Sample holding device for X-ray analysis

Patent metadata

Field	Value
Publication number	US-11525790-B2
Application number	US-202016992670-A
Country	US
Kind code	B2
Filing date	Aug 13, 2020
Priority date	Aug 16, 2019
Publication date	Dec 13, 2022
Grant date	Dec 13, 2022

Abstract

A sample holder (10) filled with a sample is held in a base member (20), and an airtight member (30) is mounted on the base member (20) so as to cover the surroundings of the sample holder (10), thereby forming a sample holding structure in a closed space. The airtight member (30) includes a fitting portion (35) which is configured to be fitted and mounted in a mounting portion (21).

First claim

The invention claimed is:

1. A sample holding device for X-ray analysis comprising:
a sample holder having a sample filling portion for filling a sample;
a base member for holding the sample holder; and
an airtight member configured to be freely detachably mounted on the base member,
wherein the base member has a mounting portion for mounting the airtight member thereon, the airtight member has a fitting portion configured to be fitted and mounted in the mounting portion,
a locking mechanism is provided to the mounting portion and the fitting portion so as to prevent the airtight member from coming off the base member through engagement in a step of fitting the fitting portion into the mounting portion,
the airtight member includes a main body portion having a hollow portion therein, and the fitting portion formed so as to protrude from a lower surface of the main body portion,
a lower end surface of the fitting portion is opened and communicates with the hollow portion in the main body portion,
an X-ray transmission window is formed by cutting out the main body portion, and an X-ray window material is formed around the X-ray transmission window so as to cover the X-ray transmission window, and
an operating portion for enabling an operator to perform a fitting operation while gripping the operating portion is formed in a surface region of the main body portion where the X-ray transmission window is not formed.

2. The sample holding device for X-ray analysis according to claim 1 , wherein the X-ray window material is formed of any one of metal, artificial mineral and polymer.

3. The sample holding device for X-ray analysis according to claim 1 , wherein the base member includes a holding groove configured to freely detachably hold the sample holder, and the sample holder includes a fitting convex portion configured to be fitted and held in the holding groove,
wherein the sample filling portion of the sample holder is formed by a recessed groove, and an opening surface of the recessed groove is formed in a rectangular shape, and
wherein the sample holding device for X-ray analysis further comprises a configuration in which a long side or short side of a rectangular shape on the opening surface of the recessed groove is arranged in a direction perpendicular to an optical axis of incident X-rays by changing an orientation of the fitting convex portion of the sample holder around a central axis by 90° with respect to the holding groove of the base member and fitting the fitting convex portion into the holding groove of the base member.

4. The sample holding device for X-ray analysis according to claim 3 , wherein an upper surface of the base member is arranged at the same height position as an X-ray irradiation position in an X-ray analysis apparatus when the sample holding device for X-ray analysis is mounted in the X-ray analysis apparatus, and an opening surface of the recessed groove is positioned so as to be flush with an upper surface of the base member when the sample holder is held in the base member.

5. The sample holding device for X-ray analysis according to claim 1 , wherein the airtight member is provided with a knife edge in the hollow portion of the main body portion, the knife edge hanging downward from a ceiling surface and shielding scattered X-rays incident through the X-ray transmission window.

6. The sample holding device for X-ray analysis according to claim 1 , wherein the mounting portion of the base member is formed by a concave portion or a convex portion, the fitting portion of the airtight member is formed in a tubular shape that allows the fitting portion to be fitted into the mounting portion, and the locking mechanism is provided to each fitting surface of the mounting portion and the fitting portion.

Assignees

• Rigaku Denki Co Ltd

Inventors

• Ito Koichiro

Classifications

• G01N2223/309

  support of sample holder · CPC title

• G01N23/20025 Primary

  Sample holders or supports therefor · CPC title

• G01N23/2204 Primary

  Specimen supports therefor; Sample conveying means therefore · CPC title

• G01N2223/056

  diffraction · CPC title

• G21F7/02

  Observation devices permitting vision but shielding the observer {(optical systems per se G02)} · CPC title