Method of fabricating a fiber preform filled with refractory ceramic particles

Patent metadata

Field	Value
Publication number	US-10239795-B2
Application number	US-201515538982-A
Country	US
Kind code	B2
Filing date	Dec 18, 2015
Priority date	Dec 23, 2014
Publication date	Mar 26, 2019
Grant date	Mar 26, 2019

Abstract

A method of fabricating a fiber preform filled with refractory ceramic particles, includes placing a fiber texture including refractory ceramic fibers in a mold cavity; injecting a slip including a powder of refractory ceramic particles present in a liquid medium, the slip being injected into the pores of the fiber texture present in the mold cavity, injection being performed through at least a first face or a first edge of the fiber texture; and draining the liquid medium of the slip that has penetrated into the fiber texture through the porous material part, the draining being performed at least through a second face or a second edge of the fiber texture different from the first face or the first edge, the porous material part also serving to retain the refractory particle powder in the pores of the fiber texture to obtain a fiber preform filled with refractory particles.

First claim

The invention claimed is:

1. A method of fabricating a fiber preform filled with refractory ceramic particles, the method comprising the following steps:
a) placing a fiber texture comprising refractory ceramic fibers in a mold cavity defined by a mold and a countermold;
b) injecting a slip comprising a powder of refractory ceramic particles present in a liquid medium, the slip being injected into pores of the fiber texture present in the mold cavity, injection being performed through at least a first face of said fiber texture, wherein during step b), the slip is injected into the mold cavity through one or more injection ports, and prior to step b), the slip presents a volume content of refractory ceramic particles that is less than or equal to 40%; and
c) draining the liquid medium of the slip that has penetrated into the fiber texture through a porous material part having thickness greater than or equal to 0.1 mm, the draining being performed at least through a second face of the fiber texture different from the first face, the first face and the second face both extending from edge to edge, and each edge extending along a thickness of the fiber texture, said porous material part also serving to retain the powder of refractory ceramic particles in the pores of the fiber texture in order to obtain a fiber preform filled with refractory particles, the porous material part being present between the mold and the fiber texture or between the countermold and the fiber texture, and the porous material part being present between at least one outlet vent and the fiber texture, pumping being performed at the outlet vent in order to drain the liquid medium through said outlet vent.

2. A method according to claim 1 , wherein the mold constitutes a rigid support on which the fiber texture is present, and the countermold is rigid.

3. A method according to claim 1 , wherein the mold constitutes a rigid support on which the fiber texture is present and the countermold is deformable.

4. A method according to claim 1 , wherein the countermold exerts pressure on the fiber texture during and/or after step b).

5. A method according to claim 4 , wherein the fiber texture is compacted between the mold and the countermold during and/or after step b).

6. A method according to claim 1 , wherein during step b), the slip is injected through a plurality of different zones of an outside surface of the fiber texture.

7. A method according to claim 6 , wherein a distributor element is present in the mold cavity to distribute the flow of slip, said distributor element defining a plurality of openings through which the slip flows during step b) in order to reach the first face of the fiber texture.

8. A method according to claim 1 , wherein during step b), the slip is also injected through an edge of the fiber texture.

9. A method according to claim 1 , wherein the slip includes an organic binder.

10. A method according to claim 1 , wherein the fiber texture comprises refractory oxide fibers, and wherein the refractory particles are refractory oxide particles.

11. A method according to claim 1 , wherein a pressure less than or equal to 950 mbar is applied to the outlet vent during step c).

12. A method according to claim 1 , wherein the slip is injected under pressure during step b).

13. A method according to claim 12 wherein, during step b), the slip is injected at an injection pressure greater than or equal to 1.1 bar.

14. A method according to claim 1 , wherein the fiber texture is made directly as a single piece by three-dimensional weaving.

15. A method according to claim 1 , wherein at least one of the one or more injection ports is in front of the first face.

16. A method of fabricating a composite material part and including the following step:
sintering refractory ceramic particles present in a fiber preform, wherein the fiber preform is obtained by performing a process to form a refractory matrix in pores of said fiber preform, the process comprising
a) placing a fiber texture comprising refractory ceramic fibers in a mold cavity defined by a mold and a countermold;
b) injecting a slip comprising a powder of the refractory ceramic particles present in a liquid medium, the slip being injected into pores of the fiber texture present in the mold cavity, injection being performed through at least a first face of said fiber texture, wherein during step b), the slip is injected into the mold cavity through one or more injection ports, and prior to step b), the slip presents a volume content of refractory ceramic particles that is less than or equal to 40%; and
c) draining the liquid medium of the slip that has penetrated into the fiber texture through a porous material part having thickness greater than or equal to 0.1 mm, the draining being performed at least through a second face of the fiber texture different from the first face, the first face and the second face both extending from edge to edge, and each edge extending along a thickness of the fiber texture, said porous material part also serving to retain the powder of refractory ceramic particles in the pores of the fiber texture in order to obtain a fiber preform filled with refractory particles, the porous material part being present between the mold and the fiber texture or between the countermold and the fiber texture, and the porous material part being present between at least one outlet vent and the fiber texture, pumping being performed at the outlet vent in order to drain the liquid medium through said outlet vent.

Assignees

• Safran Aircraft Engines
• Safran

Inventors

• Billotte Cabre Catherine
• Droz Nicolas
• Liais Ludovic
• Podgorski Michael
• Ruiz Edu
• Turenne Sylvain

Classifications

• C04B2235/5224

  Alumina or aluminates · CPC title

• C04B35/62886

  by wet chemical techniques · CPC title

• D03D25/005

  Three-dimensional woven fabrics · CPC title

• C04B2235/5445

  submicron sized, i.e. from 0,1 to 1 micron · CPC title

• C04B35/14

  based on silica · CPC title