Hardness testing system using multiple depth measurements and related methods

Patent metadata

Field	Value
Publication number	US-10969317-B2
Application number	US-201816103147-A
Country	US
Kind code	B2
Filing date	Aug 14, 2018
Priority date	Aug 14, 2018
Publication date	Apr 6, 2021
Grant date	Apr 6, 2021

Abstract

An apparatus includes a holder to support an indenter relative to a sample, a depth sensor, and a controller. The operations include applying a first force on the sample with the indenter and determining a first depth of the indenter based on data generated by the sensor, moving the indenter from the first depth to a greater predetermined depth, then applying the first force on the sample with the indenter and determining a second depth of the indenter based on second data generated by the sensor, and determining a value indicative of hardness of the sample based on a difference between the first depth and the second depth. The apparatuses described can use a single scale for hardness that enables hardness values for different materials to be compared to one another.

First claim

What is claimed is:

1. An apparatus comprising:
a holder to support an indenter with respect to a sample of material;
a depth sensor; and
a controller to execute instructions for performing operations comprising
controlling the holder to apply a first force on the sample with the indenter and determining a first depth of the indenter based on first data generated by the depth sensor;
controlling the holder to move the indenter from the first depth to a second depth greater than the first depth, the second depth being a predetermined depth;
after the indenter is moved to the second depth, controlling the holder to apply the first force on the sample with the indenter and determining a third depth of the indenter based on second data generated by the depth sensor; and
determining a value indicative of hardness of the sample based on a difference between the first depth and the third depth.

2. The apparatus of claim 1 , further comprising a drive system configured to move the holder, wherein the depth sensor comprises an encoder coupled with the drive system.

3. The apparatus of claim 2 , wherein the first data and the second data generated by the depth sensor each comprise data indicative of a corresponding drive position of the drive system.

4. The apparatus of claim 1 , wherein the depth sensor comprises an optical sensor configured to detect a position of the indenter with respect to the sample.

5. The apparatus of claim 1 , wherein the first data and the second data generated by the depth sensor each comprise data indicative of a corresponding position of the indenter with respect to the sample or relative to a support configured to hold the sample relative to the indenter.

6. The apparatus of claim 1 , further comprising a force sensor to measure a force applied to the sample by the indenter.

7. The apparatus of claim 6 , wherein the first force is greater than a noise threshold of the force sensor.

8. The apparatus of claim 1 , further comprising a contact sensor to detect when the indenter contacts the sample,
wherein controlling the holder to apply the first force on the sample with the indenter and determining the first depth of the indenter comprises:
detecting, using the contact sensor, when the indenter contacts the sample, and
determining the first depth of the indenter when the indenter contacts the sample.

9. The apparatus of claim 8 , wherein the contact sensor is a conductivity sensor configured to detect a change in conductivity when the indenter contacts the sample.

10. The apparatus of claim 8 , wherein the contact sensor is a force sensor configured to detect a change in force when the indenter contacts the sample.

11. The apparatus of claim 1 , wherein controlling the holder to apply the first force on the sample with the indenter and determining the first depth of the indenter comprises controlling the holder to apply the first force with the indenter for less than 1 second.

12. The apparatus of claim 1 , further comprising a support to hold the sample such that the sample is prevented from rotating when the indenter applies a force to the sample.

13. The apparatus of claim 1 , wherein the predetermined depth is between 50 and 300 micrometers.

14. The apparatus of claim 1 , wherein:
controlling the holder to move the indenter from the first depth to the second depth comprises causing the indenter to apply a second force when the indenter is moved from the first depth to the second depth, and
the operations further comprise after controlling the holder to move the indenter from the first depth to the second depth, controlling the indenter to maintain the second force applied to the sample by the indenter for 2 to 15 seconds.

15. The apparatus of claim 14 , wherein:
controlling the holder to maintain the second force applied to the sample by the indenter for 2 to 15 seconds comprises causing the indenter to move from the second depth to a fourth depth, and
the operations further comprise determining a value indicative of creep based on a difference between the fourth depth and the second depth.

16. The apparatus of claim 15 , wherein the value indicative of hardness of the sample is a function of a difference between (i) the difference between the first depth and the third depth and (ii) the difference between the fourth depth and the second depth.

17. The apparatus of claim 1 , wherein the value indicative of hardness of the sample is a function of a difference between the first depth and the third depth.

18. A method of determining hardness of a sample, the method comprising:
applying, with an indenter, a first force on a sample and determining a first depth of the indenter;
moving the indenter from the first depth to a second depth greater than the first depth, the second depth being a predetermined depth;
after the indenter is moved to the second depth, applying, with the indenter, the first force on the sample and determining a third depth of the indenter; and
determining a value indicative of hardness of the sample based on a difference between the first depth and the third depth.

19. The method of claim 18 , wherein determining the first depth of the indenter comprises determining a position of the indenter based on data generated by an encoder coupled with a drive system configured to move a holder supporting the indenter.

20. The method of claim 18 , wherein determining the first depth of the indenter comprises determining a position of the indenter based on data generated by an optical sensor.

21. The method of claim 18 , wherein applying, with the indenter, the first force on the sample and determining the first depth of the indenter comprises:
detecting when the indenter contacts the sample, and
determining the first depth of the indenter when the indenter contacts the sample.

22. The method of claim 21 , wherein detecting when the indenter contacts the sample comprises detecting a change in conductivity in the indenter.

23. The method of claim 21 , wherein detecting when the indenter contacts the sample comprises detecting a change in force when the indenter contacts the sample.

24. The method of claim 18 , wherein applying, with the indenter, the first force on the sample and determining the first depth of the indenter comprises applying, with the indenter, the first force for less than 1 second.

25. The method of claim 18 , wherein the second depth is between 50 and 300 micrometers.

26. The method of claim 18 , wherein:
moving the indenter from the first depth to the second depth comprises causing the indenter to apply a second force when the indenter is moved from the first depth to the second depth, and
the method further comprises after moving the indenter from the first depth to the second depth, maintaining the second force applied to the sample by the indenter for 2 to 15 seconds.

27. The method of claim 26 , wherein:
maintaining the second force applied to the sample by the indenter for 2 to 15 seconds comprises causing the indenter to move from the second depth to a fourth depth, and
the method further comprises determining a value indicative of creep based on a difference between the fourth depth and the second depth.

28. The method of claim 27 , wherein the value indicative of hardness of the sample is a function of a difference between (i) the difference between the first depth

Assignees

• X Dev Llc

Inventors

• Smullin Sylvia Joan
• Grundmann Michael Jason

Classifications

• G01N3/068

  with optical indicating or recording means · CPC title

• G01N2203/0206

  Means for supplying or positioning specimens or exchangeable parts of the machine such as indenters... · CPC title

• G01N2203/0641

  using optical, X-ray, ultraviolet, infrared or similar detectors · CPC title

• G01N2203/021

  Treatment of the signal; Calibration · CPC title

• G01N3/42 Primary

  by performing impressions under a steady load by indentors, e.g. sphere, pyramid (G01N3/54 takes precedence) · CPC title