Apparatus to simulate biocide performance in crude pipeline conditions

Patent metadata

Field	Value
Publication number	US-11718801-B2
Application number	US-201916572206-A
Country	US
Kind code	B2
Filing date	Sep 16, 2019
Priority date	Sep 16, 2019
Publication date	Aug 8, 2023
Grant date	Aug 8, 2023

Abstract

An apparatus to simulate biocide performance in crude oil pipeline conditions is disclosed. The apparatus includes: a reactor to simulate a two-phase crude oil pipeline which includes a crude oil phase above a water phase. The reactor has an agitator to control a flow of the water phase in the reactor in response to a motor that drives an agitation rate of the agitator. A crude oil inlet supplies crude oil to the reactor for the crude oil phase. A water inlet supplies water to the reactor for the water phase. A control circuit is configured by code to control a proportion of the water to the crude oil supplied to the reactor and to control the motor to drive a desired agitation rate of the agitator. A biocide inlet supplies biocide to the reactor. A water sample outlet enables sampling of the water phase of the reactor.

First claim

What is claimed is:

1. An apparatus to simulate biocide performance in crude oil pipeline conditions, the apparatus comprising:
an agitator motor;
a reactor to simulate a two-phase crude oil pipeline and including a crude oil phase above a water phase, the reactor comprising an agitator to control a flow of the water phase in the reactor in response to the agitator motor that drives an agitation rate of the agitator;
a crude oil inlet to supply crude oil to the reactor for the crude oil phase;
a water inlet to supply water to the reactor for the water phase;
a control circuit configured by logic or code to
control a proportion of the water to the crude oil supplied to the reactor by the crude oil inlet and the water inlet, and
control the agitator motor to drive a desired agitation rate of the agitator;

a biocide inlet to supply biocide to the reactor;
a water sample outlet to sample the water phase of the reactor;
a plurality of coupon holders each configured to
hold a corrosion coupon at a bottom of the agitated water phase of the reactor during the simulation of the two-phase crude oil pipeline, and
permit removing and replacing of the held corrosion coupon during the simulation;

a ball valve for each coupon holder, the ball valve being configured to seal the reactor during the removal and replacement of the corrosion coupon; and
a height-adjustable dip tube to obtain a mixed sample of the crude oil phase and the water phase of the reactor at an interphase region of the crude oil phase and the water phase in the reactor.

2. The apparatus of claim 1 , wherein
the reactor further comprises a plurality of reactors each having a dedicated biocide inlet and a dedicated water sample outlet, and
the control circuit is further configured by logic or code to independently control the proportion of the water to the crude oil and to independently control the agitator motor in each reactor.

3. The apparatus of claim 1 , further comprising:
a crude oil pump to pump the crude oil from a crude oil supply to the crude oil inlet; and
a water pump to pump the water from a water supply to the water inlet,
wherein the control circuit controls the proportion of the water to the crude oil by controlling the crude oil pump and the water pump.

4. The apparatus of claim 1 , wherein
the reactor further comprises a bucket and the agitator comprises a rotor at the bottom of the bucket, the agitation rate being a rotation speed of the rotor, and
the control circuit further controls the agitator motor to adjust a height of the rotor above the bottom of the bucket.

5. The apparatus of claim 1 , further comprising a heating element to heat the reactor and a temperature sensor to sense a temperature of the reactor, wherein the control circuit is further configured by logic or code to control the temperature of the reactor by using the temperature sensor to sense the temperature of the reactor and by using the heating element to heat the reactor in response to the sensed temperature.

6. The system of claim 1 , further comprising a nitrogen (N 2 ) gas inlet to supply N 2 gas to the reactor in order to provide anoxic conditions to the reactor during and after the simulation.

7. A method to simulate biocide performance in crude oil pipeline conditions, the method comprising:
simulating a two-phase crude oil pipeline in a reactor including a crude oil phase above a water phase;
controlling, using a processing circuit, a flow of the water phase in the reactor by controlling an agitator motor of an agitator to drive a desired agitation rate of the agitator in order to agitate the water phase;
supplying, through a crude oil inlet under the control of the processing circuit, crude oil to the reactor for the crude oil phase;
supplying, through a water inlet under the control of the processing circuit, water to the reactor for the water phase to reach a desired proportion of the water to the crude oil supplied to the reactor;
supplying, through a biocide inlet, biocide to the reactor;
sampling, through a water sample outlet, the water phase of the reactor;
holding, at each of a plurality of coupon holders, a corrosion coupon at a bottom of the agitated water phase of the reactor during the simulation of the two-phase crude oil pipeline;
removing and replacing, at each coupon holder, the held corrosion coupon during the simulation;
sealing, using a ball valve for each coupon holder, the reactor during the removal and replacement of the corrosion coupon; and
obtaining, using a height-adjustable dip tube, a mixed sample of the crude oil phase and the water phase of the reactor at an interphase region of the crude oil phase and the water phase in the reactor.

8. The method of claim 7 , wherein
the reactor further comprises a plurality of reactors each with a respective agitator motor,
controlling the flow of the water phase comprises independently controlling the flow of the water phase in each reactor by controlling the respective agitator motor to drive the desired agitation rate of the agitator of the reactor,
supplying the crude oil to the reactor comprises independently supplying the crude oil to each reactor, and
supplying the water to the reactor comprises independently supplying the water to each reactor to reach the desired proportion of the water to the crude oil supplied to the reactor.

9. The method of claim 7 , wherein
the reactor further comprises a plurality of reactors each having a dedicated biocide inlet and a dedicated water sample outlet,
supplying the biocide to the reactor comprises independently supplying, through the dedicated biocide inlet of each reactor, the biocide to the reactor, and
sampling the water phase of the reactor comprises independently supplying, through the dedicated water sample outlet of each reactor, the water phase of the reactor.

10. The method of claim 7 , wherein
the reactor further comprises a bucket and the agitator comprises a rotor at the bottom of the bucket, the agitation rate being a rotation speed of the rotor, and
controlling the motor further comprises controlling the motor to adjust a height of the rotor above the bottom of the bucket.

11. The method of claim 7 , further comprising supplying, through a nitrogen (N 2 ) gas inlet, N 2 gas to the reactor in order to provide anoxic conditions to the reactor during and after the simulation.

Assignees

• Saudi Arabian Oil Co

Inventors

• Zhu Xiangyang
• Al-Saleh Mazen A
• Ali Qurban

Classifications

• C10G75/02 Primary

  by addition of corrosion inhibitors · CPC title

• B01J19/18

  Stationary reactors having moving elements inside (B01J19/08, B01J19/26 take precedence) · CPC title

• C12M37/06

  Means for testing the completeness of the sterilization (testing for sterility conditions C12Q1/22) · CPC title

• C12M41/38

  of metabolites or enzymes in the cells · CPC title

• B01J2219/00164

  controlling the flow · CPC title