Tube furnace device for an atomizing furnace

Patent metadata

Field	Value
Publication number	US-11047802-B2
Application number	US-201716494821-A
Country	US
Kind code	B2
Filing date	Mar 27, 2017
Priority date	Mar 27, 2017
Publication date	Jun 29, 2021
Grant date	Jun 29, 2021

Abstract

The invention relates to a tube furnace device for an atomizing furnace and to an analyzing apparatus comprising an atomizing furnace and a tube furnace device, in particular for atomic absorption spectrometry, the tube furnace device comprising a sample carrier means (11) and a bearing means (12) for supporting and forming electrical contact with the sample carrier means, the sample carrier means having a receiving tube (16) forming a tubular receiving space (17) for receiving an analyte, the sample carrier means having two bearing protrusions on the receiving tube for forming a connection with the bearing means, the bearing protrusions extending perpendicularly, preferably orthogonally, in relation to a longitudinal axis of the receiving tube, wherein the tube furnace device has a contact pressure means (13) via which a contact pressure force (14) can be exerted on the bearing protrusions in the direction of a passant line (20) in relation to a circular cross section (21) of the receiving tube.

First claim

The invention claimed is:

1. A tube furnace device ( 10 ) for an atomizing furnace, in particular for atomic absorption spectrometry, the tube furnace device comprising a sample carrier ( 11 ) and a bearing ( 12 ) for supporting and forming electrical contact with the sample carrier, the sample carrier having a receiving tube ( 16 ) forming a tubular receiving space ( 17 ) for receiving an analyte, the sample carrier having two bearing protrusions ( 15 ) on the receiving tube for forming a connection with the bearing, the bearing protrusions extending perpendicularly in relation to a longitudinal axis ( 18 ) of the receiving tube, characterized in that the tube furnace device has a contact pressure ( 13 ) via which a contact pressure force ( 14 ) is exerted on the bearing protrusions in the direction of a passant line ( 20 ) in relation to a circular cross section ( 21 ) of the receiving tube;
wherein the contact pressure ( 13 ) has two contact pressure elements ( 22 , 23 ), each contact pressure element being associated with one bearing protrusion ( 15 ) and the bearing ( 12 ) has two bearing seats ( 29 , 30 ), each bearing seat being associated with one bearing protrusion ( 15 ).

2. The tube furnace device according to claim 1 , characterized in that the tube furnace device ( 10 ) is made entirely of graphite.

3. The tube furnace device according to claim 1 , characterized in that the receiving tube ( 16 ) is transversally electrically heated via the bearing protrusions ( 15 ).

4. The tube furnace device according to claim 1 , characterized in that the bearing protrusion ( 15 ) is composed of a bearing body ( 34 ) and a support web ( 35 ), the support web connecting the bearing body to the receiving tube ( 16 ).

5. The tube furnace device according to claim 1 , characterized in that the contact pressure elements ( 22 , 23 ) are arranged on the bearing protrusions ( 15 ) in such a manner that the contact pressure force ( 14 ) is exerted perpendicularly on the bearing protrusions in relation to a longitudinal axis ( 19 ) of the bearing protrusions.

6. The tube furnace device according to claim 1 , characterized in that a passage opening ( 24 ) is formed in one contact pressure element ( 22 ), the passage opening being coaxial with an opening ( 26 ) formed in a wall ( 25 ) of the receiving tube ( 16 ) for receiving an analyte.

7. The tube furnace according to claim 1 , characterized in that each bearing protrusion ( 15 ) is arranged between a contact pressure element ( 22 , 23 ) and a bearing seat ( 29 , 30 ).

8. The tube furnace device according to claim 1 , characterized in that the respective contact pressure elements ( 22 , 23 ) and the respective bearing seats ( 29 , 30 ) are arranged in relation to each other in such a manner that an electrically isolating gap ( 28 ) is formed.

9. The tube furnace device according to claim 1 , characterized in that a contact pressure element ( 22 , 23 ) and the associated bearing seat ( 29 , 30 ) together form a floating bearing for supporting the sample carrier ( 11 ).

10. The tube furnace device according to claim 1 , characterized in that the bearing protrusions ( 15 ) and the bearing seats ( 29 , 30 ) each form a contact surface pair ( 38 ) with a bearing surface ( 36 ) of a bearing protrusion ( 15 ) and a seat surface ( 37 ) of a bearing seat ( 29 , 30 ).

11. The tube furnace device according to claim 10 , characterized in that the contact surface pair ( 38 ) is formed in such a manner that a force action of the contact pressure force ( 14 ) on the receiving tube ( 16 ) is avoided.

12. The tube furnace according to claim 10 , characterized in that the seat surface ( 37 ) has two partial surfaces, a first partial surface ( 39 ) being parallel and a second partial surface ( 40 ) being perpendicular to an effective direction of the contact pressure force ( 14 ), a force component of the contact pressure force being exertable on the first partial surface via the second partial surface.

13. The tube furnace device according to claim 10 , characterized in that the tube furnace device ( 10 ) comprises a gas conductor ( 43 ) for forming a gas flow onto the receiving tube ( 16 ).

14. The tube furnace device according to claim 13 , characterized in that the bearing seats ( 29 , 30 ) each form a gas duct ( 32 ) of the gas conductor ( 43 ).

15. The tube furnace device according to claim 13 , characterized in that the bearing protrusions ( 15 ) have passage bores ( 44 ) of the gas conductor ( 43 ) which extend in the direction of the receiving tube ( 16 ).

16. The tube furnace device according to claim 15 , characterized in that the passage bores ( 44 ) are connected to the respective gas duct ( 32 ) in a sealing manner via the contact surface pair ( 38 ).

17. The tube furnace device according to claim 1 , characterized in that the bearing seats ( 29 , 30 ) each have a connecting pin ( 27 ) for connecting the tube furnace device ( 10 ) to a tube furnace seat of an atomizing furnace.

18. The tube furnace according to claim 1 , characterized in that the tube furnace device ( 10 ) comprises a cover ( 48 ) for covering longitudinal ends ( 52 ) of the sample carrier ( 11 ), the cover being composed of plate-shaped cover elements ( 49 , 50 ) having a passage opening ( 51 ) arranged coaxially with the receiving tube ( 16 ).

Assignees

• Schunk Kohlenstofftechnik Gmbh
• Shimadzu Corp

Inventors

• Gaertner Ralf
• Weck Rudolf
• Honda Akira
• Kobayashi Osuke

Classifications

• G01N21/3103

  Atomic absorption analysis · CPC title

• G01N21/74 Primary

  using flameless atomising, e.g. graphite furnaces · CPC title

• F27B9/06

  heated without contact between combustion gases and charge; electrically heated · CPC title

• F27D11/00

  Arrangement of elements for electric heating in or on furnaces · CPC title

• F27D11/02

  Ohmic resistance heating · CPC title