Methods to convert thca into thc
US-2026077276-A1 · Mar 19, 2026 · US
US10245526B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-10245526-B2 |
| Application number | US-201515511981-A |
| Country | US |
| Kind code | B2 |
| Filing date | Sep 15, 2015 |
| Priority date | Sep 18, 2014 |
| Publication date | Apr 2, 2019 |
| Grant date | Apr 2, 2019 |
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An extractor suitable for using a solvent to separate a compound from a solid or semisolid substance containing the compound. The extractor includes a conveying assembly having an inclined conveyor for receiving the substance from a substance inlet and moving the substance through the solvent, an inclined upper surface associated with the first conveyor and an inclined lower surface associated with the first conveyor. The conveyor is configured to move the substance downward through the solvent along the upper surface toward a lower end of the conveyor and upward through the solvent along the lower surface toward an upper end of the conveyor.
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What is claimed is: 1. An extractor suitable for using a solvent to separate a compound from a solid or semisolid substance containing the compound, comprising: a substance inlet for introducing the substance into the extractor; a substance outlet for removing the substance from the extractor; a solvent inlet for introducing the solvent into the extractor; a solvent outlet for removing the solvent from the extractor; and a first conveying assembly including: an inclined first conveyor for receiving the substance from the substance inlet and moving the substance through the solvent, the first conveyor including an upper end and a lower end opposite its upper end, wherein the first convey includes an inclined first upper surface and an inclined first lower solid surface substantially parallel to the inclined first upper surface; wherein the first conveyor is configured to move the substance downward through the solvent along the first upper surface toward the lower end and upward through the solvent along the first lower solid surface toward the upper end, wherein the compound comprises rubber and the solid or semisolid substance comprises guayule plant matter. 2. The extractor of claim 1 , wherein the solvent flows from the solvent inlet to the solvent outlet in a direction generally counter to the movement of the substance from the substance inlet to the substance outlet. 3. The extractor of claim 1 , further comprising: a second conveying assembly including: a second inclined conveyor positioned between the first conveyor and the substance outlet and substantially parallel to the first conveyor, the second conveyor including an upper end and a lower end opposite its upper end, wherein the second conveyor includes an inclined second upper surface and an inclined second lower solid surface substantially parallel to the inclined second upper surface; wherein the second conveyor is configured to move the substance downward through the solvent along the second upper surface toward the second conveyor lower end and upward through the solvent along the second lower solid surface toward the second conveyor upper end. 4. The extractor of claim 3 , wherein the first lower surface includes an upper terminal end positioned above the second conveyor such that substance falls from the first lower solid surface toward the second upper surface when moved beyond the upper terminal end by the first conveyor. 5. The extractor of claim 1 , further comprising a tank configured to contain solvent at a predetermined level within the extractor, wherein the upper terminal end of the first lower solid surface is positioned at or below the level of solvent in the extractor. 6. The extractor of claim 1 , wherein the first conveyor is inclined at an angle in the range of approximately 20 degrees to approximately 30 degrees. 7. The extractor of claim 1 , further comprising: an exit conveying assembly including: an exit conveyor positioned between the first conveyor and the substance outlet and substantially parallel to the first conveyor, the exit conveyor including an upper end and a lower end opposite its upper end, wherein the exit conveyor includes an inclined exit upper surface and an inclined exit lower surface substantially parallel with the inclined exit upper surface; wherein the exit conveyor is configured to move the substance downward through the solvent along the exit upper surface toward the exit conveyor lower end and upward through the solvent along the exit lower surface toward the exit conveyor upper end. 8. The extractor of claim 7 , wherein the exit conveyor has a length that is approximately 175% to approximately 200% the length of the first conveyor. 9. The extractor of claim 7 , wherein the inclined exit lower surface at least partially comprises an inclined screen section, wherein the exit conveyor is configured to move the substance from the inclined exit lower surface upward along the inclined screen section toward the inclined exit conveyor upper end, wherein the inclined screen section is configured to allow solvent to drain from the substance. 10. The extractor of claim 9 , wherein a solvent inlet is configured to spray solvent onto the inclined screen section. 11. The extractor of claim 9 , wherein the inclined screen section comprises approximately 40% to approximately 55% the length of the exit conveyor. 12. A method of separating a compound from a solid or semi-solid substance using the extractor of claim 9 and at least one solvent, the method comprising: introducing the substance into a pool of at least one solvent capable of dissolving the compound; conveying the substance downward along the first inclined surface through the pool of the solvent; conveying the substance upward along the second inclined solid surface through the pool of solvent; and conveying the substance upward along the inclined screen to separate the solvent from the substance. 13. The method of claim 12 , wherein prior to the conveying the substance upward along the inclined screen, the method further comprises: moving the substance from the upper end of the second inclined solid surface to a third inclined surface; conveying the substance downward along the third inclined surface through the pool of the solvent; and conveying the substance upward along a fourth inclined solid surface through the pool of solvent. 14. The method of claim 12 , further comprising at least one of the following: a. introducing solvent into the pool of solvent by spraying solvent over the inclined screen; b. keeping the substance substantially constantly immersed in the solvent after introducing the substance into the pool of solvent and before conveying the substance upward along the inclined screen; or c. flowing the solvent in a direction substantially counter to the direction of conveying the substance upward along the second inclined solid surface. 15. The extractor of claim 1 , further comprising a clarifying conveyor and an inclined clarifying lower surface associated with the clarifying conveyor, wherein the clarifying conveyor is positioned between the substance inlet and the solvent outlet and is configured to move the substance upward through the solvent along the clarifying lower surface toward the first conveyor. 16. The extractor of claim 1 , further comprising a separator in fluid communication with the solvent outlet, the separator configured to separate small particles of substance from the solvent that exits the solvent outlet. 17. The extractor of claim 1 , wherein the substance outlet includes a run-down screen configured to receive solvent-containing substance from the exit conveyor and allow at least a portion of the solvent to drain from the solvent-laden substance while on the screen; wherein the run-down screen has no moving parts and removal of the substance from the run-down screen is gravity fed. 18. The extractor of claim 1 , wherein each conveyor includes paddles configured to assist in moving the substance along the upper and lower surfaces associated with each respective conveyor. 19. The extractor of claim 1 , further comprising at least one additional solvent inlet, solvent outlet, substance inlet, or substance outlet. 20. The extractor of claim 1 , wherein the extractor comprises additional conveying assemblies for moving the substance through the solvent such that the extractor has a total of six conveying assemblies arranged in series, each additional conveying assembly including an i
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