Solidifying liquid anionic surfactants

Patent metadata

Field	Value
Publication number	US-11377628-B2
Application number	US-201916258942-A
Country	US
Kind code	B2
Filing date	Jan 28, 2019
Priority date	Jan 26, 2018
Publication date	Jul 5, 2022
Grant date	Jul 5, 2022

Abstract

The invention relates to solidification of liquid anionic surfactants with a binder, carrier, or both binder and carrier to form a solidified surfactant composition. In particular, the invention relates to solidification of liquid surfactants utilizing drying device(s), wherein the feed composition contains at least one liquid surfactant and the binder, carrier, or binder and carrier to form a solidified surfactant composition. The solidified surfactant compositions can be useful in various cleaning compositions.

First claim

What is claimed is:

1. A method of preparing a solidified surfactant composition comprising:
adding to a drying device:
a liquid anionic surfactant comprising a sulfate surfactant, a sulfonate surfactant, or a combination thereof; and one or more of
a solid binder comprising a natural polymer, a urea derivative, a polyacrylate, a polyethylene glycol (PEG), or a combination thereof; wherein the solid binder is dissolved with the liquid surfactant in a ratio of between about 4:1 to about 1:60 by actives, and
a solid carrier comprising an alpha olefin sulfonate, linear alkyl sulfonate, sodium lauryl sulfate, sodium alkyl sulfate, sodium carbonate, magnesium carbonate, sodium acetate, magnesium acetate, sodium sulfate, magnesium sulfate, sodium chloride, or combination thereof, wherein the carrier and the liquid surfactant are in a ratio of between about 5:1 to about 1:30 by actives, and wherein the carrier is a solid component when added to the drying device;
drying the liquid surfactant and one or more of binder and solid carrier to form a solidified surfactant composition;
wherein the drying device comprises a spray dryer; wherein the spray dryer has an inlet and an outlet wherein the inlet temperature is between about 20° C. and about 250° C.; and wherein the outlet temperature is less than about 150° C.; and
wherein the liquid surfactant is solidified in the solidified surfactant composition, and wherein the solidified surfactant composition has less than about 5 wt-% water.

2. The method of claim 1 , wherein the liquid surfactant is a C4-C18 alkyl sulfate, a C4-C18 alkyl ether sulfate, an alkyl benzene sulfonate, an ammonium lauryl sulfate, a linear alkyl benzene sulfonate, a linear alkyl benzene sulfonic acid, an isopropylamine dodecylbenzene sulfonate, or a combination thereof.

3. The method of claim 1 , wherein the liquid surfactant is a sodium lauryl ether sulfate.

4. The method of claim 1 , wherein the method comprises the binder and wherein the binder is a PEG having a melting point of at least about 40° C., a gum, a cellulose, a cellulose ester, a chitin, a chitosan, a starch, protein, a lignin, a natural rubber, or a combination thereof.

5. The method of claim 1 , wherein the method comprises the carrier.

6. The method of claim 1 , wherein the solidified surfactant composition contains at least about 10 wt. % active surfactants.

7. The method of claim 1 , wherein the drying process is performed in a batch system.

8. The method of claim 1 , wherein the drying process is performed in a continuous system.

9. The method of claim 1 , wherein the method comprises the binder and the carrier.

Assignees

• Ecolab Usa Inc

Inventors

• Lo Wendy
• Olson Erik C
• Hansen Jon D
• Molinaro Katherine J
• Rosenthal Corey

Classifications

• C11D3/3749

  Polyolefins; Halogenated polyolefins; Natural or synthetic rubber; Polyarylolefins or halogenated polyarylolefins · CPC title

• C11D1/29

  Sulfates of polyoxyalkylene ethers · CPC title

• C11D3/10

  Carbonates {; Bicarbonates} · CPC title

• C11D3/222

  Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin · CPC title

• C11D3/38

  Products with no well-defined composition {, e.g. natural products} · CPC title