Additive attachment on toner particles by plasma
US-9223237-B2 · Dec 29, 2015 · US
US10754270B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-10754270-B2 |
| Application number | US-201816492818-A |
| Country | US |
| Kind code | B2 |
| Filing date | Feb 15, 2018 |
| Priority date | Mar 17, 2017 |
| Publication date | Aug 25, 2020 |
| Grant date | Aug 25, 2020 |
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Provided is a toner including a binder resin, and a charge-controlling agent, wherein a volume average particle diameter X of the toner after a stress treatment satisfies Formula (1), and an amount Y of fine toner particles having particle diameters of 3 micrometers or smaller and circularity of 0.70 or less satisfies Formula (2).
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The invention claimed is: 1. A toner comprising: a binder resin; and a charge-controlling agent, wherein a volume average particle diameter X of the toner after a stress treatment below satisfies Formula (1) below, and an amount Y of fine toner particles having particle diameters of 3 micrometers or smaller and circularity of 0.70 or less satisfies Formula (2) below, 6.0 ≤X (micrometers)≤8.5 Formula (1) Y (% by mass)≤4.3 X (micrometers)−14.6 Formula (2) where the stress treatment includes charging a container formed of polypropylene having a volume of 100 mL with 5 g of the toner and 10 g of alumina beads having particle diameters of 0.5 mm, and shaking the toner by shaking the container using a shaker (YS-8D, available from YAYOI Co., Ltd.) with a stroke width of 80 mm, a stroke number of 250 times/min, and a shaking duration of 1 hour. 2. The toner according to claim 1 , wherein the amount Y of the fine toner particles satisfies Formula (3) below, Y (% by mass)≤3.8 X (micrometers)−14.6 Formula (3) 3. The toner according to claim 1 , wherein the amount Y of the fine toner particles satisfies Formula (4) below, Y (% by mass)≤3.2 X (micrometers)−14.6 Formula (4) 4. The toner according to claim 1 , wherein the charge-controlling agent includes an azo iron dye. 5. The toner according to claim 1 , wherein the toner includes a THF-insoluble component in an amount of 10% by mass through 40% by mass, a molecular-weight distribution of a THF-soluble component of the toner obtained by gel permeation chromatography (GPC) has a main peak between 10,000 and 16,000, where a half-value width of the main peak is a molecular weight of 60,000 through 90,000, and within the THF-soluble component of the toner, a component having a molecular weight of 2,000 or less as determined by GPC is from 15.0% by mass through 25.0% by mass and a component having a molecular weight of 100,000 or greater as determined by GPC is 10.0% by mass or less. 6. A toner production method comprising: kneading toner materials with melting the toner materials to obtain a melt-kneaded product; pulverizing the melt-kneaded product to obtain a pulverized product; and classifying the pulverized product obtained by the pulverizing, wherein the toner production method is a method for producing the toner according to claim 1 , a volume average particle diameter X of the toner after a stress treatment below satisfies Formula (1), and an amount Y of fine toner particles having particle diameters of 3 micrometers or smaller and circularity of 0.70 or less satisfies Formula (2). 7. An image forming method comprising: forming an image by one-component development using the toner according to claim 1 . 8. An image forming apparatus comprising: an electrostatic-latent-image bearer; an electrostatic latent image-forming unit configured to form an electrostatic latent image on the electrostatic-latent-image bearer; and a developing unit including a developer and configured to develop the electrostatic latent image with the developer to form a visible image, wherein the developer includes the toner according to claim 1 . 9. A process cartridge comprising: an electrostatic-latent-image bearer; and a developing unit including a developer and configured to develop an electrostatic latent image formed on the electrostatic-latent-image bearer with the developer to form a visible image, wherein the process cartridge is detachably mounted in a main body of an image forming apparatus, and the developer includes the toner according to claim 1 .
Post-treatment · CPC title
characterised by their structure; characterised by non-homogenuous distribution of components (microcapsular toners G03G9/093) · CPC title
Separation; Classifying · CPC title
characterised by their shape, e.g. degree of sphericity · CPC title
by mixing the toner components in a liquefied state; melt kneading; reactive mixing · CPC title
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