor of each reactor to adjust a height of the rotor above the bottom of the bucket of the reactor.

Assignees

• Saudi Arabian Oil Co

Inventors

• Zhu Xiangyang
• Al-Saleh Mazen A
• Ali Qurban

Classifications

• C12M37/06

  Means for testing the completeness of the sterilization (testing for sterility conditions C12Q1/22) · CPC title

• C12M41/38

  of metabolites or enzymes in the cells · CPC title

• C12M1/121

  with sterilisation means · CPC title

• C12M1/02

  with agitation means; with heat exchange means · CPC title

• C10G2300/80

  Additives · CPC title