Hybrid tray for introducing a low CO2 feed stream into a distillation tower

Patent metadata

Field	Value
Publication number	US-11306267-B2
Application number	US-201916440021-A
Country	US
Kind code	B2
Filing date	Jun 13, 2019
Priority date	Jun 29, 2018
Publication date	Apr 19, 2022
Grant date	Apr 19, 2022

Abstract

A method of separating a feed stream in a distillation tower. Vapor is permitted to rise upwardly from a distillation section of the distillation tower. A feed stream is introduced into a controlled freeze zone section of the distillation tower, the controlled freeze zone section being situated above the distillation section. The feed stream is released above a level of a liquid retained by a melt tray assembly in the controlled freeze zone section. Vapor from the distillation section is directed into the liquid retained by the melt tray assembly. A solid is formed from the feed stream in the controlled freeze zone section.

First claim

What is claimed is:

1. A distillation tower for separating a feed stream, the distillation tower comprising:
a distillation section permitting vapor to rise upwardly from said distillation section;
a controlled freeze zone section situated above the distillation section, the controlled freeze zone constructed and arranged to form a solid from a feed stream, the controlled freeze zone section including
a spray assembly in the controlled freeze zone upper section, and
a melt tray assembly in the controlled freeze zone lower section;

wherein the melt tray assembly includes
a feed stream manifold that directs the feed stream into the distillation tower,
at least one vapor stream riser that directs the vapor from the distillation section into liquid retained by the melt tray assembly, wherein the at least one vapor stream riser passes through the feed stream manifold without mixing the feed stream with the vapor stream from the distillation section, and
at least one feed stream riser, each feed stream riser having a lower end operationally connected to the feed stream manifold and an upper end positioned above a level of the liquid retained by the melt tray assembly, wherein the feed stream is released above the level of the liquid retained by the melt tray assembly.

2. The distillation tower of claim 1 , further comprising:
a distribution cap disposed on the upper end of one or more of the at least one feed stream risers, the distribution cap configured to distribute the feed stream throughout the controlled freeze zone section.

3. The distillation tower of claim 2 , further comprising openings on the top of the distribution cap to permit the feed stream to pass through.

4. The distillation tower of claim 1 , further comprising a cap or tray positioned above the distribution cap, the cap or tray further distributing the feed stream throughout the controlled freeze zone section.

5. The distillation tower of claim 1 , further comprising:
a bubble cap arranged above each of the at least one vapor risers, each bubble cap arranged above an upper end of the respective vapor riser, the bubble cap having a closed upper end and an open lower end, the open lower end situated below the level of the liquid retained by the melt tray assembly.

6. The distillation tower of claim 1 , wherein the controlled freeze zone further comprises:
the spray assembly arranged above the melt tray assembly, the spray assembly configured to spray a liquid into the feed stream exiting the at least one feed stream riser.

7. The distillation tower of claim 1 , wherein the melt tray assembly further comprises a heating mechanism configured to heat the liquid retained by the melt tray assembly.

8. The distillation tower of claim 1 , wherein the feed stream comprises a hydrocarbon and a contaminant, and wherein the feed stream contains less than 30% contaminant when introduced into the controlled freeze zone section.

Assignees

• Valencia Jaime A
• Mart Charles J
• Smith Ransdall K
• Maher David W
• Exxonmobil Upstream Res Co

Inventors

• Valencia Jaime A
• Mart Charles J
• Smith Ransdall K
• Maher David W

Classifications

• B01D1/16 Primary

  by spraying (B01D1/22 takes precedence) · CPC title

• C07C7/05

  with the aid of auxiliary compounds · CPC title

• B01D3/20

  Bubble caps; Risers for vapour; Discharge pipes for liquid · CPC title

• F25J2205/04

  in the feed line, i.e. upstream of the fractionation step · CPC title

• F25J1/0022

  Hydrocarbons, e.g. natural gas · CPC title