Extractor and related methods

Patent metadata

Field	Value
Publication number	US-11458415-B2
Application number	US-202017102006-A
Country	US
Kind code	B2
Filing date	Nov 23, 2020
Priority date	Sep 18, 2014
Publication date	Oct 4, 2022
Grant date	Oct 4, 2022

Abstract

An extractor suitable for using a solvent to separate a compound from a solid or semisolid substance containing the compound. The extractor includes a conveying assembly having an inclined conveyor for receiving the substance from a substance inlet and moving the substance through the solvent, an inclined upper surface associated with the first conveyor and an inclined lower surface associated with the first conveyor. The conveyor is configured to move the substance downward through the solvent along the upper surface toward a lower end of the conveyor and upward through the solvent along the lower surface toward an upper end of the conveyor.

First claim

What is claimed is:

1. A method of separating rubber from guayule biomass using solvent extraction, the method comprising:
introducing the guayule biomass into a pool comprising at least one solvent capable of dissolving rubber;
conveying the guayule biomass downward along a first inclined surface through the pool of the at least one solvent capable of dissolving rubber;
conveying the guayule biomass upward along a second inclined surface through the pool of the at least one solvent capable of dissolving rubber; and
conveying the guayule biomass upward along an inclined screen to separate the at least one solvent capable of dissolving rubber from the from the guayule biomass.

2. The method of claim 1 , wherein prior to conveying the guayule biomass upward along the inclined screen, the method further comprises:
moving the guayule biomass from the upper end of the second inclined surface to a third inclined surface;
conveying the guayule biomass downward along the third inclined surface through the pool of the at least one solvent capable of dissolving rubber; and
conveying the guayule biomass upward along a fourth inclined surface through the pool of the at least one solvent capable of dissolving rubber.

3. The method of claim 1 , further comprising introducing the at least one solvent into the pool of the at least one solvent capable of dissolving rubber by spraying the at least one solvent over the inclined screen.

4. The method of claim 1 , further comprising keeping the guayule biomass substantially constantly immersed in the the at least one solvent after introducing the guayule biomass into the pool of the the at least one solvent and before conveying the guayule biomass upward along the inclined screen.

5. The method of claim 1 , further comprising flowing the at least one solvent capable of dissolving rubber in a direction substantially counter to the direction of conveying the guayule biomass upward along the second inclined surface.

6. The method of claim 1 , wherein the at least one solvent capable of dissolving rubber is a non-polar organic solvent selected the group consisting of from alkanes having from 4 to 9 carbon atoms; cycloalkanes and alkyl cycloalkanes having from 5 to 10 carbon atoms; aromatics and alkyl substituted aromatics having from 6 to 12 carbon atoms; and combinations thereof.

7. The method of claim 6 , wherein the pool of the at least one solvent capable of dissolving rubber further includes at least one polar solvent selected from the group consisting of alcohols having 1 to 8 carbon atoms; ethers and esters having from 2 to 8 carbon atoms; cyclic ethers having from 4 to 8 carbon atoms; and ketones having from 3 to 8 carbon atoms; and combinations thereof.

8. The method of claim 7 , wherein the at least one polar solvent includes acetone.

9. The method of claim 1 , wherein the at least one solvent capable of dissolving rubber includes hexane, cyclohexane, or a combination thereof.

10. The method of claim 1 , wherein the conveying along the first and second inclined surfaces is facilitated by a rotating conveyor.

11. The method of claim 10 , wherein the rotating conveyor is a continuous conveyor.

12. The method of claim 10 , wherein the rotating conveyor has a plurality of spaced apart paddles.

13. The method of claim 10 wherein the rotating conveyor is capable of both clockwise and counterclockwise operation.

14. The method of claim 1 , wherein the guayule biomass has an average size of 1 inch or less upon being introduced to the pool of the at least one solvent capable of dissolving rubber.

15. A method of separating rubber from guayule biomass using solvent extraction, the method comprising:
introducing the guayule biomass into a pool of solvents comprising at least one solvent capable of dissolving rubber and at least one polar solvent, wherein the at least one solvent capable of dissolving rubber is selected from the group consisting of hexane, cyclohexane, pentane, and combinations thereof and the at least one polar solvent comprises acetone;
conveying the guayule biomass downward along a first inclined surface through the pool of the solvents;
conveying the guayule biomass upward along a second inclined surface through the pool of the solvents; and
conveying the guayule biomas upward along an inclined screen to separate the solvents from the guayule biomass.

16. The method of claim 15 , wherein prior to conveying the guayule biomass upward along the inclined screen, the method further comprises:
moving the guayule biomass from the upper end of the second inclined surface to a third inclined surface;
conveying the guayule biomass downward along the third inclined surface through the pool of solvents; and
conveying the guayule biomass upward along a fourth inclined surface through the pool of solvents.

17. The method of claim 15 , further comprising introducing the solvents into the pool of solvents by spraying the solvents over the inclined screen.

18. The method of claim 15 , further comprising keeping the guayule biomass substantially constantly immersed in the solvents after introducing the guayule biomass into the pool of solvents and before conveying the guayule biomass upward along the inclined screen.

19. The method of claim 15 , wherein the conveying along the first and second inclined surfaces is facilitated by a rotating conveyor.

20. The method of claim 15 , wherein the guayule biomass has an average size of 1 inch or less upon being introduced to the pool of solvents.

Assignees

• Bridgestone Corp

Inventors

• White Robert W
• Hartzell Michael R

Classifications

• B01D11/0284

  Multistage extraction · CPC title

• B03B5/08

  on vanners · CPC title

• B01D11/023 Primary

  using moving bands, trays fixed on moving transport chains · CPC title

• C08C2/02

  Purification · CPC title

• B01D2011/002

  Counter-current extraction · CPC title