Composition supply method, composition, supply device, and composition filling method

Patent metadata

Field	Value
Publication number	US-11896918-B2
Application number	US-202117235590-A
Country	US
Kind code	B2
Filing date	Apr 20, 2021
Priority date	Apr 24, 2020
Publication date	Feb 13, 2024
Grant date	Feb 13, 2024

Abstract

The present disclosure provides a method for stably supplying a highly pure n-butylamine gas having a constant composition. The present disclosure is a composition supply method including: a filling step of filling a container with a composition containing n-butylamine in an amount of 99.5% by volume or more and isobutylamine in an amount of 0.001% by volume or more and 0.5% by volume or less; a warming step of warming the container filled with the composition to 50° C. or higher; and a gas supply step of supplying a gas containing n-butylamine and isobutylamine from the warmed container to a predetermined device.

First claim

What is claimed is:

1. A composition supply method comprising:
a filling step of filling a container with a composition containing n-butylamine in an amount of 99.5% by volume or more and isobutylamine in an amount of 0.001% by volume or more and 0.5% by volume or less;
a warming step of warming the container filled with the composition to 50° C. or higher; and
a gas supply step of supplying a gas containing n-butylamine and isobutylamine from the warmed container to a predetermined device.

2. The composition supply method according to claim 1 , further comprising, prior to the gas supply step, a discharging step of discharging 5% by mass or more of the composition in the container in the form of gas from the warmed container.

3. The composition supply method according to claim 1 , further comprising, prior to the gas supply step, a discharging step of discharging 10% by mass or more of the composition in the container in the form of gas from the warmed container.

4. The composition supply method according to claim 1 ,
wherein the warming step involves warming the container to 60° C. to 90° C.

5. The composition supply method according to claim 1 ,
wherein the warming step involves warming the container to 70° C. to 75° C.

6. The composition supply method according to claim 1 ,
wherein the composition is prepared by distillation of a mixture containing n-butylamine and isobutylamine prior to the filling step.

7. The composition supply method according to claim 1 ,
wherein the composition contains n-butylamine in an amount of 99.5% by volume or more and isobutylamine in an amount of 0.001% by volume or more and 0.2% by volume or less.

8. The composition supply method according to claim 1 ,
wherein the composition contains n-butylamine in an amount of 99.9% by volume or more and isobutylamine in an amount of 0.001% by volume or more and 0.05% by volume or less.

9. The composition supply method according to claim 2 ,
wherein the filling step, the heating step, and the discharging step are carried out for multiple containers prior to the gas supply step, and the gas supply step is started for a first container and subsequently started for a second container after 50% by mass or more of the composition in the first container is used.

10. The composition supply method according to claim 9 ,
wherein the amount of the composition in the form of gas supplied from the first container is different from the amount of the composition in the form of gas supplied from the second container in the gas supply step.

11. A composition comprising n-butylamine in an amount of 99.5% by volume or more and isobutylamine in an amount of 0.001% by volume or more and 0.5% by volume or less.

12. The composition according to claim 11 , comprising n-butylamine in an amount of 99.5% by volume or more and isobutylamine in an amount of 0.001% by volume or more and 0.2% by volume or less.

13. The composition according to claim 11 , comprising n-butylamine in an amount of 99.9% by volume or more and isobutylamine in an amount of 0.001% by volume or more and 0.05% by volume or less.

14. A supply device comprising multiple containers filled with a composition comprising n-butylamine in an amount of 99.5% by volume or more and isobutylamine in an amount of 0.001% by volume or more and 0.5% by volume or less, wherein when the containers are warmed to 50° C. or higher, the supply device is configured to supply an n-butylamine composition in the form of gas.

15. A composition filling method comprising:
a filling step of filling a container with a composition containing n-butylamine in an amount of 99.5% by volume or more and isobutylamine in an amount of 0.001% by volume or more and 0.5% by volume or less;
a warming step of warming the container filled with the composition to 50° C. or higher; and
a discharging step of discharging 5% by mass or more of the composition in the container in the form of gas from the warmed container.

Assignees

• Central Glass Co Ltd

Inventors

• Shinmen Masutaka
• Miyake Azusa
• Imachi Masayoshi
• Sezaki Ryusei

Classifications

• H10P95/00

  Generic processes or apparatus for manufacture or treatments not covered by the other groups of this subclass · CPC title

• B01B1/005 Primary

  Evaporation for physical or chemical purposes; Evaporation apparatus therefor, e.g. evaporation of liquids for gas phase reactions · CPC title

• B01J7/00

  Apparatus for generating gases (production of inert gas mixtures B01J19/14; for generating specific gases, see the relevant subclasses, e.g. C01B, C10J {; in "air bags" on vehicles B60R21/26; for starter gas F02C7/26; blasting cartridges for producing gas under pressure F42B3/04}) · CPC title

• B01J19/0013

  Controlling the temperature of the process · CPC title

• B67C3/007

  Applications of control, warning or safety devices in filling machinery (flow-control B67C3/28) · CPC title