Electrofracturing test system and method of determining material characteristics of electrofractured material samples

Patent metadata

Field	Value
Publication number	US-9719908-B1
Application number	US-201514625287-A
Country	US
Kind code	B1
Filing date	Feb 18, 2015
Priority date	Feb 18, 2014
Publication date	Aug 1, 2017
Grant date	Aug 1, 2017

Abstract

A device for electrofracturing a material sample and analyzing the material sample is disclosed. The device simulates an in situ electrofracturing environment so as to obtain electrofractured material characteristics representative of field applications while allowing permeability testing of the fractured sample under in situ conditions.

First claim

What is claimed is:

1. A device for electrofracturing a material sample, comprising:
a pressure vessel comprising an internal cavity;
a pressurized fluid supply system fluidly coupled to the internal cavity;
a material sample disposed within the internal cavity;
a voltage source electrically coupled to the material sample to provide a voltage pulse across the material sample; and
a gas measurement system fluidly coupled to the material sample;
wherein the voltage source provides a pulse of between 150 kv and 1 MV.

2. The device of claim 1 , wherein the pressurized fluid system is capable of pressurizing the internal cavity up to 20,000 psi.

3. The device of claim 1 , wherein the voltage source provides a pulse of 1 MV.

4. The device of claim 1 , wherein the voltage source provides a pulse of 200 kV.

5. The device of claim 1 , wherein the voltage source is capable of providing a pulse having a pulse width of between 100 picoseconds (ps) and 1 day.

6. The device of claim 1 , wherein the gas measurement system comprises a mass spectrometer.

7. The device of claim 1 , wherein the gas measurement system comprises a flow meter.

8. The device plate of claim 1 , wherein the material sample is shale.

9. The device of claim 1 , wherein the material sample is disposed with a test assembly disposed within the internal cavity, the test assembly comprising:
a first nonconductive end cap on a first surface of the material sample;
a second nonconductive end cap on a second surface of the material sample opposite the first surface;
a first and second conductors passing through the first and second nonconductive end caps, respectively, and contacting the material sample; and
a jacketing material sealing the material sample between the first and second nonconductive end caps.

10. A method of electrofracturing a material sample, comprising:
providing a material sample;
subjecting the material sample to an external pressure;
subjecting the material sample to a voltage potential;
flowing a test fluid across the material sample; and
measuring the amount of test gas that flows from the material sample;
wherein the voltage potential is between 150 kv and 1 MV.

11. The method of claim 10 , further comprising:
determining the permeability of the material sample.

12. The method of claim 10 , wherein the external pressure is between 2,000 psi and 20,000 psi.

13. The method of claim 10 , wherein the voltage potential is capable of fracturing the material sample.

14. The method of claim 10 , wherein the voltage potential is pulsed two or more times and the time between pulses is 100 μs to 1 day.

15. The method of claim 10 , wherein the voltage potential has a pulse width of between 100 picoseconds (ps) and 1 day.

Assignees

• Sandia Corp

Inventors

• Bauer Stephen J
• Glover Steven F
• Pfeifle Tom
• Su Jiann-Cherng
• Williamson Kenneth Martin
• Broome Scott Thomas
• Gardner William Payton
• Pena Gary

Classifications

• G01N1/28

  Preparing specimens for investigation {including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q}(mounting specimens on microscopic slides G02B21/34; means for supporting the objects or the materials to be analysed in electron microscopes H01J37/20 {; laboratory gas handling apparatus B01L5/00}) · CPC title

• G01N15/082 Primary

  Investigating permeability by forcing a fluid through a sample · CPC title

• G01N2001/1062

  Sampling under constant temperature, pressure, or the like · CPC title

• G01N2203/0232

  High pressure · CPC title

• G01N2203/006

  Crack, flaws, fracture or rupture · CPC title