Wet granulation for manufacture of thermal insulation material

Patent metadata

Field	Value
Publication number	US-11226153-B2
Application number	US-201817042300-A
Country	US
Kind code	B2
Filing date	Apr 10, 2018
Priority date	Apr 10, 2018
Publication date	Jan 18, 2022
Grant date	Jan 18, 2022

Abstract

An appliance cabinet includes a structural envelope having an exterior surface and an interior surface that defines an insulating cavity, wherein the insulating cavity defines an at least partial vacuum. A plurality of silica-based agglomerates are disposed within the insulating cavity, wherein each agglomerate of the plurality of silica-based agglomerates includes silica-based powder insulation material that is water-densified and is at least substantially free of a material binder. A secondary insulation material is disposed within interstitial spaces defined between the plurality of silica-based agglomerates, wherein the plurality of silica-based agglomerates defines an interior structure that resists inward compressive forces exerted as a result of the at least partial vacuum defined within the insulating cavity.

First claim

What is claimed is:

1. A method for forming a granulated insulation material for use in an appliance cabinet, the method comprising steps of:
combining a powder insulation material and a binder to define an at least partially wetted insulation material;
mixing the at least partially wetted insulation material to define a plurality of wet insulation granules;
evaporating at least a portion of the binder from the plurality of wet insulation granules to define a plurality of dry insulation agglomerates, wherein the plurality of wet insulation granules and the plurality of dry insulation agglomerates are substantially the same size.

2. The method of claim 1 , wherein the binder is water.

3. The method of claim 2 , wherein the step of evaporating the water from the plurality of wet insulation granules is performed by heating the plurality of wet insulation granules.

4. The method of claim 3 , wherein the step of evaporating the water from the plurality of wet insulation granules is performed free of material drying agents.

5. The method of claim 1 , wherein the powder insulation material includes at least one of a silica-based powder insulation material, a plurality of perlite microspheres, a plurality of hollow glass microspheres and an opacifier.

6. The method of claim 1 , wherein the step of mixing the at least partially wetted insulation material includes mixing the at least partially wetted insulation material according to various mixing parameters, wherein the mixing parameters at least partially determine a granule size of the plurality of dry insulation agglomerates.

7. The method of claim 6 , wherein the granule size of the plurality of dry insulation agglomerates is further determined by an amount of water that is combined with the powder insulation material.

8. The method of claim 1 , further comprising a step of:
combining the plurality of dry insulation agglomerates with a secondary insulation material, wherein the secondary insulation material substantially occupies interstitial spaces defined between the plurality of dry insulation agglomerates.

9. A method for forming a vacuum insulated structure for use in an appliance, the method comprising steps of:
combining a silica-based powder insulation material and water to define an at least partially wetted insulation material;
mixing the at least partially wetted insulation material to define a plurality of wet insulation granules;
evaporating water from the wet insulation granules to define a plurality of dry insulation agglomerates;
disposing the plurality of dry insulation agglomerates within an insulating cavity defined within a structural envelope;
expressing air from the insulating cavity to define an at least partial vacuum within the insulating cavity.

10. The method of claim 9 , wherein the plurality of dry insulation agglomerates defines an interior structure that resists an inward compressive force exerted on the exterior of the structural envelope as a result of the at least partial vacuum defined within the insulating cavity.

11. The method of claim 9 , wherein an amount of water by weight in the at least partially wetted insulation material is less than an amount of the silica-based powder insulation material by weight in the at least partially wetted insulation material.

12. The method of claim 9 , wherein the silica-based powder insulation material includes at least one of a plurality of perlite spheres, a plurality of hollow microspheres, and an opacifier, and wherein the plurality of dry insulation agglomerates define composite aggregates.

13. The method of claim 9 , wherein the step of disposing the plurality of dry insulation agglomerates within the insulating cavity includes disposing a secondary insulation material into the insulating cavity, wherein the secondary insulation material substantially occupies interstitial spaces defined between the plurality of dry insulation agglomerates.

14. The method of claim 9 , wherein the step of mixing the at least partially wetted insulation material includes mixing the at least partially wetted insulation material according to a set of mixing parameters, wherein the mixing parameters at least partially determine a granule size of the plurality of dry insulation agglomerates, and wherein the granule size of the plurality of dry insulation agglomerates is further determined by an amount of the water that is combined with the silica-based powder insulation material.

15. The method of claim 9 , wherein the step of evaporating water from the wet insulation granules is performed by heating the wet insulation granules, and wherein the step of evaporating water from the wet insulation granules is performed free of material drying agents.

16. The method of claim 9 , wherein the plurality of wet insulation granules and the plurality of dry insulation agglomerates are substantially the same size.

17. An appliance cabinet comprising:
a structural envelope having an exterior surface and an interior surface that defines an insulating cavity, wherein the insulating cavity defines an at least partial vacuum;
a plurality of silica-based agglomerates disposed within the insulating cavity, wherein each agglomerate of the plurality of silica-based agglomerates includes a silica-based powder insulation material that is water-densified and is at least substantially free of a material binder; and
a secondary insulation material that is disposed within interstitial spaces defined between the plurality of silica-based agglomerates, wherein the plurality of silica-based agglomerates defines an interior structure that resists inward compressive forces exerted as a result of the at least partial vacuum defined within the insulating cavity.

18. The appliance cabinet of claim 17 , wherein each agglomerate of the plurality of silica-based agglomerates is in direct engagement with at least one adjacent agglomerate of the plurality of silica-based agglomerates, and wherein a portion of the plurality of silica-based agglomerates are in direct engagement with the interior surface of the structural envelope.

19. The appliance cabinet of claim 17 , wherein at least a portion of the agglomerates of the plurality of silica-based agglomerates defines a silica-based aggregate having at least one of perlite spheres, hollow microspheres and an opacifier.

20. The appliance cabinet of claim 17 , wherein the material binder used in formation of the plurality of silica-based agglomerates is water, and wherein the secondary insulation material is at least one of a silica-based material, insulating gas, perlite spheres, glass microspheres, and an opacifier.

Assignees

• Whirlpool Co

Inventors

• Nigam Ashish
• Roy Shayta

Classifications

• C04B2111/28

  Fire resistance, i.e. materials resistant to accidental fires or high temperatures · CPC title

• F16L59/028

  Compositions for or methods of fixing a thermally insulating material · CPC title

• C04B30/00 Primary

  Compositions for artificial stone, not containing binders · CPC title

• C04B2111/00965

  for household applications, e.g. use of materials as cooking ware · CPC title

• C04B14/18

  Perlite · CPC title