Method of manufacturing erasable toner

Patent metadata

Field	Value
Publication number	US-9217941-B2
Application number	US-201414152878-A
Country	US
Kind code	B2
Filing date	Jan 10, 2014
Priority date	Jan 17, 2013
Publication date	Dec 22, 2015
Grant date	Dec 22, 2015

Abstract

According to one embodiment, a method of manufacturing an erasable toner includes washing toner particles including therein a coloring material that is erasable by heating and a binder resin to obtain a toner cake having the amount of water of 20% by weight to 60% by weight, and drying the toner cake at 40° C. or more and at a temperature which is lower than the complete color erasing temperature of the toner particles by 30° C. or more.

First claim

What is claimed is:

1. A method of manufacturing an erasable toner comprising the steps of:
washing and compressing, in a filter press at a compression pressure between 0.05 MPa and 0.4 MPa, toner particles including a coloring material that is erasable by heating to a color erasing temperature and a binder resin to obtain a toner cake having an amount of water between 20% and 60% by weight, wherein the coloring material includes a coloring compound, a developer and a color erasing agent, and is encapsulated by a shell component; and
drying the toner cake at a temperature of 40° C. or more and at least 30° C. lower than the color erasing temperature.

2. The method of manufacturing an erasable toner according to claim 1 ,
wherein the drying comprises hot air drying by a flash jet method.

3. The method of manufacturing an erasable toner according to claim 2 ,
wherein a hot air speed in the flash jet method is between from 20 m/s and 100 m/s.

4. The method of manufacturing an erasable toner according to claim 2 ,
wherein the amount of toner being supplied per unit airflow during drying in the flash jet method is between 1 g/m 3 and 15 g/m 3 .

5. The method of manufacturing an erasable toner according to claim 1 , further comprising the step of:
incorporating hydrophobic silica and titanium oxide into toner particles obtained after the step of drying the toner cake.

6. A method of making an erasable toner, containing toner particle, comprising:
wet mixing a coloring material, a color developing material, a color erasing agent and a binder resin to form toner particles, the color erasing agent including a discoloring temperature regulating agent and being encapsulated by a shell component;
washing and compressing, in a filter press at a compression pressure between 0.05 MPa and 0.4 MPa, a mixture of the toner particles and water; and
drying the resulting mixture such that the resulting mixture has 0.1% by weight to 2.0% by weight of water as a percentage of the total weight of the mixture; wherein
no more than 20% of the resulting toner particles have a diameter of less than 2.5 μm; and
the mixture is dried without affecting the color rendering capability of the toner.

7. The method of making an erasable toner according to claim 6 , wherein, after the washing and compressing step, the resulting mixture has a water content between 20% and 60% by weight.

8. The method of making an erasable toner according to claim 7 , wherein the drying step occurs at a drying temperature at least 30° C. lower than the color erasing temperature of the toner, and at a temperature sufficient to dry the mixture to a water content less than 2.0% by weight without diminishing the color rendering capability of the toner.

9. The method of making an erasable toner according to claim 8 , wherein the drying step occurs at a temperature of at least 40° C.

10. The method of making an erasable toner according to claim 7 , further comprising the step of:
adjusting the liquidity and electrification characteristics of the toner particles.

11. The method of making an erasable toner according to claim 10 , wherein the step of adjusting the liquidity and electrification characteristics of the toner particles includes the step of incorporating an inorganic particulates into the mixture after the drying step.

12. The method of making an erasable toner according to claim 10 , further comprising the step of:
incorporating resin particles having a diameter of 1 μm or less into the mixture after the step of drying the mixture.

Assignees

• Toshiba Tec Kk

Inventors

• Itou Tsuyoshi
• Takeda Kazuhisa
• Noda Yasuhito
• Aoki Takayasu
• Ikuta Masahiro
• Hara Takafumi
• Udo Motonari

Classifications

• G03G9/0815

  Post-treatment · CPC title

• G03G9/081 Primary

  by mixing the toner components in a liquefied state; melt kneading; reactive mixing · CPC title

• G03G9/0926

  characterised by physical or chemical properties · CPC title

• G03G9/09708

  Inorganic compounds · CPC title

• G03G9/09725

  Silicon-oxides; Silicates · CPC title