Wet granulation for manufacture of thermal insulation material

Patent metadata

Field	Value
Publication number	US-11740009-B2
Application number	US-202117545026-A
Country	US
Kind code	B2
Filing date	Dec 8, 2021
Priority date	Apr 10, 2018
Publication date	Aug 29, 2023
Grant date	Aug 29, 2023

Abstract

An appliance cabinet includes a structural envelope having an exterior surface and an interior surface that defines an insulating cavity, wherein the insulating cavity defines an at least partial vacuum. A plurality of silica-based agglomerates are disposed within the insulating cavity, wherein each agglomerate of the plurality of silica-based agglomerates includes silica-based powder insulation material that is water-densified and is at least substantially free of a material binder. A secondary insulation material is disposed within interstitial spaces defined between the plurality of silica-based agglomerates, wherein the plurality of silica-based agglomerates defines an interior structure that resists inward compressive forces exerted as a result of the at least partial vacuum defined within the insulating cavity.

First claim

What is claimed is:

1. A method for forming a granulated insulation material for use in an insulated structure of an appliance, the method comprising steps of:
combining a powder insulation material and a temporary binder to define a partially wetted insulation material;
mixing the partially wetted insulation material to define wet insulation granules;
evaporating the temporary binder from the wet insulation granules to define dry insulation agglomerates, wherein the wet insulation granules and the dry insulation agglomerates are substantially the same size.

2. The method of claim 1 , wherein the partially wetted insulation material contains an amount of temporary binder to define clumps of the powder insulation material.

3. The method of claim 1 , wherein the temporary binder is water.

4. The method of claim 1 , wherein the powder insulation material includes at least one of a silica-based material, pearlite, glass microspheres and an opacifier.

5. The method of claim 1 , wherein the step of mixing the partially wetted insulation material includes mixing the partially wetted insulation material according to various mixing parameters, wherein the mixing parameters at least partially determine a granule size of the dry insulation agglomerates.

6. The method of claim 5 , wherein the granule size of the dry insulation agglomerates is further determined by an amount of temporary binder that is combined with the powder insulation material.

7. The method of claim 1 , further comprising a step of:
combining the dry insulation agglomerates with a secondary insulation material, wherein the secondary insulation material substantially occupies interstitial spaces defined between the dry insulation agglomerates.

8. The method of claim 1 , wherein the step of evaporating the temporary binder from the wet insulation granules is performed by heating the wet insulation granules.

9. The method of claim 8 , wherein the step of evaporating the temporary binder from the wet insulation granules is performed free of material drying agents.

10. A method for forming an insulated structure for use in an appliance, the method comprising steps of:
combining a powder insulation material and temporary binder to define a partially wetted insulation material;
mixing the partially wetted insulation material to define wetted insulation granules;
evaporating the temporary binder from the wetted insulation granules to define dry insulation agglomerates;
disposing the dry insulation agglomerates within a cavity defined within a structural envelope;
expressing gas from the cavity to define an at least partial vacuum within the cavity.

11. The method of claim 10 , wherein the dry insulation agglomerates define an interior structure that resists an inward compressive force exerted on the exterior of the structural envelope as a result of the at least partial vacuum defined within the cavity.

12. The method of claim 10 , wherein an amount of powder insulation material by weight in the partially wetted insulation material is greater than an amount of the temporary binder by weight in the partially wetted insulation material.

13. The method of claim 10 , wherein the powder insulation material includes at least one of a silica-based material, perlite, glass spheres, and an opacifier.

14. The method of claim 13 , wherein the dry insulation agglomerates define composite aggregates.

15. The method of claim 10 , wherein the step of disposing dry insulation agglomerates within the cavity includes disposing a secondary insulation material into the cavity, wherein the secondary insulation material substantially occupies interstitial spaces defined between the dry insulation agglomerates.

16. The method of claim 10 , wherein the step of evaporating temporary binder from the wetted insulation granules is performed at least by heating the wetted insulation granules.

17. The method of claim 10 , wherein the wetted insulation granules and the dry insulation agglomerates are substantially the same size.

18. An insulating structure for an appliance, the insulating structure comprising:
a structural envelope having an exterior surface and an interior surface that defines an insulating cavity, wherein the insulating cavity defines an at least partial vacuum;
dried silica-based agglomerates that are disposed within the insulating cavity, wherein each agglomerate of the dried silica-based agglomerates includes a silica-based powder insulation material that is water-densified and is at least substantially free of a material binder; and
a secondary insulation material that is disposed within interstitial spaces defined between the dried silica-based agglomerates, wherein the dried silica-based agglomerates define an interior structure that resists inward compressive forces exerted as a result of the at least partial vacuum defined within the insulating cavity.

19. The insulating structure of claim 18 , wherein each agglomerate of the dried silica-based agglomerates is in direct engagement with at least one adjacent agglomerate of the dried silica-based agglomerates.

20. The insulating structure of claim 18 , wherein the secondary insulation material is at least one of a silica-based material, insulating gas, perlite, glass microspheres, and an opacifier.

Assignees

• Whirlpool Co

Inventors

• Nigam Ashish
• Roy Shayta

Classifications

• F25D23/065 Primary

  Details · CPC title

• C04B14/18

  Perlite · CPC title

• C04B14/24

  porous, e.g. foamed glass · CPC title

• F16L59/028

  Compositions for or methods of fixing a thermally insulating material · CPC title

• C04B2103/56

  Opacifiers · CPC title