Method of producing olefin using circulating fluidized bed process
US-11439982-B2 · Sep 13, 2022 · US
US11512019B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-11512019-B2 |
| Application number | US-201716321613-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jul 14, 2017 |
| Priority date | Aug 10, 2016 |
| Publication date | Nov 29, 2022 |
| Grant date | Nov 29, 2022 |
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A fluidized-bed-type apparatus and method for treating gypsum, which activates or improves fluidity of gypsum powder to promote an effect of treatment of gypsum, such as modification or homogenization of the gypsum powder. The apparatus for treating gypsum includes a reactor vessel, a conditioned air supply port, a horizontal partition wall and a plurality of stationary vanes. The wall allows a conditioned air flow to flow upward into a reaction region. The vanes are arranged at an angular interval in a circumferential direction. A fluidized bed of calcined gypsum is provided in the vessel. The vane deflects the conditioned air flow flowing upward into the reaction region, toward a radially outward and circumferential direction of the reaction region. The calcined gypsum makes a saltational fluid motion or saltational movement in the vessel with the air flow.
Opening claim text (preview).
The invention claimed is: 1. A gypsum treating apparatus including a reactor vessel, an inlet port for gypsum powder and a gaseous fluid flow supply port, the reactor vessel having an inner wall surface with a circular or annular horizontal cross-section or configuration, said inlet port being configured to feed gypsum powder into a reaction region in the reactor vessel, and said gaseous fluid flow supply port being positioned in a bottom part of the reaction region and configured to provide an upward gaseous fluid flow in the reaction region to agitate the gypsum powder accumulated in the bottom part of the reaction region; comprising: a plurality of stationary vanes extending toward said inner wall surface from a support which is positioned in a center area of the reaction region, wherein the vanes are spaced from each other at an angular interval in a circumferential direction of said reaction region and the vanes are spaced apart at a horizontal distance from said inner wall surface to produce a circumferentially directed movement of the gypsum powder in a vicinity of the inner wall surface; wherein said vanes are positioned at a level at which the vanes are at least partially embedded in the gypsum powder accumulated in the reaction region, the adjacent vanes being configured to form a fluid path therebetween into which said flow spouted from a bottom surface of the reaction region is introduced and in which the gypsum powder is fluidized by the flow, and the fluid path being inclined to deflect said flow toward a radially outward and circumferential direction of said reaction region; and wherein a lower edge portion of said vane is curved as seen in its plan view, and an outer end portion of the lower edge portion is spaced at a predetermined horizontal distance (dc) from a circumferential wall of said reactor vessel defining said inner wall surface, and the horizontal distance (dc) is set to be in a range from 0.2× a diameter (da) to 0.05× the diameter (da), wherein the diameter (da) is an inner diameter of said circumferential wall. 2. The apparatus as defined in claim 1 , wherein said vanes adjacent to each other define said fluid path which opens toward a peripheral zone of said reaction region and which extends upward in a direction generally inclined with respect to a vertical direction and opens to an upper space. 3. The apparatus as defined in claim 1 , wherein, with respect to angular positions of outer and inner ends of a lower part of said vane around a center axis of said reactor vessel or said reaction region, the outer end of the lower part of the vane residing backward in a direction of deflection of said flow is located at an angular position forward in the direction of deflection, relative to the inner end of the lower part of the vane residing forward in said direction of deflection, or wherein proximal end portions of the adjacent vanes supported by said support are superimposed as seen in their plan views, so that an overlapping area (η) of the adjacent vanes is formed in a periphery of said support. 4. The apparatus as defined in claim 1 , wherein said angular interval is set to be an angle in a range from 10 degrees to 60 degrees. 5. The apparatus as defined in claim 1 , wherein each of said vanes is a curved plate defining the curved fluid path, which deflects the gypsum powder upwardly moving together with said flow, toward the radially outward and circumferential direction. 6. A gypsum treating method for use by the apparatus of claim 1 , wherein the upward gaseous fluid flow introduced into said reaction region from said bottom surface of the reaction region is guided toward the radially outward and circumferential direction of the reaction region by said vane, and the gypsum powder is fluidized in the radially outward and circumferential direction of the reaction region, owing to deflection of said flow, whereby the gypsum powder is energized in a circumferential direction of a body of the reactor vessel, or movement of the gypsum powder in the circumferential direction is augmented in a vicinity of said inner wall surface. 7. A gypsum treating method for use by the apparatus of claim 1 , wherein said inlet port is connected to an apparatus for gypsum calcination or a gypsum calciner through a gypsum supply passage, so that said reaction region is fed with the calcined gypsum produced by the apparatus for gypsum calcination or the gypsum calciner, whereby a treatment for modifying or homogenizing the calcined gypsum is performed. 8. The method as defined in claim 6 , wherein air or gas regulated in a predetermined temperature and/or a predetermined humidity, or humid air or humid gas containing moisture equal to or greater than a predetermined quantity of moisture content is introduced into said reaction region as said upward gaseous fluid flow. 9. The method as defined in claim 7 , wherein air or gas regulated in a predetermined temperature and/or a predetermined humidity, or humid air or humid gas containing moisture equal to or greater than a predetermined quantity of moisture content is introduced into said reaction region as said upward gaseous fluid flow. 10. A gypsum treating apparatus including a reactor vessel, an inlet port for gypsum powder and a gaseous fluid flow supply port, the reactor vessel having an inner wall surface with a circular or annular horizontal cross-section or configuration, said inlet port being configured to feed gypsum powder into a reaction region in the reactor vessel, and said gaseous fluid flow supply port being positioned in a bottom part of the reaction region and configured to provide an upward gaseous fluid flow in the reaction region to agitate the gypsum powder accumulated in the bottom part of the reaction region; comprising: a plurality of stationary vanes extending toward said inner wall surface from a support which is positioned in a center area of the reaction region, wherein the vanes are spaced from each other at an angular interval in a circumferential direction of said reaction region and the vanes are spaced apart at a horizontal distance from said inner wall surface to produce a circumferentially directed movement of the gypsum powder in a vicinity of the inner wall surface; wherein said vanes are positioned at a level at which the vanes are at least partially embedded in the gypsum powder accumulated in the reaction region, the adjacent vanes being configured to form a fluid path therebetween into which said flow spouted from a bottom surface of the reaction region is introduced and in which the gypsum powder is fluidized by the flow, and the fluid path being inclined to deflect said flow toward a radially outward and circumferential direction of said reaction region; and wherein said reactor vessel is provided with a partition wall defining said bottom surface of said reaction region, and a plenum chamber supplied with gas for said flow under pressure is formed between the partition wall and a bottom wall of the reactor vessel, and wherein the partition wall has a gas permeability resistance such that a dynamic pressure of the gas supplied to the plenum chamber is converted to a static pressure at least partially and a gas permeability such that the gas is caused to flow therethrough from said chamber into said reaction region in accordance with a difference in a gaseous pressure between said reaction region and said chamber. 11. The apparatus as defined in claim 10 , wherein said plenum chamber is divided into a plurality of plenum chamber sections by a partition wall or partition walls, and each of the plenum chamber sections is provided with said gaseous fluid flow supply port for said upward gaseous fluid flow, so
with fluidised bed containing a rotatable device or being subject to rotation {or to a circulatory movement, i.e. leaving a vessel and subsequently re-entering it} · CPC title
for the dry process, e.g. dehydrating in a fluidised bed or in a rotary kiln {, i.e. to obtain beta-hemihydrate (C04B11/0281 - C04B11/0288 take precedence)} · CPC title
Ingredients added before, or during, the calcining process, e.g. calcination modifiers · CPC title
using hot gas streams in which the material is moved · CPC title
starting from anhydrite · CPC title
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