Method and device for carrying out endothermic gas phase-solid or gas-solid reactions
US-11691115-B2 · Jul 4, 2023 · US
US11266966B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-11266966-B2 |
| Application number | US-201715851613-A |
| Country | US |
| Kind code | B2 |
| Filing date | Dec 21, 2017 |
| Priority date | Dec 21, 2017 |
| Publication date | Mar 8, 2022 |
| Grant date | Mar 8, 2022 |
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A process and apparatus is disclosed for gradually starting fluidization in a bed of particulate from the top down so as to avoid thrusting the entire mass of particulates upwardly in the bed at the same time which may damage internals in the bed. The particulate bed may comprise a catalyst cooler for an FCC unit containing internals such as cooling, fluidization and support equipment.
Opening claim text (preview).
The invention claimed is: 1. A process for fluidizing a bed of catalyst in a vessel comprising internals and said bed of catalyst: fluidizing an upper section of the bed of catalyst by distributing gas below said upper section; fluidizing a lower section of the bed of catalyst that is below said upper section by distributing gas below said lower section; and initiating said fluidizing of said upper section before initiating said fluidizing of said lower section. 2. The process of claim 1 further comprising fluidizing an intermediate section of the bed of catalyst that is below said upper section and above said lower section by distributing gas below said intermediate section and above said lower section and initiating said fluidizing of said upper section before initiating said fluidizing of said intermediate section and initiating said fluidizing of said intermediate section before initiating said fluidizing of said lower section. 3. The process of claim 1 further comprising fluidizing said upper section with gas distributed from a fluidization distributor protruding laterally through the side of the vessel. 4. The process of claim 1 further comprising fluidizing said lower section with gas distributed from an elongated fluidization distributor extending longitudinally through the vessel. 5. The process of claim 1 further comprising reducing the flow rate of fluidizing gas below said upper section to fluidize said upper section after initiating fluidizing said lower section. 6. The process of claim 5 further comprising increasing the flow rate of distributing gas below said lower section for fluidizing said lower section gradually. 7. The process of claim 1 further comprising delivering water to an inner tube of a nested tubes; indirectly heating said water to steam or to higher pressure steam in said catalyst bed; withdrawing said steam from said catalyst bed through an outer tube of said nested tubes. 8. The process of claim 1 further comprising: combusting coke from spent catalyst in a regenerator to provide regenerated catalyst and flue gas; passing hot catalyst from said regenerator to said vessel to cool said hot catalyst; and passing cooled catalyst back to said regenerator. 9. A process for starting fluidization of a bed of catalyst in a catalyst cooler vessel comprising internals and said bed of catalyst: fluidizing an upper section of the bed of catalyst by distributing gas below said upper section; fluidizing a lower section of the bed of catalyst that is below said upper section by distributing gas below said lower section; initiating said fluidizing of said upper section before initiating said fluidizing of said lower section; combusting coke from spent catalyst in a regenerator vessel and disengaging hot catalyst from flue gas in said regenerator vessel; and passing said hot catalyst to said catalyst cooler vessel to said bed of catalyst to cool said hot catalyst; and passing said cooled catalyst to said regenerator vessel. 10. The process of claim 9 further comprising fluidizing an intermediate section of the bed of catalyst that is below said upper section and above said lower section by distributing gas below said intermediate section and above said lower section and initiating said fluidizing of said upper section before initiating said fluidizing of said intermediate section and initiating said fluidizing of said intermediate section before initiating said fluidizing of said lower section. 11. The process of claim 9 further comprising reducing the flow rate of distributing gas below said upper section to fluidize said upper section after initiating fluidizing said lower section. 12. The process of claim 11 further comprising increasing the flow rate of fluidizing gas below said lower section for fluidizing said lower section gradually. 13. The process of claim 9 further comprising delivering water to an inner tube of a nested tubes; indirectly heating said water to steam or higher pressure steam in said catalyst bed; withdrawing said steam from said catalyst bed through an outer tube of said nested tubes. 14. The process of claim 9 further comprising fluidizing said upper section with gas distributed from a fluidization distributor protruding laterally through the side of the vessel. 15. The process of claim 11 further comprising fluidizing said lower section with gas distributed from an elongated fluidization distributor extending longitudinally through the vessel.
Indirectly heating or cooling material within regeneration zone or prior to entry into regeneration zone · CPC title
Means for reactor start-up · CPC title
Multi-circuit heat-exchangers, e.g. integrating different heat exchange sections in the same unit or heat-exchangers for more than two fluids (F28D7/103 takes precedence) · CPC title
Tubes · CPC title
the surrounding tube being closed at one end, e.g. return type (F28D7/14 takes precedence) · CPC title
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