Polycrystalline cubic boron nitride and method for manufacturing the same
US-2021087058-A1 · Mar 25, 2021 · US
US11845658B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-11845658-B2 |
| Application number | US-202117795796-A |
| Country | US |
| Kind code | B2 |
| Filing date | Aug 2, 2021 |
| Priority date | Aug 2, 2021 |
| Publication date | Dec 19, 2023 |
| Grant date | Dec 19, 2023 |
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A polycrystalline cubic boron nitride comprising 99.5% by volume or more of cubic boron nitride, wherein the polycrystalline cubic boron nitride has a heat conductivity of 300 W/mK or more, the polycrystalline cubic boron nitride has a carbon content of 100 ppm or more and 1000 ppm or less in terms of mass, the polycrystalline cubic boron nitride comprises a plurality of crystal grains, and the plurality of crystal grains have a median diameter d50 of an equivalent circle diameter of 0.9 μm or more and 10 μm or less.
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The invention claimed is: 1. A polycrystalline cubic boron nitride comprising 99.5% by volume or more of cubic boron nitride, wherein the polycrystalline cubic boron nitride has a heat conductivity of 300 W/mK or more, the polycrystalline cubic boron nitride has a carbon content of 100 ppm or more and 1000 ppm or less in terms of mass, the polycrystalline cubic boron nitride comprises a plurality of crystal grains, and the plurality of crystal grains have a median diameter d50 of an equivalent circle diameter of 0.9 μm or more and 10 μm or less. 2. The polycrystalline cubic boron nitride according to claim 1 , wherein the polycrystalline cubic boron nitride has a dislocation density of 4.5×10 15 /m 2 or less. 3. The polycrystalline cubic boron nitride according to claim 1 , wherein the polycrystalline cubic boron nitride has an oxygen content of 700 ppm or less in terms of mass. 4. The polycrystalline cubic boron nitride according to claim 1 , wherein the polycrystalline cubic boron nitride has a total content of an alkali metal element and an alkaline earth metal element of 10 ppm or less in terms of mass. 5. The polycrystalline cubic boron nitride according to claim 1 , wherein the polycrystalline cubic boron nitride has a heat conductivity of 500 W/mK or more. 6. The polycrystalline cubic boron nitride according to claim 1 , wherein, in an X-ray diffraction spectrum of the polycrystalline cubic boron nitride, a ratio of an X-ray diffraction intensity I (220) of the (220) plane to an X-ray diffraction intensity I (111) of the (111) plane, I (220)/I (111), is 0.10 or more and 0.30 or less. 7. The polycrystalline cubic boron nitride according to claim 2 , wherein the dislocation density is calculated by using a modified Williamson-Hall method and a modified Warren-Averbach method. 8. The polycrystalline cubic boron nitride according to claim 2 , wherein the dislocation density is measured using synchrotron radiation as an X-ray source. 9. A heatsink using the polycrystalline cubic boron nitride according to claim 1 .
Ceramics or glasses (H10W40/254, H10W40/257, H10W40/255, H10W40/251, H10W40/253 take precedence) · CPC title
characterised by the applied pressure or type of atmosphere, e.g. in vacuum, hydrogen or a specific oxygen pressure · CPC title
Pressure sintering · CPC title
characterised by the treatment temperature · CPC title
Multi-step sintering · CPC title
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