Forming a surface layer on a ceramic matrix composite article

Patent metadata

Field	Value
Publication number	US-10774010-B2
Application number	US-201715499946-A
Country	US
Kind code	B2
Filing date	Apr 28, 2017
Priority date	May 2, 2016
Publication date	Sep 15, 2020
Grant date	Sep 15, 2020

Abstract

Techniques for infiltrating a CMC substrate may include infiltrating the CMC substrate with a first slurry to at least partially fill at least some inner spaces of the CMC substrate, where the first slurry includes first solid particles, drying the first slurry to form an infiltrated CMC including the first solid particles, depositing a second slurry including a carrier material and second solid particles on a surface of the infiltrated CMC, where the second solid particles include a plurality of fine ceramic particles, a plurality of coarse ceramic particles, and a plurality of diamond particles, drying the second slurry to form an article having an outer surface layer including the second solid particles on the infiltrated CMC, and infiltrating the article with a molten infiltrant to form a composite article.

First claim

What is claimed is:

1. A method comprising:
infiltrating a ceramic matrix composite (CMC) substrate with a first slurry, wherein the CMC substrate comprises a reinforcement material defining a plurality of pores and the first slurry at least partially fills some of the pores of the CMC substrate, and wherein the first slurry comprises a carrier material and first solid particles comprising a first ceramic material;
drying the first slurry to form an infiltrated CMC comprising the first solid particles;
depositing a second slurry comprising a carrier material and second solid particles on an outer surface of the infiltrated CMC, wherein the second solid particles comprise a plurality of fine ceramic particles defining a fine particle average size, a plurality of coarse ceramic particles defining a coarse particle average size, and a plurality of diamond particles, wherein the fine particle average size is less than the coarse particle average size;
drying the second slurry to form an article having an outer surface layer on the outer surface of the infiltrated CMC, the outer surface layer comprising the second solid particles, wherein the first solid particles define a first solid content percent within the pores of the CMC substrate, and wherein the outer surface layer defines a second solid content percent greater than the first solid content percent; and
infiltrating the article with a molten infiltrant to form a composite article.

2. The method of claim 1 , wherein drying the second slurry comprises wicking the carrier material of the second slurry into at least some of the pores of the CMC substrate.

3. The method of claim 1 , wherein a composition of the first slurry is different than a composition of the second slurry.

4. The method of claim 1 , wherein a composition of the first slurry is same as a composition of the second slurry.

5. The method of claim 1 , wherein at least one of the first ceramic material, the plurality of coarse ceramic particles, or the plurality of fine ceramic particles comprise at least one of boron carbide, silicon carbide, silicon nitride, or molybdenum carbide.

6. The method of claim 1 , wherein the second slurry comprises about 40 percent by volume (vol. %) to about 70 vol. % of the second solid particles.

7. The method of claim 1 , wherein the second solid particles comprise between about 1 percent by volume (vol. %) and about 10 vol. % of the plurality of diamond particles.

8. The method of claim 1 , wherein the second solid particles comprise between about 40 percent by volume (vol. %) and about 50 vol. % of the plurality of coarse ceramic particles, and comprise between about 40 percent by volume (vol. %) and about 59 vol. % of the plurality of fine ceramic particles.

9. The method of claim 1 , wherein drying the second slurry comprises using a mold to define the outer surface layer.

10. The method of claim 1 , wherein the molten infiltrant comprises silicon.

11. The method of claim 1 , wherein the second slurry defines a viscosity of less than about 1000 centipoise.

12. The method of claim 1 , further comprising mechanically smoothing the second slurry after depositing the second slurry and before the second slurry has dried.

13. The method of claim 1 , wherein drying the first slurry forms a first surface layer comprising the first solid particles on the CMC substrate.

14. The method of claim 1 , wherein a surface finish of the outer surface layer on the outer surface of the infiltrated CMC is smoother than a surface finish of the outer surface of the infiltrated CMC prior to deposition of the second slurry.

Assignees

• Rolls Royce High Temperature Composites Inc

Inventors

• Shim Sungbo
• Lazur Andrew Joseph
• Shinavski Robert

Classifications

• C04B35/5607

  based on refractory metal carbides · CPC title

• C04B35/563

  based on boron carbide · CPC title

• C04B35/584

  based on silicon nitride · CPC title

• C04B35/565

  based on silicon carbide · CPC title

• C04B35/80

  Fibres, filaments, whiskers, platelets, or the like · CPC title