Autosampler with sample agitation system

Patent metadata

Field	Value
Publication number	US-11397142-B1
Application number	US-201916724915-A
Country	US
Kind code	B1
Filing date	Dec 23, 2019
Priority date	Aug 7, 2015
Publication date	Jul 26, 2022
Grant date	Jul 26, 2022

Abstract

A sample agitation system for an automated sampling device is described. In an example implementation, the sample agitation system includes a sample probe configured to contact a sample positioned within a sample vessel. Further, the sample agitation system includes an actuator coupled to the sample probe that is configured to stir the sample positioned within the sample vessel in one or more rotational directions. The directions may include, but are not limited to, clockwise motion, anti-clockwise motion, or the like. In some implementations, a sample probe support arm can be coupled to the sample probe and/or the actuator. The actuator can move the sample probe support arm in a translational, a rotational, and/or a vertical direction to rotate the sample probe and stir the sample.

First claim

What is claimed is:

1. An autosampler device, comprising:
a sample probe configured to contact a sample positioned within a sample vessel and configured to aspirate at least a portion of the sample from the sample vessel;
a sample probe support arm coupled to the sample probe;
a z-axis support member coupled to the sample probe support arm, the z-axis support member having an axis passing longitudinally through the z-axis support member, wherein the sample probe support arm is configured to rotate about the axis for positioning the sample probe, and wherein the sample probe support arm is configured to translate along the axis for positioning the sample probe into the sample vessel to contact the sample; and
an actuator coupled to the sample probe via the sample probe support arm, the actuator configured to position the sample probe into the sample located within the sample vessel using at least two dimensions of motion, the actuator configured to move the sample probe in one or more directions relative to the sample vessel to agitate the sample.

2. The autosampler device of claim 1 , wherein the actuator is configured to move the sample probe in at least a horizontal direction relative to the sample vessel.

3. The autosampler device of claim 1 , further including a drive assembly operably coupled to the actuator, the drive assembly configured to move the sample probe support arm in at least one of a translational, a rotational, or a vertical direction to agitate the sample.

4. The autosampler device of claim 1 , further including a controller operably coupled to the actuator, the controller configured to cause the actuator to execute at least one programmed instruction based on a user parameter.

5. The autosampler device of claim 4 , wherein the user parameter includes at least one of an agitation speed, an agitation time interval, or an agitation direction.

6. The autosampler device of claim 1 , wherein the sample probe includes one or more structures positioned on an outer surface of the sample probe, the one or more structures configured to contact the sample, the one or more structures configured to induce or increase agitation of the sample during motion of the sample probe.

7. The autosampler device of claim 6 , wherein the at least one structure of the one or more structures includes a portion that is offset relative to a z-axis.

8. An autosampler device, comprising:
a sample probe configured to contact a sample positioned within a sample vessel and configured to aspirate at least a portion of the sample from the sample vessel;
a sample probe support arm coupled to the sample probe;
a z-axis support member coupled to the sample probe support arm, the z-axis support member having an axis passing longitudinally through the z-axis support member, wherein the sample probe support arm is configured to rotate about the axis for positioning the sample probe, and wherein the sample probe support arm is configured to translate along the axis for positioning the sample probe into the sample vessel to contact the sample; and
an actuator coupled to at least one of the sample probe or the sample probe support arm, the actuator configured to oscillate the sample probe and to agitate the sample positioned within the sample vessel in a path through at least one of x, y, or z planes relative to the sample vessel, the actuator configured to offset the sample probe from a position within the sample vessel, to oscillate the sample probe about the position, and to return the sample probe to the position to aspirate the sample.

9. The autosampler device of claim 8 , further including a drive assembly operably coupled to the actuator, the drive assembly configured to move the sample probe support arm in at least one of a translational, a rotational, or a vertical direction to oscillate the sample probe.

10. The autosampler device claim 8 , further including a controller operably coupled to the actuator, the controller configured to cause the actuator to execute at least one programmed instruction based on a user parameter.

11. The autosampler device claim 10 , wherein the user parameter includes at least one of an agitation speed, an agitation time interval, or an agitation direction.

12. The autosampler device of claim 8 , wherein the sample probe includes one or more structures positioned on an outer surface of the sample probe, the one or more structures configured to induce or increase agitation of the sample during motion of the sample probe.

13. The autosampler device of claim 1 , wherein the actuator is directly coupled to the sample probe.

14. The autosampler device of claim 8 , wherein the actuator is directly coupled to at least one of the sample probe or the sample probe support arm.

15. The autosampler device of claim 8 , wherein the sample probe support arm carries the sample probe, the sample probe support arm movably mounted relative to the sample vessel.

Assignees

• Elemental Scientific Inc

Inventors

• Toms Andrew D

Classifications

• G01N35/00722

  Communications; Identification · CPC title

• B01F2101/23

  Mixing of laboratory samples e.g. in preparation of analysing or testing properties of materials · CPC title

• B01F27/90

  with paddles or arms · CPC title

• B01F27/806

  with vertical displacement of the stirrer, e.g. in combination with means for pivoting the stirrer about a vertical axis in order to co-operate with different receptacles · CPC title

• G01N2001/386

  Other diluting or mixing processes · CPC title