Multiple layer panels having reduced levels of edge defects

Patent metadata

Field	Value
Publication number	US-10946621-B2
Application number	US-201816002334-A
Country	US
Kind code	B2
Filing date	Jun 7, 2018
Priority date	Oct 8, 2013
Publication date	Mar 16, 2021
Grant date	Mar 16, 2021

Abstract

A process for producing a multilayer glass laminate panel having two glass sheets with a poly(vinyl butyral) interlayer sandwiched therebetween, the process comprising the steps of: providing two glass sheets; providing a poly(vinyl butyral) interlayer, and inserting the interlayer between the two glass sheets to produce a laminate; removing air from the produced laminate; applying heat and pressure to the laminate for a hold time, wherein the laminate is free of bubbles at the edges of the laminate. The multilayer glass laminate panel has improved optical properties, and specifically reduced levels of edge defects, such as edge bubbles in the laminate.

First claim

The invention claimed is:

1. A process for producing a multilayer glass laminate panel comprising two glass sheets with a poly(vinyl butyral) interlayer sandwiched therebetween, the process comprising the steps of:
providing two glass sheets;
providing a poly(vinyl butyral) interlayer, wherein said interlayer is tri-layer having two rigid skin layers and a soft core layer, where said skin layers have a glass transition temperature of from 30° C. or greater and said core layer has a glass transition temperature of less than about 4° C. and inserting the interlayer between the two glass sheets to produce a laminate;
removing air from the produced laminate; and
autoclaving the laminate for a hold time, wherein the heat is at a temperature in the range of from about 110° C. to about 155° C., the pressure is from 4.1 to about 6.9 bars, and the hold time is in a range of from about 10 minutes to about 60 minutes;

wherein the glass laminate panel is free of bubbles at the edges of the laminate panel;
and wherein the pummel adhesion rating ranges from 3 to 7.

2. The process of claim 1 , wherein the heat is at a temperature in the range of from about 115° C. to about 150° C.

3. The process of claim 1 , wherein the heat is at a temperature in the range of from about 130° C. to about 150° C.

4. The process of claim 1 , wherein the hold time is in a range of from about 20 minutes to about 40 minutes.

5. A process for producing a multilayer glass laminate panel comprising two glass sheets with a poly(vinyl butyral) interlayer sandwiched therebetween, the process comprising the steps of:
providing two glass sheets;
providing a multilayer poly(vinyl butyral) interlayer wherein said interlayer is tri-layer having two rigid skin layers and a soft core layer, where said skin layers have a glass transition temperature of from 30° C. or greater and said core layer has a glass transition temperature of less than about 4° C., and inserting the interlayer between the two glass sheets to produce a laminate;
removing air from the produced laminate; and
autoclaving the laminate for a hold time, wherein the heat is at a temperature in the range of from about 110° C. to about 155° C., the pressure is in a range of from about 4.1 to about 6.9 bars, and the hold time is in a range of from about 10 minutes to about 60 minutes and wherein the glass laminate panel is free of bubbles at the edges of the laminate panel and wherein the pummel adhesion rating ranges from 3 to 5.

6. The process of claim 5 , wherein the heat is at a temperature in the range of from about 130° C. to about 150° C.

7. The process of claim 5 , wherein the hold time is in a range of from about 20 minutes to about 40 minutes.

Assignees

• Solutia Inc

Inventors

• Lu Jun
• Aw Kok Leong William
• D'Errico John Joseph

Classifications

• B32B17/10036 Primary

  comprising two outer glass sheets · CPC title

• B32B17/10871

  in combination with particular heat treatment · CPC title

• B32B2605/00

  Vehicles · CPC title

• Y10T428/31627

  Next to aldehyde or ketone condensation product · CPC title

• B32B17/10761

  containing vinyl acetal · CPC title