Preparing method of monomolecular nano-thin film

Patent metadata

Field	Value
Publication number	US-11534795-B2
Application number	US-201916656734-A
Country	US
Kind code	B2
Filing date	Oct 18, 2019
Priority date	Oct 23, 2018
Publication date	Dec 27, 2022
Grant date	Dec 27, 2022

Abstract

The present disclosure relates to a method of preparing a monomolecular nano-thin film, including: coating, on a substrate, a dispersion solution containing a compound represented by the following Chemical Formula 1; and performing annealing to the coated substrate:in the above Chemical Formula 1,X and Y are each independently nitrogen, carbon, sulfur, or oxygen,R1 and R2 are each independently hydrogen, oxygen, a hydroxy group (—OH), or a linear or branched C1 to C10 alkyl group.

First claim

What is claimed is:

1. A method of preparing a monomolecular nano-thin film, comprising:
coating, on a surface of a substrate, a dispersion solution containing a compound represented by the following Chemical Formula 2; and
forming the monomolecular nano-thin film on the surface of the substrate by annealing the coated substrate:

wherein in the above Chemical Formula 2,
Y is nitrogen or carbon,
R 1 and R 2 are each independently hydrogen, oxygen, a hydroxy group (—OH), or a linear or branched C 1 to C 10 alkyl group.

2. The method of preparing a monomolecular nano-thin film of claim 1 ,
wherein the dispersion solution further contains a nanomaterial.

3. The method of preparing a monomolecular nano-thin film of claim 1 ,
wherein the nanomaterial is embedded on the substrate by the compound represented by Chemical Formula 2.

4. The method of preparing a monomolecular nano-thin film of claim 2 ,
wherein the nanomaterial includes a material having a shape selected from the group consisting of nanowire, nanoparticle, nanotube, nanofiber, nanorod, and combinations thereof.

5. The method of preparing a monomolecular nano-thin film of claim 2 ,
wherein the nanomaterial contains a metal selected from the group consisting of Ag, Au, Pt, Al, Cu, Cr, V, Mg, Ti, Sn, Pb, Pd, W, Ni, and combinations thereof.

6. The method of preparing a monomolecular nano-thin film of claim 2 ,
wherein the nanomaterial includes a silver (Ag) nanowire.

7. The method of preparing a monomolecular nano-thin film of claim 1 ,
wherein the annealing is performed at from 20° C. to 350° C.

8. The method of preparing a monomolecular nano-thin film of claim 1 ,
wherein the dispersion solution contains a solvent selected from the group consisting of isopropyl alcohol, water, ethylene glycol, diethylene glycol, polyethylene glycol, glycerol, propyl glycol, pentaerythritol, vinyl alcohol, polyvinyl alcohol, and combinations thereof.

9. The method of preparing a monomolecular nano-thin film of claim 1 ,
wherein the substrate includes a substrate selected from the group consisting of a metal substrate, a plastic substrate, a glass substrate, a silicon substrate, a silicon oxide substrate, a Teflon film substrate, a sapphire substrate, a nitride substrate, and combinations thereof.

10. The method of preparing a monomolecular nano-thin film of claim 9 ,
wherein the metal substrate contains a metal element selected from the group consisting of Cu, Al, Fe, Ni, Au, Pt, Ag, and combinations thereof.

11. The method of preparing a monomolecular nano-thin film of claim 9 ,
wherein the plastic substrate includes a plastic substrate selected from the group consisting of polyethylene terephthalate (PET), poly(ether sulfone) (PES), polyethylene naphthalate (PEN), polycarbonate (PC), polystyrene (PS), polyimide (PI), polyethylene (PE), and combinations thereof.

12. The method of preparing a monomolecular nano-thin film of claim 1 ,
wherein the coating is one selected from the group consisting of bar coating, spin coating, nozzle printing, spray coating, slot die coating, gravure printing, ink jet printing, screen printing, electrohydrodynamic jet printing, electrospray, and combinations thereof.

Assignees

• Research & Business Found Sungkyunkwan Univ

Inventors

• Lim Byungkwon
• Bok Shingyu

Classifications

• H10P14/6342

  Liquid deposition, e.g. spin-coating, sol-gel techniques or spray coating · CPC title

• H10P14/65

  characterised by treatments performed before or after the formation of the materials · CPC title

• B05D2202/25

  based on Al · CPC title

• C09D7/70

  characterised by shape, e.g. fibres, flakes or microspheres · CPC title

• C08K7/06

  Elements · CPC title