Method and systems for determining dielectric breakdown voltages of fluid samples using dielectric fluid testers

Patent metadata

Field	Value
Publication number	US-11624722-B2
Application number	US-202016858423-A
Country	US
Kind code	B2
Filing date	Apr 24, 2020
Priority date	Apr 24, 2020
Publication date	Apr 11, 2023
Grant date	Apr 11, 2023

Abstract

Described herein are dielectric fluid testers for determining dielectric breakdown of fluid samples, systems comprising such testers, and methods using thereof. A dielectric fluid tester comprises a container and two electrodes. The test heads of these electrodes protrude inside the container and face each other, forming a gap. In some examples, one or both electrodes are movable for adjusting the gap and/or the volume inside the container available for a fluid sample. For example, the container includes two internal seals, one of which has a fixed position and is slidably coupled to a respective electrode. The other seal is slidably coupled to the container and moves together with the corresponding electrode. The container comprises an access port, providing a fluid communication between the fluid sample and an external pressure-controlling source. In some examples, the access port is used to deliver and remove the fluid sample from the container.

First claim

What is claimed is:

1. A dielectric fluid tester for determining a dielectric breakdown voltage of a fluid sample, the dielectric fluid tester comprising:
a container, for containing the fluid sample, the container comprising an insulating cap, a housing, and an access port, which protrudes from outside of the container into the container through the insulating cap and is configured to connect to a pressure-controlling source and fluidically couple the pressure-controlling source to the fluid sample while the fluid sample is inside the container;
a first electrode, comprising a first test head and protruding from outside the container into the container through the insulating cap; and
a second electrode, comprising a second test head and protruding from outside the container into the container, wherein the first test head and the second test head face each other and are separated by a gap, forming a test zone within the container between the first test head and the second test head, and wherein the first test head and the second test head are configured to determine the dielectric voltage breakdown of the fluid sample.

2. The dielectric fluid tester of claim 1 , wherein at least one of the first electrode or the second electrode is movably coupled to the container such that the gap between the first test head and the second test head is adjustable.

3. The dielectric fluid tester of claim 1 , wherein both the first electrode and the second electrode are movably coupled to the container such that the gap between the first test head and the second test head is adjustable by either one of the first electrode or the second electrode.

4. The dielectric fluid tester of claim 3 , further comprising a first seal, wherein:
the first seal is coupled to the first electrode;
the first seal is positioned inside the container and slidably sealed against the housing; and
the first seal at least partially defines a volume inside the container available for the fluid sample.

5. The dielectric fluid tester of claim 4 , further comprising a second seal, wherein:
the second seal is slidably sealed around the second electrode;
the second seal is positioned inside the container and coupled to the housing; and
the second seal, together with the first seal and the housing, defines the volume inside the container available for the fluid sample.

6. The dielectric fluid tester of claim 5 , wherein the access port protrudes through the second seal.

7. The dielectric fluid tester of claim 3 , wherein:
the container further comprises an additional insulating cap; and
the first electrode is movably coupled to the insulating cap.

8. The dielectric fluid tester of claim 1 , wherein the first electrode is collinear to the second electrode.

9. The dielectric fluid tester of claim 1 , wherein the access port comprises an interior opening, disposed proximate to an interior wall of the housing.

10. The dielectric fluid tester of claim 1 , further comprising a ground plane, positioned parallel to an exterior wall of the housing.

11. The dielectric fluid tester of claim 1 , wherein a volume inside the container available for the fluid sample is less than 100 milliliters.

12. A method for detecting a dielectric breakdown voltage of a fluid sample using a dielectric fluid tester, the method comprising:
delivering the fluid sample into a container of the dielectric fluid tester, the container comprising an insulating cap, a housing, and an access port, which protrudes from outside of the container into the container through the insulating cap and is configured to connect to a pressure-controlling source and fluidically couple the pressure-controlling source to the fluid sample while the fluid sample is inside the container the dielectric fluid tester comprising a first electrode, comprising a first test head, and protruding from outside the container into the container through the insulating cap, and a second electrode, comprising a second test head and protruding from outside the container into the container through the insulating cap;
applying a voltage between the first electrode and the second electrode; and
determining the dielectric breakdown voltage by at least one of:
adjusting a gap between the first test head and the second test head,
adjusting the voltage between the first electrode and the second electrode,
adjusting temperature of the fluid sample inside the container, or
adjusting pressure inside the container.

13. The method of claim 12 , wherein determining the dielectric breakdown voltage comprises simultaneously performing two or more of:
adjusting the gap between the first test head and the second test head,
adjusting the voltage between the first electrode and the second electrode,
adjusting temperature of the fluid sample inside the container, or
adjusting pressure inside the container.

14. The method of claim 12 , further comprising, prior to applying the voltage between the first electrode and the second electrode, reducing the pressure inside the container to degas the fluid sample, wherein the fluid sample is liquid.

15. The method of claim 12 , wherein the fluid sample has a volume of less than 100 milliliters.

16. The method of claim 12 , further comprising, prior to delivering the fluid sample into the container, adjusting a volume inside the container available for the fluid sample.

17. The method of claim 16 , wherein adjusting the volume inside the container available for the fluid sample comprises moving a first seal, slidably sealed against the housing, inside the container.

18. The method of claim 17 , wherein the first seal is coupled to the first electrode, and wherein moving the first seal comprises moving the first electrode relative to the insulating cap.

19. The method of claim 12 , wherein adjusting the gap between the first test head and the second test head comprises rotating at least one of the first electrode or the second electrode relative to the container.

20. A system for determining a dielectric breakdown voltage of a fluid sample, the system comprising:
a dielectric fluid tester, comprising a container, a first electrode, comprising a first test head and protruding from outside of the container into the container, and a second electrode, comprising a second test head and protruding from outside of the container into the container, wherein the first test head and the second test head face each other and are separated by a gap, and wherein the first test head and the second test head are configured to determine the dielectric voltage breakdown of the fluid sample;
a power supply, electrically coupled to each of the first electrode and the second electrode and configured to control a voltage applied between the first electrode and the second electrode; and
a pressure-controlling source, fluidically coupled to an interior of the container and configured to control pressure inside the container.

Assignees

• Boeing Co

Inventors

• King Garnel
• Coad Dennis Lynn

Classifications

• G01N27/06

  of a liquid (involving electrolysis G01N27/26) · CPC title

• G01N27/226

  Construction of measuring vessels; Electrodes therefor · CPC title

• G01N27/221 Primary

  by investigating the dielectric properties (using microwaves G01N22/00; measuring loss factors or dielectric constants per se G01R27/26) · CPC title

• G01N27/92 Primary

  by investigating breakdown voltage (G01N27/60, G01N27/62 take precedence) · CPC title