Apparatus and method for isolation and/or preparation of particles

Patent metadata

Field	Value
Publication number	US-11549871-B2
Application number	US-201816500973-A
Country	US
Kind code	B2
Filing date	Apr 5, 2018
Priority date	Apr 7, 2017
Publication date	Jan 10, 2023
Grant date	Jan 10, 2023

Abstract

An apparatus and a method for isolating and/or preparing particles are provided.

First claim

The invention claimed is:

1. Method for isolation and/or preparation of particles comprising the following steps:
a) Providing a feed material comprising particles to be isolated and/or prepared in a chamber provided with a filter having a filter surface, optionally introducing liquid before, during or after the feed material is placed in the chamber;
b) If the material in the chamber from step a) contains liquid, the feed material is filtered by draining out said liquid through an outlet for filtrate leaving retentate on the filter surface;
c) Directing more than one gas jet towards the feed material from step a) or the retentate from step b) loosening the material from the retentate side of the filter surface;
d) Removing the loosened material through an outlet for loosened material, wherein said more than one gas jet is provided from more than one gas inlet placed on the retentate side of the filter surface; wherein at least one gas jet contributes to create a vortex of gas and particles inside the chamber by directing a flow of gas sufficiently off-centre of the chamber; and wherein the loosened material is suspended in the gas from said gas jet and carried from the filter surface to the outlet for loosened material by the gas of said gas jet.

2. Method according to claim 1 , wherein
c) at least one or more gas jet is provided on the retenate side of the filter which is not contributing to creating a vortex inside the chamber.

3. Method according to claim 2 , wherein at least one gas jet is directed towards retentate side of the filter surface in an angle pointing towards the filter surface or pointing towards the centre of the chamber in an angle approximately parallel to the filter surface.

4. Method according to claim 1 , wherein
a) liquid is introduced before, during or after provision of the feed material and at least one gas jet provides agitation of the liquid suspension of material to be filtered.

5. Method according to claim 1 , wherein
c) the flow (F) of gas from at least one gas jet is added in a direction tangential to a circle having a radius r f between 0.3·r min and 0.9·r min .

6. An apparatus comprising a chamber ( 1 ), the chamber ( 1 ) comprises an inlet ( 2 ) for feed material to be isolated and/or prepared in the form of a slurry or a particular material, optionally an inlet for liquid, a filter having a filter surface ( 3 ) on which surface material ( 8 ) is positioned at least during use of the apparatus, an outlet ( 4 ) for filtrate, an outlet ( 5 ) for prepared particles comprising an opening ( 5 a ) to a passage through a wall of the chamber ( 1 ), more than one gas inlet ( 6 , 9 ) placed on the retentate side of the filter through which gas jets are provided, characterized in that the more than one inlet ( 6 , 9 ) is configured to direct a flow (F) of gas in form of a gas jet towards the material ( 8 ) on the filter surface ( 3 ) thereby loosening the material from the filter surface; wherein at least one gas inlet ( 6 ) is configured to direct a flow (F) of gas in form of a gas jet approximately parallel to the filter surface ( 3 ) within distance h i from the filter surface ( 3 ) and to direct the flow (F) of gas sufficiently off-centre (C) of the chamber, where the centre (C) is defined as a central axis of the chamber ( 1 ), to create a vortex inside the chamber ( 1 ) when the material ( 8 ) has been suspended.

7. Apparatus according to the claim 6 , wherein the chamber ( 1 ) is formed like a cylinder or like a truncated cone, or the chamber ( 1 ) has an oval cross section or the cross section of the chamber ( 1 ) has no corners with an angle of 90° or below.

8. Apparatus according to the claim 6 , wherein the inlet ( 6 ) for drying gas is configured to direct a gas jet tangentially to a circle having a radius r f smaller than the smallest distance r min between the central axis C and an inner wall of the chamber ( 1 ) and larger than 0.

9. Apparatus according to the claim 6 , wherein the inlet ( 6 ) for gas is configured to direct a gas jet tangentially to a circle having a radius r f between 0.3·r min and 0.9·r min .

10. Apparatus according to the claim 6 , wherein the chamber ( 1 ) comprises more than one opening ( 5 a ) for dried product ( 5 a ) positioned at varying distance from the filter surface ( 3 ) and/or the chamber ( 1 ) comprises one or more openings ( 5 a ) which can be moved axially thereby varying the distance between the opening of the outlet ( 5 ) and the filter surface ( 3 ).

11. Apparatus according to the claim 6 , wherein the chamber ( 1 ) comprises more than one opening ( 5 a ) for dried product ( 5 a ) positioned at varying distance from the central axis C and/or the chamber ( 1 ) comprises one or more openings ( 5 a ) which can be moved radially thereby varying the distance between the opening of the outlet ( 5 ) and the central axis C of the chamber ( 1 ).

12. Apparatus according to the claim 6 , which apparatus comprises an inlet ( 2 ) for liquid.

13. Apparatus according to the claim 6 , wherein the chamber ( 1 ) comprises more than one tangential inlet ( 6 ) for gas.

14. Apparatus according to the claim 6 , wherein the apparatus is further provided with an inlet ( 9 ) for gas jet directed to the centre C of the chamber ( 1 ).

15. Apparatus according to the claim 6 , wherein the gas inlets ( 6 , 9 ) are placed at the end of the chamber ( 1 ) closest to the retentate side of the filter surface ( 3 ), optionally through the wall of the chamber ( 1 ) at a height h j above the filter surface ( 3 ).

16. Apparatus according to the claim 6 , wherein an outlet ( 7 ) for gas is placed at the center or off-center of the chamber with an opening above the filter surface ( 3 ).

17. Apparatus for isolation and/or preparation of a suspended material according to the claim 6 , which apparatus comprises more than one chamber ( 1 ).

18. Use of an apparatus according to the claim 6 for controlling drying and/or granulometry of loosened particulate material in a single chamber ( 1 ) or in a number of parallel chambers in order to obtain a target-degree of drying and a target-particle size distribution.

19. Use of an apparatus according to the claim 6 for controlling drying and/or granulometry of a loosened particulate material in a chamber ( 1 ) or in a number of parallel chambers by providing at least one gas jets ( 6 ) causing a vortex and then controlling temperature of the gas jet, retention time of the loosened particulate material in the chamber ( 1 ), velocity of the gas flow and amount of inflowing gas in such a way that target degree of drying and a target-particle size distribution of the loosened particulate material is obtained.

Assignees

• H Lundbeck As

Inventors

• Sogaard Steen
• Skovby Tommy Carsten Lund
• Mortensen Asmus Ringlebjerg
• Gad Jens Andersen

Classifications

• G01N1/2211 Primary

  with cyclones · CPC title

• G01N1/4077 Primary

  by other techniques involving separation of suspended solids · CPC title

• G01N2015/0288

  Sorting the particles · CPC title

• G01N15/0272

  with screening; with classification by filtering (B01D takes precedence) · CPC title

• B01D29/03

  self-supporting · CPC title