Method for measuring amount of residual resin material in porous metal body

Patent metadata

Field	Value
Publication number	US-10908105-B2
Application number	US-201816142005-A
Country	US
Kind code	B2
Filing date	Sep 26, 2018
Priority date	Sep 29, 2017
Publication date	Feb 2, 2021
Grant date	Feb 2, 2021

Abstract

A differential thermal analysis of a plurality of metal-resin-containing layers, the resin material amounts of which are known and different from each other, is carried out. Heights of sample peaks observed at one temperature in the differential thermal analysis are measured, and a correlation between the resin material amounts and the sample peak heights is obtained. Then, a differential thermal analysis of a porous metal body is carried out, and a height of a peak observed at the same temperature is measured. An amount of a residual resin material in the porous metal body is obtained based on the measured height and the correlation.

First claim

What is claimed is:

1. A method for measuring an amount of a residual resin material in a porous metal body,
the porous metal body being prepared by forming a metal-resin-containing layer containing a metal material and a resin material having a melting point lower than a melting point of the metal material and by removing the resin material from the metal-resin-containing layer,
the method comprising:
a first thermal analysis step of carrying out a differential thermal analysis of a plurality of the metal-resin-containing layers, the resin material amounts of which are known and different from each other,
a correlation obtaining step of measuring heights of sample peaks observed at a temperature in the first thermal analysis step, to obtain a correlation between the resin material amounts and the sample peak heights,
a second thermal analysis step of carrying out a differential thermal analysis of the porous metal body, an amount of the residual resin material of which is not known, and
a residual amount measurement step of measuring a height of a peak observed in the second thermal analysis step at the same temperature as in the correlation obtaining step, to obtain the amount of the residual resin material in the porous metal body based on the measured peak height and the correlation.

2. The method according to claim 1 , wherein the first thermal analysis step and the second thermal analysis step are carried out in an oxidation atmosphere.

3. The method according to claim 1 , wherein the metal-resin-containing layer is a stack of a metal layer and a resin layer.

4. The method according to claim 3 , wherein the resin material is removed from the metal-resin-containing layer by a heat treatment.

5. The method according to claim 3 , wherein the metal-resin-containing layer is formed on a base.

6. The method according to claim 5 , wherein the metal material contains platinum, palladium, gold, rubidium, or an alloy thereof, and the base contains a carbon paper or a carbon cloth.

Assignees

• Honda Motor Co Ltd

Inventors

• WAKAKUWA Yu

Classifications

• H01M4/92

  Metals of platinum group (H01M4/94 {, H01M4/9058} take precedence) · CPC title

• H01M4/8621

  containing only metallic or ceramic material, e.g. made by sintering or sputtering · CPC title

• H01M4/8875

  Methods for shaping the electrode into free-standing bodies, like sheets, films or grids, e.g. moulding, hot-pressing, casting without support, extrusion without support · CPC title

• G01N25/22 Primary

  on combustion or catalytic oxidation, e.g. of components of gas mixtures · CPC title

• Y02E60/50

  Fuel cells · CPC title