Sacrificial materials to improve chemical vapor infiltration of B4C loaded preforms

Patent metadata

Field	Value
Publication number	US-11906010-B2
Application number	US-202217751051-A
Country	US
Kind code	B2
Filing date	May 23, 2022
Priority date	May 23, 2022
Publication date	Feb 20, 2024
Grant date	Feb 20, 2024

Abstract

A method of forming a composite component is provided. The method includes locating a fibrous preform, providing a slurry, mixing the slurry with sacrificial fibers, injecting the slurry into the fibrous preform, heating the fibrous preform, forming channels in the fibrous preform, and densifying the fibrous preform. The sacrificial fibers are suspended in the fibrous preform along an injection pathway such that heating the sacrificial fibers forms the channels along the injection pathway as the sacrificial fibers are burned away.

First claim

What is claimed is:

1. A method of forming a composite component, comprising:
mixing a slurry with sacrificial fibers, wherein the slurry is a ceramic particulate including an aqueous B 4 C based slurry, and wherein the sacrificial fibers contain at least one micro polyester particle;
injecting the mixed slurry into a fibrous preform, wherein the sacrificial fibers are suspended in the fibrous preform along an injection pathway, wherein the injection pathway is oriented substantially parallel to the Z-axis, and wherein injecting comprises penetrating the fibrous preform;
heating the fibrous preform to form channels in the fibrous preform by burning away the sacrificial fibers suspended in the injection pathway; and
densifying the fibrous preform.

2. The method of claim 1 , wherein heating the fibrous preform includes a chemical vapor infiltration (CVI) process and heating the fibrous preform to a decomposition temperature, wherein forming the channels improves CVI.

3. The method of claim 1 , wherein injecting the slurry with the sacrificial fibers into the fibrous preform includes using a syringe and multiple needle injections to inject the slurry with the sacrificial fibers into the fibrous preform.

4. The method of claim 1 , wherein injecting the slurry with the sacrificial fibers occurs prior to completing the B 4 C slurry infiltration.

5. The method of claim 1 , wherein the sacrificial fibers are a polyethylene or polyester fiber such that, in response to heating to a predetermined temperature during heating the fibrous preform, the sacrificial fibers burn away, wherein the predetermined temperature is 1000° C.

6. The method of claim 1 , wherein the slurry includes a high specific heat particulate that raises the specific heat of the composite component and a liquid carrier.

7. The method of claim 1 , further comprising mixing the B 4 C powder in water with appropriate additives to provide the slurry.

8. The method of claim 1 , wherein the sacrificial fibers make up 5% of the slurry.

9. The method of claim 1 , wherein the sacrificial fibers make up 10% of the slurry.

10. The method of claim 1 , wherein heating the fibrous preform includes a heat treatment such has heating the fibrous preform at temperatures of between 100° F. and 205° F. (38° C. and 96° C.).

11. A method of forming a brake disk, comprising:
mixing a slurry with sacrificial fibers, wherein the slurry is a ceramic particulate including an aqueous B 4 C based slurry, and wherein the sacrificial fibers contain at least one micro polyester particle;
injecting the mixed slurry into a fibrous preform wherein the sacrificial fibers are suspended in the fibrous preform along an injection pathway, wherein the injection pathway is oriented substantially parallel to the Z-axis, and wherein injecting comprises penetrating the fibrous preform; and
densifying the fibrous preform, wherein the sacrificial fibers are burned to form channels.

12. The method of claim 11 , wherein densifying the fibrous preform includes a chemical vapor infiltration (CVI) process, wherein forming the channels improves CVI.

13. The method of claim 11 , wherein injecting the slurry with the sacrificial fibers into the fibrous preform includes using a syringe to inject the slurry with the sacrificial fibers into the fibrous preform.

14. The method of claim 11 , wherein injecting the slurry with the sacrificial fibers occurs prior to completing the B 4 C slurry infiltration.

15. The method of claim 11 , wherein the sacrificial fibers are a polyethylene or polyester fiber such that, when heated to certain temperatures during heating the fibrous preform or heating the fibrous preform to carbon CVI temperatures, the sacrificial fibers burn away.

16. The method of claim 11 , wherein the sacrificial fibers make up 5% of the slurry.

17. The method of claim 11 , wherein the sacrificial fibers make up 10% of the slurry.

18. The method of claim 11 , further comprising heating the fibrous preform, wherein heating the sacrificial fibers forms channels, wherein heating the fibrous preform includes a heat treatment such has heating the fibrous preform at temperatures of between 100° F. and 205° F. (38° C. and 96° C.).

Assignees

• Goodrich Corp

Inventors

• Linck John S
• Perea Thomas

Classifications

• F16D69/02 Primary

  Composition of linings {; Methods of manufacturing} · CPC title

• C04B35/6286

  Carbides · CPC title

• C04B35/62892

  with a coating layer consisting of particles · CPC title

• C04B35/80

  Fibres, filaments, whiskers, platelets, or the like · CPC title

• C04B38/065

  characterised by physical aspects, e.g. shape, size or porosity · CPC title