Method for manufacturing a part made from a composite material by means of the injection of a laden ceramic slurry into a fibrous structure

Patent metadata

Field	Value
Publication number	US-11045974-B2
Application number	US-201917046958-A
Country	US
Kind code	B2
Filing date	Apr 4, 2019
Priority date	Apr 13, 2018
Publication date	Jun 29, 2021
Grant date	Jun 29, 2021

Abstract

A process for manufacturing a composite part includes arranging a fibrous preform in a mold including an impregnation chamber which includes in its lower part a filter by making a first face of the preform rest on the filter, the impregnation chamber being closed by a flexible membrane placed opposite a second face of the preform, the membrane separating the impregnation chamber from a compaction chamber. The process further includes injecting a compression fluid into the compaction chamber so as to apply a first pressure on the membrane and injecting a slurry including ceramic particles into the impregnation chamber with a second pressure while maintaining the injection of the compression fluid, the second injection pressure of the slurry being lower than the first pressure on the membrane.

First claim

The invention claimed is:

1. A process for manufacturing a composite part comprising:
arranging a fibrous preform in a mold comprising an impregnation chamber-which comprises in its lower part a filter by making a first face of the preform rest on said filter, the impregnation chamber being closed by a flexible membrane placed opposite a second face of the preform, said membrane separating the impregnation chamber from a compaction chamber; characterized in that the process further comprises the following steps:
injecting a compression fluid into the compaction chamber so as to apply a first pressure on the membrane;
injecting a slurry comprising ceramic particles into the impregnation chamber with a second pressure while maintaining the injection of the compression fluid, the second injection pressure of the slurry being lower than the first pressure on the membrane, and
progressively increasing the first pressure on the membrane and the second injection pressure of the slurry with maintenance of the second injection pressure of the slurry lower than the first pressure on the membrane.

2. The process as claimed in claim 1 , wherein a pressure difference between the first pressure and the second pressure is kept constant at a predetermined value.

3. The process as claimed in claim 1 wherein a pressure difference between the first pressure and the second pressure is less than 5 bar.

4. The process as claimed in claim 3 , wherein the pressure difference between the first pressure and the second pressure is less than 2 bar.

5. The process as claimed in claim 4 , wherein the pressure difference between the first pressure and the second pressure is between 0.5 and 1 bar.

6. The process as claimed in claim 1 , wherein the process further comprises a pre-saturation step carried out prior to injection of the slurry and wherein a liquid is injected through the preform into the impregnation chamber.

7. A system for manufacturing a composite part comprising:
a mold which comprises an impregnation chamber having in its lower part a filter configured to receive a first face of a preform, the impregnation chamber being closed by a flexible membrane located opposite the filter, said membrane separating the impregnation chamber from a compaction chamber;
a compression fluid injection device for injecting a compression fluid into the compaction chamber so as to apply a first pressure on the membrane;
a slurry injection device for injecting a slurry comprising ceramic particles suspended in a liquid phase into the impregnation chamber with a second pressure, and
a control unit configured to control the compression fluid injection device and the slurry injection device to maintain the second slurry injection pressure lower than the first pressure on the membrane, the control unit being further configured to progressively increase the first pressure on the membrane and the second injection pressure of the slurry while maintaining the second injection pressure of the slurry lower than the first pressure on the membrane.

8. The system as claimed in claim 7 , wherein the mold comprises a slurry inlet opening leading to a distribution grid inside the impregnation chamber.

9. The system as claimed in claim 8 , wherein the distribution grid comprises a face opposite to the slurry inlet opening which is covered by a first porous non-stick layer.

10. The system as claimed in claim 7 , wherein the mold comprises a slurry outlet opening leading to a drainage grid, said drainage grid being covered by the filter.

11. The system as claimed in claim 10 , wherein the drainage grid comprises a face opposite the slurry outlet which is covered by a second porous non-stick layer.

Assignees

• Safran Ceram

Inventors

• Philippe Eric
• Carminati Paul
• Bounia Medhy Damien
• Desjoyeaux Bertrand

Classifications

• C04B2235/5224

  Alumina or aluminates · CPC title

• C04B2235/604

  Pressing at temperatures other than sintering temperatures · CPC title

• C04B2235/77

  Density · CPC title

• B28B1/261

  Moulds therefor (absorbent moulds in general B28B7/344) · CPC title

• C04B35/18

  rich in aluminium oxide · CPC title